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139results about How to "Facilitate rearrangement" patented technology

High speed pressing and forming method of warm powder and device thereof

InactiveCN101745638AIncrease the speed of warm pressingPromote particle rearrangementShock waveIntegrated technology
The invention discloses a high speed pressing and forming method of warm powder and a device thereof. The method is an integrated technology of warm-pressing as well as high speed pressing and forming, takes the gravitational potential energy of a drop hammer as pressing energy, a punch hammer falls down to impact on an upper punch to transfer the energy to the powder so as to rapidly and densely form the powder. The punch hammer rope of the device for carrying out the method is connected with a motor by a pulley installed above a guide cylinder and is kept to freely and vertically move in the guide cylinder; a speedometer is symmetrically installed on the two sides of a side die plate; a heating ring is directly sleeved on a die; a pressure sensor is contacted with the lower die punch and is connected with a data acquisition card; and the data acquisition card is connected with a computer by a USB interface. The pressing graph of a shock wave is displayed on the computer, and the maximum value of an impact force and the time impacting on the powder can be directly read from the graphs; and the invention has simple structure, convenient use, reliability and practicability as well as relative low price, is particularly suitable for colleges and universities as well as research and development institutions.
Owner:SOUTH CHINA UNIV OF TECH

Method for improving ceramic sintering performance by adding a small amount of polylactic acid in artificial bone prepared by laser

InactiveCN103467104APromote rearrangement and densificationImprove sintering performanceProsthesisBone tissue engineeringDisadvantage
A method for improving ceramic sintering performance by adding a small amount of polylactic acid in an artificial bone prepared by laser belongs to the field of bone tissue engineering. When a selective laser sintering (SLS) technology is used for preparing a porous biphasic calcium phosphate ceramic (BCP) artificial bone, a sintering part has the disadvantages of low density and insufficient mechanical properties, and the invention aiming at the disadvantages provides the method for improving BCP sintering performance by adding 0.1-1% by mass percentage of poly-L-lactic acid (PLLA). The advantages of the method are that: a transient liquid phase introduced by use of low temperature fusion of the PLLA can promote the rearrangement and densification of BCP particles so as to improve BCP sintering performance; the PLLA can be fully oxidized until complete disappearance under reasonable process parameters, PLLA residual in the artificial bone can be avoided, and finally the high-performance porous artificial bone completely made from BCP is prepared. The invention relates to the method for improving calcium phosphate bioceramic laser sintering performance by adding a small amount of a polymer material, and the method has the characteristics of simple operation process, good product performance and wide application range.
Owner:CENT SOUTH UNIV

Large-size high-density non-binding-phase tungsten carbide target material and preparing method thereof

The invention provides a preparing method of a large-size high-density non-binding-phase tungsten carbide target material. The method includes the following steps of S1, preparing materials; S2, conducting ball-milling and screening treatment; S3, conducting sintering treatment; S4, conducting after-treatment. The raw materials include tungsten carbide powder and free carbon. The dynamic vibrationpressure is exerted in the sintering treatment process. By introducing the free carbon into the pure tungsten carbide powder, traditional medical binding phases are abandoned, the purity of the target material is ensured, and the quality of a magnetron sputtering coating can be easily improved. The dynamic vibration pressure is introduced in the sintering process, particle rearrangement is promoted in the early sintering stage of the tungsten carbide powder, the removal of residual pores is promoted in the later sintering stage, and the grain is refined when the sintering density is improved;by means of the high-pressure vibration assisted sintering, the sintering temperature is lowered by 50-200 DEG C on the basis of a traditional hot pressing process, the tungsten carbide target material with high density and fine grain is prepared, and the film coating quality is improved.
Owner:株洲万融新材科技有限公司 +1

Production process of ultrathin aluminum nitride ceramic substrate

The invention relates to the technical field of aluminum nitride ceramics, and provides a production process of an ultrathin aluminum nitride ceramic substrate. The process comprises the following steps: (1) uniformly mixing aluminum nitride powder, a composite sintering aid, a UV monomer, a reactive diluent, a photoinitiator, a dispersant and a silane coupling agent to obtain ceramic slurry; (2) subjecting the ceramic slurry to tape casting on a tape casting machine, initiating a polymerization reaction through ultraviolet radiation, subjecting the slurry to in-situ curing molding to obtain a ceramic green body, and then cutting the ceramic green body into required shapes and sizes through a mold to obtain ceramic green sheets; (3) laminating the ceramic green sheets, and putting the laminated ceramic green sheets into a glue discharging furnace for glue discharging; and (4) carrying out hot pressed sintering on the ceramic blank sheet after glue discharging under the protection of nitrogen atmosphere, cooling to room temperature after the sintering, and then carrying out powder removal and polishing processes to obtain the ultrathin aluminum nitride ceramic substrate. The prepared aluminum nitride ceramic substrate is ultrathin, good in thermal conductivity and high in bending strength.
Owner:FUJIAN HUAQING ELECTRONICS MATERIAL TECH

