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2563results about "Amino compound preparation" patented technology

Novel metal catalyst loaded by mesoporous carbon and preparation method thereof

ActiveCN102513099ANo obvious foaming phenomenonFoaming phenomenon does not decreaseCatalyst carriersOrganic compound preparationIonic liquidMonomer
The invention relates to a novel metal catalyst loaded by mesoporous carbon and a preparation method thereof. The metal catalyst is composed of 0.01-90 wt% of metal grains and 10-99.99 wt% of mesoporous carbon carrier, wherein the mesoporous carbon carrier is made of a heteroatom-doped mesoporous carbon material; the heteroatom-doped mesoporous carbon material is prepared by the following steps of: taking ionic liquid containing heteroatoms as a monomer and mixing the ionic liquid with a template agent at a room temperature; and then calcining the mixture at a temperature in a range of 400-1000 DEG C for 1-6 hours and cooling the mixture to the room temperature; and finally, removing the template agent to obtain the heteroatom-doped mesoporous carbon material. The average grain diameter of the metal grains is 1-100 nm and the mass percentage of the heteroatoms in the mesoporous carbon material is 0.01-80 wt%. The catalyst provided by the invention is good for enhancing the catalytic activity of the catalyst by adjusting the valence state of nano metal through doping the heteroatoms including nitrogen, sulfur, phosphorus, boron, fluorine and the like, and depositing and dispersing on the metal on the surface of the carrier. Furthermore, the catalyst is simple in preparation and is stable for water, air and heat.
Owner:ZHEJIANG UNIV

Method for synthesizing halogen aromatic amines by high-selectivity liquid phase hydrogenation under the condition of no solvent

The invention discloses a method for synthesizing halogen aromatic amines by halogen aromatic nitro compounds through liquid phase hydrogenation, which is characterized in that: the reaction for synthesizing the halogen aromatic amines by the halogen aromatic nitro compounds through liquid phase hydrogenation is carried out in the presence of a Pd/C catalyst under the condition of no solvent; and the method for preparing the Pd/C catalyst comprises the following steps of: performing impregnation pretreatment on active carbon by using aqueous solution of potassium halide, and filtering and washing until the filter liquor does not contain halide ions; preparing the pretreated active carbon into slurry by using de-ionized water, adding aqueous solution of HaPdCl4 dropwise for impregnation treatment, adjusting the pH value to alkali, and filtering and washing until the filter liquor is neutral; and preparing the obtained filter cakes into slurry by using de-ionized water, reducing in aqueous solution of reducing agent by a wet method, and filtering and washing until the filter liquor is neutral to obtain the Pd/C catalyst. The catalyst is adopted to prepare the halogen aromatic amines under the condition of no solvent, the selectivity is over 99.9 percent, the product quality meets the medical requirements, the production process is simplified, the production cost and energy consumption are reduced, the production efficiency is improved, and adverse factors such as solvent and product steam severely harming human bodies and polluting environment are improved.
Owner:ZHEJIANG UNIV OF TECH

Method for preparing tetrapropyl ammonium hydroxide by utilizing bipolar membrane electrodialysis

The invention discloses a method for preparing tetrapropyl ammonium hydroxide by utilizing bipolar membrane electrodialysis, and the method comprises the following steps of: using a tetrapropyl ammonium bromide aqueous solution as a raw material, processing the tetrapropyl quaternary ammonium salt aqueous solution through a microporous filter, and then enabling the processed tetrapropyl quaternary ammonium salt aqueous solution to enter a material liquid room of a bipolar membrane electrodialyzing device, respectively adding water in an acid room and an alkali room, respectively adding a sodium sulfate solution in pole liquid rooms, controlling the current density, the voltage and the temperature of the bipolar membrane electrodialyzing device to be 150-600 A/M2, 20-300 V and 5-45DEG C respectively, carrying out circulating cooling through chilled saline water in a circulating coil pipe by using an electrodialyzing compartment in a running process, stopping running when the conductivity of the material liquid room is decreased to below 2000 [mu]s/cm, obtaining a tetrapropylammonium hydroxide solution in the alkali room, and recycling a hydrobromic acid solution in the acid room. By using the method, the raw material cost is low; the selectivity is multiple; the purity of the tetrapropyl ammonium hydroxide is high; hydrobromic acid further can be recovered; and the generation of a pollutant in the process is effectively avoided.
Owner:ZHEJIANG UNIV OF TECH +1
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