1194 results about "Nickel alloy" patented technology

The invention discloses a laser cladding preparation method for improving the wear resistance of a cladding layer by doping tungsten carbide. According to the method, cladding process parameters are preliminarily obtained based on finite element heat flow analogue simulation, cladding layer preparation is carried out, cladding quality characterization is carried out to obtain the optimal cladding process parameters, and finally the cladding layer with the wear-resistant characteristic is obtained. The method comprises the following steps: firstly, constructing a heat flow coupling three-dimensional model, carrying out grid division, establishing a heat source model, defining thermophysical parameters of tungsten carbide (10-15%) nickel alloy composite powder and a matrix, and determining simulated boundary conditions; setting a multi-factor process parameter combination to carry out numerical simulation calculation, and determining laser processing process parameters of laser power, scanning speed and light spot diameter; preparing a cladding layer on the surface of the nodular cast iron by using tungsten carbide (10-15%) nickel alloy composite powder through a laser cladding method; and carrying out microscopic morphology and microhardness experiments to carry out quality analysis verification on the cladding layer, determining the optimal process parameters of laser power, scanning speed and light spot diameter when the cladding layer has no obvious defect morphology and the hardness is higher than that of the raw material, and obtaining the laser cladding preparation method for improving the wear resistance of the cladding layer by doping tungsten carbide. The invention provides a new research method and a high-quality preparation approach for improving the wear resistance of the cladding layer by tungsten carbide, and can be widely applied to the fields of strengthening and repairing mining machinery, aerospace parts and the like.

The invention relates to a high-frequency and high-performance iron-nickel alloy magnetic powder core and a preparation method and application thereof, belongs to the field of metal magnetic powder cores, and solves the problems that in the prior art, when a metal magnetic powder core is applied at high frequency, high magnetic conductivity, high magnetic conductivity stability and high quality factor are difficult to consider, and the saturation flux density is low. And the preparation process is tedious. The invention discloses a preparation method of a high-frequency high-performance iron-nickel alloy magnetic powder core. The preparation method comprises the following steps: S1, preparing raw materials; s2, performing pretreatment; s3, the pretreated iron-nickel alloy powder and nano SiO2 powder are blended, and inorganic insulation coating powder is obtained; s4, adding the inorganic insulating coating powder into a first coating agent to obtain inorganic and first organic insulating coating powder; s5, adding the inorganic and first organic insulation coating powder into a second coating agent to obtain inorganic and double-layer organic insulation coating powder; and S6, compression molding. The comprehensive magnetic performance of the iron-nickel magnetic powder core is improved, and the preparation process is simplified.

The invention relates to the technical field of hydraulic test of nickel alloy pipes, and discloses a hydraulic test system for a thin-wall nickel alloy pipe. According to the system, in the axial loading state of the thin-wall nickel alloy pipe, a closed water pressure cavity is established through an annular sealing clamp, and then strain distribution data on the surface of the pipe body is collected through a distributed optical fiber sensor array. And constructing a three-dimensional stress field reconstruction model based on the acquired strain distribution data, calculating an equivalent plastic deformation threshold value of the pipe body under different water pressure gradients, adjusting a water pressure loading curve slope parameter according to the equivalent plastic deformation threshold value, and generating a dynamic water pressure loading instruction. And the high-frequency pressure pulse generator executes the instruction, synchronously triggers the X-ray diffractometer to collect lattice distortion data of the tube body, inputs the data into the material microscopic damage evolution model, and outputs a microscopic defect spatial distribution map. And finally, material constitutive parameters of the three-dimensional stress field reconstruction model are corrected based on the atlas, closed-loop feedback control is formed, and multi-dimensional data acquisition and accurate management and control of the thin-wall nickel alloy pipe hydrostatic test are achieved.

