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25576results about How to "Ease of industrial production" patented technology

Titanium carbonitride based metal ceramic based on high-entropy alloy binder phase and preparation method of metal ceramic

Disclosed is a titanium carbonitride based metal ceramic material based on a high-entropy alloy binder phase. The binder phase of the titanium carbonitride based metal ceramic material is high-entropy alloy, the hard phase of the titanium carbonitride based metal ceramic material is carbonitride solid solution, the high-entropy alloy binder phase includes at least four of ferrum, cobalt, nickel, chromium, aluminum, vanadium, titanium, copper, zirconium, molybdenum, manganese and rare earth elements, and the molar content ratio of each element ranges from 5% to 35%. In a preparation method, the titanium carbonitride based metal ceramic material based on the high-entropy alloy binder phase comprises raw materials including, in weight percent, 3-30% of the high-entropy alloy binder phase, 0-30% of second carbide powder and the balance carbonitride solid solution powder, the carbonitride solid solution powder includes at least one of Ti (Cx, N1-x), (Ti, M1...) and (Cx, N1-x), the M1 component of the (Ti, M1...) and (Cx, N1-x) includes at least one of W, Mo, Ta, Nb, V, Cr, Zr, Hf, Y and lanthanide, and 0<x<1 in the Ti (Cx, N1-x), (Ti, M1...) and (Cx, N1-x). The preparation method includes the process steps of (1) ball-milling mixing, (2) forming and (3) low-pressure sintering.
Owner:SICHUAN UNIV

Method for extracting cannabidiol from cannabis

The invention discloses a method for extracting cannabidiol from cannabis. The method comprises the following steps: smashing and drying extraction fractions of cannabis to obtain medicine material powder; extracting the medicine material powder with 30% to 100% (V / V) of ethanol to obtain an extracting solution; concentrating the extracting solution to obtain an extract; carrying out water precipitation on the extract, and removing impurities to obtain a water precipitation solution; centrifuging the water precipitation solution and adding 10% to 100% (V / V) of ethanol into an obtained precipitate, and dissolving the precipitate to obtain an alcoholic solution of the precipitate; carrying out column chromatography on the alcoholic solution of the precipitate; eluting an obtained eluant after the concentration column chromatography, and adding ethanol for supersaturated dissolution to obtain a crystal substance; adding the crystal substance into purified water or ethanol for washing to obtain a primary product; blending the primary product with purified water, and drying to obtain the cannabidiol. Only highly safe ethanol is adopted as a solvent, the purity of the cannabidiol in a finished product is improved, and the psychotoxic component of tetrahydrocannabinol is also removed, so that the product safety is improved, and the method is applicable for industrial production.
Owner:YUNNAN HANSU BIO TECH CO LTD

Normal-temperature synthesis method for polycarboxylic acid water-reducing agent

The invention discloses a normal-temperature synthesis method for a polycarboxylic acid water-reducing agent, and belongs to the field of cement concrete water-reducing agents. The water-reducing agent is prepared by the following steps of: copolymerizing polyoxyethylene ether monomer or polyoxyethylene ester monomer a containing unsaturated double bonds, unsaturated monocarboxylic acid and derivative monomer thereof b, unsaturated dicarboxylic acid c and unsaturated sulfonic acid or salt monomer thereof d in aqueous solution under the action of an oxidation reduction initiator, and finally neutralizing the solution by using alkali solution to obtain the water-reducing agent. The reaction can be performed at room temperature by adopting an oxidation reduction initiating system, and the appropriate reaction temperature is between 5 and 30 DEG C; and the synthesis process does not need heating, so energy is saved, and high-temperature side reaction is effectively controlled. The prepared polycarboxylic acid high-performance water-reducing agent has the characteristics of high water-reducing rate and good collapse protecting performance. The water-reducing agent has wide application range, and the method has low production process requirement and is suitable for industrialized large-scale production.
Owner:BEIJING UNIV OF TECH