Easy-to-tear polypropylene packing bag and manufacturing method thereof

The invention discloses an easy-to-tear type polypropylene packing bag and a manufacturing method thereof. The packing bag comprises a heat-seal layer which is made of polypropylene film through one-way orientation stretching. The manufacturing method comprises the following steps: firstly, polypropylene film which meets sanitary requirements is taken as the material, and one-way orientation stretching is performed to the polypropylene film after the polypropylene film is heated to 100 to 600 DEG C, and the stretch ratio is 1.1 to 5; secondly, temperature reduction treatment performed to the film which is processed through orientation stretching, concretely the temperature of the film which is processed through orientation stretching is quenched to the environment temperature; thirdly, corona treatment is performed to the film which is stretched, to ensure the surface tension of the film to be larger than 38 dynes, thereby a shaped easy-to-tear type polypropylene packing film is obtained, and is rolled; fourthly, the film is superposed on a required additional layer to obtain the wall layer of the packing bag, namely, a composite layer structure; and fifthly, the wall layer is folded and a plurality sides are sealed to form a bag shape with an opening to obtain a finished packing bag. When the packing bag is torn along the stretching direction of the heat-seal layer, the opening is in a straight-line shape.
Owner:ZHEJIANG GOLDSTONE PACKING

Method for forming nickel silicide with microwave annealing

The invention discloses a method for forming nickel silicide with microwave annealing. The method comprises the following steps of: pre-cleaning the surface of exposed silicon for removing natural oxide; depositing nickel or nickel alloy and coating a layer of barrier layer on the surface of the nickel or nickel alloy; utilizing microwave radiation so that a part of the nickel or nickel alloy is reacted with the silicon to form high-resistance one-silication two-nickel in the process of heating a wafer to a first temperature at the same time; removing the barrier layer of the surface of the nickel or nickel alloy and unreacted nickel or nickel alloy; and utilizing microwave radiation so that the high-resistance one-silication two-nickel is changed to low-resistance nickle silicide in the process of heating the wafer to a second temperature at the same time. In the method, the surface of a silicon wafer is radiated by utilizing the microwave during heating at the same time, therefore, the activity of atomic motion is improved, and atomic realignment is promoted. The first temperature for heating is reduced so that the first step of diffusion of nickel is limited. The activity of the atomic motion is improved on the basis of the second temperature, therefore, the atomic realignment is promoted, the uniformity of the nickle silicide is helped to be improved, and the performance of devices is improved.
Owner:SHANGHAI HUALI MICROELECTRONICS CORP

Method for preparing inorganic polymer composite material by low-temperature cold burning and ceramization application thereof

ActiveCN109437813ARealization of ceramic applicationLiquidPolymer scienceHigh energy
The invention discloses a method for preparing an inorganic polymer composite material by low-temperature cold burning and ceramization application thereof. The invention relates to a method for preparing an inorganic polymer composite material and the application thereof in order to solve the problems of low mechanical property and high sintering temperature of an existing inorganic polymer. Thepreparation method comprises the following steps: I, mixing a silicate powder, an aluminosilicate powder and a second phase material by adopting a high-energy ball milling process; II, adding water and a water reducing agent in to an inorganic polymer composite material dry powder, and mechanically stirring uniformly to obtain a plastic inorganic polymer green body; III, pressurizing and thermallyinsulating the green body, and controlling a pressure for pressure forming to be 250 to 600 Mpa; IV, putting a molded sample into an oven for curing to obtain the inorganic polymer composite material. The inorganic polymer composite material is subjected to high-temperature ceramization treatment at a temperature of 400 to 800 DEG C to obtain a ceramized product. The inorganic polymer composite material prepared by the method has excellent mechanical properties and low temperature for high-temperature ceramization.
Owner:HARBIN INST OF TECH

High-oxidation-resistance non-cement bonded Al2O3-SiC-C refractory castable and preparation method thereof

The invention discloses a high-oxidation-resistance non-cement-bonded Al2O3-SiC-C refractory castable and a preparation method thereof, and belongs to the field of amorphous refractory materials. The preparation method comprises the following steps: taking 50.0-60.0 wt% of brown fused alumina aggregate, 15.0-20.0 wt% of silicon carbide, 3.0-5.0 wt% of spherical asphalt, 5.0-10.0 wt% of corundum fine powder, 5.0-10.0 wt% of active alpha aluminum oxide micro powder, 3.0-5.0 wt% of mullite sol, 2.0-4.0 wt% of silicon micro powder, 0.5-2.0 wt% of lithium-containing aluminosilicate and 1.0-2.0 wt% of metal aluminum powder / monatomic silicon powder compound antioxidant as raw materials; and adding 0.20-0.30 wt% of a water reducing agent and 6-8wt% of water into the raw materials, carrying out stirring, pouring, molding, and subsequent heat treatment to obtain the high-oxidation-resistance non-cement-bonded Al2O3-SiC-C refractory castable for the large-scale blast furnace tapping channel. The prepared castable has extremely outstanding in oxidation resistance and excellent in normal-temperature / high-temperature mechanical property, thermal shock resistance and slag corrosion resistance, so that the safety coefficient and the service life of the tapping channel of the large blast furnace can be greatly improved, and the stable operation of the whole ironmaking process flow is guaranteed.
Owner:ANHUI UNIVERSITY OF TECHNOLOGY