The invention belongs to the field of electrical electronics and advanced non-ferrous metal additive manufacturing, and particularly relates to a preparation method of a laser additive manufacturing copper alloy-tungsten copper composite electrical contact, which comprises the following steps of: preparing a nickel or nickel alloy coating on a copper alloy base material by adopting coaxial powder feeding laser cladding to serve as a middle layer, and then preparing a tungsten copper coating by laser cladding to obtain the copper alloy-tungsten copper composite electrical contact. The composite electrical contact is composed of a pure copper or copper alloy base material layer, a pure nickel or nickel alloy coating and a tungsten copper coating in sequence. The electrical contact obtained by the invention has relatively high electrical conductivity and thermal conductivity, and also has good arc ablation resistance; the copper alloy-tungsten copper electrical contact is prepared by adopting the laser cladding technology, so that the production cost can be effectively reduced, the production efficiency is improved, meanwhile, later maintenance and repair are facilitated, and the method is green and environment-friendly.

The invention discloses a special composite enamel coating for a chromium-nickel alloy base material and a preparation method of the special composite enamel coating, when the special composite enamel coating structurally comprises one layer, the special composite enamel coating comprises the following components in parts by mass: 40-65 parts of a basic glass phase, 30-55 parts of a high-melting-point ceramic reinforced phase, 2-10 parts of a thermal expansion coefficient regulator and 0.5-5 parts of an interface bonding accelerant. Compared with the prior art, the enamel coating can achieve nearly perfect thermal expansion coefficient matching with a chromium-nickel alloy matrix, a tough chemical bonding interface is formed, the enamel coating can stably work for a long time in the extreme high-temperature environment of 1,100 DEG C or above, and meanwhile the enamel coating has the excellent abrasion resistance, repeated rapid cooling and rapid heating cycle resistance and thermal shock resistance.

The invention discloses a cathode roller with a honeycomb surface structure. A precise honeycomb micro-pattern structure is arranged on the surface of the cathode roller. The invention also discloses a method for manufacturing alloy foil by using the cathode roller, which comprises the following steps: dissolving ferric salt in ultrapure water to obtain a ferric salt solution; dissolving nickel salt in ultrapure water to obtain a nickel salt solution; mixing the two solutions and filtering; preparing various additive solutions, mixing all the additive solutions with the obtained iron-nickel solution to obtain an electrolyte, filtering the electrolyte, and transferring the filtered electrolyte into an electrolytic cell of a crude foil engine; and applying current to a cathode roller and an anode plate which are separately arranged in the electrolytic bath, electrically depositing iron and nickel on the surface of the cathode roller, and rolling through a roll-to-roll process to obtain the iron-nickel alloy foil. The alloy foil manufactured by the method has the characteristics of low surface roughness, high tensile strength and high ductility.

The invention relates to a method for manufacturing a bipolar plate (2), comprising the following steps: - Provision of two steel half-sheets (3, 4), wherein at least one of the two half-sheets (3, 4) has an embossed structure (5), - Construction of a three-dimensional metal structure (7) from at least one powder (12) of a metal different from the steel of the half-sheets (3, 4), wherein the metal is selected from the group comprising titanium, titanium alloys, nickel, nickel alloys, chromium, chromium alloys, ferrochrome alloys, copper, copper alloys, silver, silver alloys, or gold, platinum, iridium, rhodium, ruthenium and their alloys, on a first half-sheet (3) of the two half-sheets (3, 4) by means of a laser (10) with green laser light and consequently a wavelength in the range of 495 nm to 550 nm, and - Forming a material-bonded connection of the 3D metal structure (7) with a second half-sheet (4) of the two half-sheets (3, 4) using the same laser (10), wherein the half-sheets (3, 4) are joined to form a bipolar plate (2). The invention further relates to a bipolar plate (2) for an electrochemical cell (20).