Nanometer lithium titanate/graphene composite negative electrode material and preparation process thereof

The invention relates to the field of negative electrode materials of lithium ion batteries, and specifically to a nanometer lithium titanate/graphene composite negative electrode material and a preparation process thereof. According to the invention, micron-sized lithium titanate prepared by the solid phase method is subjected to ultrafine ball milling to obtain nanometer powder, and the nanometer lithium titanate powder and graphene are uniformly compounded and subjected to heat treatment so as to obtain a high performance lithium ion battery negative electrode material; the invention is characterized in that uniform distribution of graphene in the nanometer lithium titanate powder is realized through in situ compounding; the weight of graphene in the composite negative electrode material accounts for 0.5 to 20%, and the weight of lithium titanate accounts for 80 to 99.5%. The lithium ion battery negative electrode material has good electrochemical performance, 1C capacity greater than 165 mAh/g, 30C capacity greater than 120 mAh/g and 50C capacity greater than 90 mAh/g. Nanometer lithium titanate in the lithium ion battery negative electrode material prepared in the invention has high phase purity; the preparation process of the material is simple and is easy for industrial production.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Graphene/polysiloxane composite coating material and preparation method thereof

The invention provides a graphene / polysiloxane composite coating material and a preparation method thereof. The method comprises the following steps: modifying the graphene surface with active groups by a chemical modification technique to obtain modified graphene, mixing the modified graphene with a silane compound, a dispersion medium, a non-essential comonomer and a non-essential accelerator, and carrying out hydrolytic condensation or hydrolytic condensation-free radical polymerization to generate a graphene / polysiloxane composite resin in situ; and mixing the resin with a non-essential blend resin, a non-essential curing agent, a non-essential solvent, a non-essential pigment and filler and a non-essential aid, and carrying out physical blending, amino epoxy addition reaction, Michael addition reaction and the like to form a film, thereby obtaining the graphene / polysiloxane composite coating material. The uniformly dispersed graphene lamellae and polysiloxane have strong interface effects, also have the gas / liquid barrier and heat shielding effects, and endow the coating with excellent corrosion resistance, flame retardancy and the like, thereby greatly enhancing the mechanical properties, corrosion resistance, scratch resistance, wear resistance and the like of the coating.
Owner:FUDAN UNIV

Method of preparing taurine

The invention relates to method for preparing taurine, comprising the following steps: (1) reacting epoxy ethane with sodium sulfite under 0.05 to 0.1MPa, with pH value of 6.5 to 7.5 and at temperature between 75 and 85 DEG C to obtain hydroxyethyl sodium sulfonate; (2) carrying out ammonolysis reaction on the hydroxyethyl sodium sulfonate and liquid ammonia under 14 to 21MPa and at temperature between 160 and 280 DEG C to obtain ammonolysis solution containing sodium taurate; (3) introducing the ammonolysis solution into a single flash evaporator for primary flash evaporating at a temperature between 160 and 200 DEG C and under 1.3 to 2.0MPa; introducing the flash evaporated liquid into a secondary flash evaporating and falling film evaporator, using the primary flash vapor as a heating medium to carry out flash evaporating and falling film evaporating on the primary flash evaporated liquid in the secondary flash evaporating and falling film evaporator at a temperature between 110 and 140 DEG C and at 0.1 to 0.6MPa; evaporating and concentrating the flash evaporated liquid subjected to secondary flash evaporating and falling film evaporating with flash vapor and steam as heating media in a multi-effect flash evaporating and falling film evaporator; and (4) neutralizing the sodium taurate by sulphuric acid to obtain the taurine. The method for preparing the taurine has the advantages of short time, high yield and low cost, and is easy for industrialized production. In addition, by primary flash evaporating and secondary flash evaporating processes, almost all the ammonia and 40% to 60% of water in the flash evaporated liquid can be removed, thus having double effects of removing ammonia and condensing.
Owner:王代龙 +1
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