The invention relates to the field of waste liquid treatment, and particularly discloses a DMF (
Dimethyl Formamide)-containing waste liquid
recovery process. The invention relates to a DMF-containing waste liquid
recovery process. The process comprises the following steps: S1, coarse
steaming treatment; s2, light component removal treatment; s3, heavy component removal treatment: adding an alkaline amine compound into the first kettle residual liquid obtained in S2, and heavy component removal; and S4, carrying out secondary coarse
steaming treatment to obtain a DMF product. In the
recovery process, the temperature, the pressure and the
ethanolamine addition amount of each process are precisely matched, so that the separation efficiency is ensured, the
energy consumption is reduced, closed-loop cooperation of
physical separation-
chemical corrosion prevention-secondary purification is formed, efficient recovery of DMF is realized, the recovery purity meets the industrial requirements, and the method is suitable for industrial production. Meanwhile, the equipment
corrosion contradiction in the high-temperature rectification process is effectively relieved, the process meets the industrial production requirement, high-purity DMF can be obtained, the recovery rate is not lower than 95%, and the purity is not lower than 99.9%.