The invention discloses a comprehensive recovery method for copper-nickel concentrate, which comprises the following steps: smelting the copper-nickel concentrate to obtain smelting slag and high-nickel copper matte which are layered up and down; performing side-blowing converting on the air-quenched and granulated high-nickel copper matte to obtain high-nickel converting slag which is layered up and down and qualified crude copper; the liquid smelting slag and the high-nickel converting slag are mixed for two-step reduction smelting, iron slag and copper-nickel alloy which are layered up and down are obtained through weak reduction, and reducing slag and molten iron which are layered up and down are obtained through strong reduction. According to the method disclosed by the invention, one-step removal of the Ni element is realized through side-blowing reinforced stirring of the granulated copper matte, so that application of the high-nickel copper concentrate to large-scale continuous copper smelting becomes possible. And meanwhile, through cooperative treatment of the smelting slag and the converting slag, short-process comprehensive recovery of Cu, Ni and Fe elements is achieved. The deeply depleted tailings are subjected to water quenching to form a calcium-silicon glass body which has a curing effect on heavy metal ions and is a high-quality building raw material, high-valued and full-quality utilization of mineral resources is realized, and the method is a brand-new technical route for widening the application range of raw materials, reducing cost and improving efficiency in a copper smelting plant.

The invention relates to the technical field of iron-nickel alloy foil preparation, and discloses a low-curl iron-nickel alloy foil suitable for an all-solid-state battery and a preparation method of the low-curl iron-nickel alloy foil. The electrolyte solution is added into an electrolytic cell, and current is applied to the electrolyte solution; the method comprises the following steps: depositing an iron-nickel alloy on the surface of a cathode roller, stripping to obtain an iron-nickel alloy foil, carrying out electrophoresis on the iron-nickel alloy foil by using a magnesium oxide electrophoresis solution in an electrophoresis cell to form a magnesium oxide coating on the iron-nickel alloy foil, cleaning with an acid solution, and carrying out electrochemical fluorination treatment on the iron-nickel alloy foil to obtain the magnesium oxide coating on the iron-nickel alloy foil. Forming a fluorinated layer on the magnesium oxide coating; and the iron-nickel alloy foil is subjected to heat treatment at the temperature not exceeding 600 DEG C in a heat treatment chamber, and the iron-nickel alloy foil is obtained after cooling. The high-quality iron-nickel invar iron-nickel alloy foil can solve the curling problem and is suitable for all-solid-state batteries.

The invention provides a copper-nickel alloy foil and a preparation method and application thereof, and belongs to the technical field of lithium ion battery negative electrode current collectors, and the preparation method comprises the following steps: preparing a copper-nickel composite electrolyte, and adding a coordination agent, a pH buffer agent and an additive into the copper-nickel composite electrolyte to obtain a mixed electrolyte; the coordination agent comprises a main coordination agent and an auxiliary coordination agent, and the main coordination agent comprises at least one of trisodium citrate, potassium sodium tartrate and sodium pyrophosphate; the auxiliary coordination agent comprises at least one of ammonia water, glycine and triethanolamine; and a cathode and an anode are placed in the mixed electrolyte, the pH of the mixed electrolyte is controlled to be 6-10, direct current is applied for electrochemical deposition, and the copper-nickel alloy foil is obtained. According to the method, the alkalescence system is adopted, the main coordination agent and the auxiliary coordination agent are used, full coordination of free Cu < 2 + > and Ni < 2 + > is achieved, precipitation is avoided, the hydrogen evolution phenomenon is greatly reduced, and the alloy foil quality is improved.

A firearm suppressor is provided, including a tubular core, a baffle carried within the core, and a tubular mount. The core may be attached end-to-end to the mount. A cap may be attached end-to-end to the core opposite the mount. An intermediate member may be included, extending between the mount and the cap, and residing outboard of the core. The intermediate member may be welded to the mount and to the cap. The mount, the cap, and the intermediate member may be composed of one or more of titanium, aluminum, resins, polymers, composites, carbon fiber, and ceramics, whereas the core and the baffle may be composed of one or more of cobalt, nickel alloy, steel, stainless steel, and cobalt alloy.

