The invention belongs to the technical field of
glycine preparation, and particularly discloses a preparation method of
glycine. The method comprises the following steps: controlling the
reaction temperature, efficiently synthesizing
ammonium chloroacetate from
chloroacetic acid and
liquid ammonia in a reactor, carrying out catalytic ammonolysis on the
ammonium chloroacetate and
ammonia gas in a reactor filled with a
solid catalyst to realize continuity and reinforcement of the process, and carrying out
alcohol precipitation crystallization, separation and purification to obtain
glycine. The
solid catalyst provided by the invention has the advantages of simple preparation, reproducibility, long service life, no
metal pollution, easily available raw materials, controllable cost, long-acting cyclic utilization, high efficiency, simple
recovery and the like; the method for preparing glycine by using the
solid catalyst solves the problems of high consumption, high
recovery cost, low production and purification efficiency and
pollution caused by the traditional catalyst, and is a key technology for green and low-cost industrial production of glycine.