High-specific-gravity tungsten-based alloy formation method based on pre-alloyed powder

The invention discloses a high-specific-gravity tungsten-based alloy formation method based on pre-alloyed powder. The high-specific-gravity tungsten-based alloy formation method based on the pre-alloyed powder comprises the steps that firstly, according to the designed ingredients and proportion of the high-specific-gravity tungsten-based alloy, material mixing, pressing, vacuum sintering and forging machining are sequentially conducted, then a tungsten-based alloy rod is obtained, and pre-alloyed powder is obtained through a plasma-rotating electrode powder manufacturing method; secondly, athree-dimensional model of the high-specific-gravity tungsten-based alloy is established, slicing and designing are conducted, and then slice layers and scanning data are obtained; thirdly, with the pre-alloyed powder as the raw material, according to the slice layers and the scanning data, a powder bed type electron beam additive manufacturing forming device is adopted to form the high-specific-gravity tungsten-based alloy. According to the high-specific-gravity tungsten-based alloy formation method based on the pre-alloyed powder, by utilizing the different melting points between tungsten and other elements in the high-specific-gravity tungsten-based alloy, the pre-alloyed powder with tungsten powder particles being wrapped inside low-melting-point element solid solution is prepared, sothat the shells of the pre-alloyed powder are easy to melt and adhere to one another for formation, and therefore the formation difficulty of the pre-alloyed powder is lowered; and with the pre-alloyed powder as the raw material, preparation of the high-specific-gravity tungsten-based alloy is achieved.
Owner:NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH

Method for preparing high-performance cementing material from modified calcium-magnesium phosphate rock tailings

The invention provides a method for preparing a high-performance cementing material from modified calcium-magnesium phosphate rock tailings. The method comprises the following steps: separating out aphosphate tailing sample with the particle size of 20 [mu]m or less for later use; sequentially carrying out magnesium flotation and phosphorus flotation on slime with the particle size of 20 [mu]m orabove, and dividing the slime into three parts, namely a magnesium-calcium component, a phosphorus component and a siliceous component; calcining the magnesian component, stirring and mixing the partof which the MgO grade is lower than 20%, the siliceous component and slime of which the particle size is less than 20 [mu]m, and aging and calcining to obtain clinker; and cooling the calcined clinker to room temperature under a dry condition, adding silica fume, mineral powder, carbide slag, sodium metaaluminate, polyaluminium chloride and a water reducing agent modifier, and preparing the cementing material at a certain water-cement ratio. The phosphate tailings are treated and then combined with different components to obtain the phosphate tailing-based cementing material, so that industrial solid wastes which are the phosphate tailings are changed into a characteristic resource and are completely and comprehensively utilized, the purpose of zero emission of the phosphate tailings isachieved, and green development and sustainable development of phosphorus chemical enterprises are promoted.
Owner:湖北冶金地质研究所

Rapid sintering equipment for dynamically loading coupling alternating current and sintering method

The invention relates to rapid sintering equipment for dynamically loading coupling alternating current. The rapid sintering equipment comprises the following components including a furnace frame, a dynamic loading system,a sintering control system and an alternating current control system; a furnace body is arranged in the furnace frame, and a closed pressure maintaining cabin is formed in the furnace body; the dynamic loading system comprises a dynamic loading generation part and a dynamic loading control part, and the dynamic loading generation part is arranged in the pressure maintaining cabin and used for heating a sintering material; the dynamic loading control part is arranged outside the pressure maintaining cabin, the output end of the dynamic loading control part is connected with the dynamic loading generation part, and the dynamic loading control part is used for outputting coupled total dynamic loading to the dynamic loading generation part; the sintering control system isarranged outside the pressure maintaining cabin, and the output end of the sintering control system is connected with the input end of the dynamic loading control part; and the alternating current control system is arranged outside the pressure maintaining cabin, the input end of the alternating current control system is connected with the output end of the sintering control system, and the output end of the alternating current control system is connected with the dynamic loading generation part. The equipment can remarkably improve the sintering driving force, inhibit grain growth, improve the density of a sintered body and improve the material performance.
Owner:TSINGHUA UNIV
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