The invention relates to the field of electrochemical polishing of cobalt-based alloys, in particular to an environment-friendly electrochemical polishing solution of a cobalt-chromium-tungsten-nickel alloy and a polishing method of the environment-friendly electrochemical polishing solution. The cobalt-based alloy comprises the following chemical elements in percentage by mass: 15.0-25.0% of Cr; w: 10.0% to 20.0%; 0.0% to 15.0% of Ni; the balance is Co and unavoidable impurity elements such as O, N and H. The environment-friendly polishing solution comprises the following chemical components by mole percent: 0.5-2 mol / L of ChCl; 0.7 to 1.0 L of ethylene glycol; 0 to 0.3 L of ethanol; 0.1 to 0.3 L of glacial acetic acid; and a small amount of citric acid. According to the electrolytic polishing, alloy serves as an anode, a U-shaped titanium plate serves as a cathode, the voltage is 40-60 V, the current density is 0.5-2 A / cm < 2 >, and the polishing temperature is normal temperature. The method has the advantages that the environment-friendly electrolyte is adopted, the surface of the cobalt-chromium-tungsten-nickel alloy can be polished, pollution caused by electrolyte of a traditional chromium oxide system and an acid system is avoided, the follow-up repeated cleaning procedure is reduced, and material precision control is improved.

The invention discloses a preparation method of an ultra-large-diameter copper-nickel alloy seamless tube, which comprises the following steps of: obtaining a cold-rolled raw material which is uniform in internal structure and free from pores by using forging and cross piercing methods, and then performing cold rolling to eliminate an as-cast state, performing hot working on the structure to fully refine crystal grains and drawing the raw material which meets the equipment requirements in diameter and wall thickness; the large-diameter seamless pipe with the diameter of 508 mm is prepared, and the produced large-diameter seamless pipe is excellent in mechanical performance, uniform in grain size and internal structure and high in practicability and economic benefits.

The invention discloses a production process of a novel copper-based alloy bimetallic synthesis material, and relates to the field of alloy materials.The production process comprises the steps that a copper-nickel alloy is selected as a base material, a titanium alloy is selected as a functional layer, and stress distribution of a bonding layer is designed and optimized through gradient component distribution; preparing a copper-nickel alloy liquid by utilizing vacuum induction melting, supporting and fixing a core rod through three points, and controlling temperature and flow velocity for pouring to form co-growth crystals; the surface of the base material is cleaned through a sand blasting process, a Cu-Ti nano coating is coated through a PVD technology, and a nanoscale convex-concave structure is formed; building a mathematical model of a temperature field and a component diffusion field, and optimizing and combining area temperature distribution and diffusion behaviors through simulation analysis; through gradient temperature control annealing treatment, residual stress is eliminated, and diffusion is promoted; the bonding performance is evaluated by combining shear strength and microhardness tests; and dividing the production process based on the modular design. The method can be widely applied to the industrial fields with high-temperature, high-strength and corrosion-resistant requirements.

The invention discloses conductive paste, a crystalline silicon solar cell and a preparation method of the crystalline silicon solar cell, and belongs to the technical field of photovoltaic cells. The conductive paste comprises glass powder which accounts for 1.5 wt%-6 wt% of total solids in the conductive paste; an organic carrier accounting for 9 wt% to 15 wt% of total solids in the conductive paste; a first conductive metal, which accounts for 70 wt% to 88 wt% of total solids in the conductive paste; a second conductive metal which accounts for 1 wt% to 10 wt% of the total solid content in the conductive paste; wherein the specific surface area of the second conductive metal is larger than 0.5 m < 2 > / g and smaller than 1.8 m < 2 > / g, and the second conductive metal is selected from nickel or nickel alloy. The nickel or the nickel alloy with the specific surface area is adopted to replace part of silver, the influence on the density of a sintered silver structure and the conductivity of a silver / nickel electrode can be reduced, the photoelectric conversion efficiency of the solar cell can be maintained by adding the nickel powder, and the preparation cost of the solar cell can be reduced by reducing the use amount of the silver.

The invention discloses a seawater conductivity sensor electrode material based on a copper-nickel-based nanostructure and a preparation method, the electrode material comprises: a substrate, a copper-nickel-based nanostructure layer being formed on the surface of the substrate; the substrate comprises an insulating compound and a coating coated on the surface of the insulating compound, the insulating compound comprises at least one of high-resistance silicon, silicon oxide, aluminum oxide ceramic and plastic, the coating comprises a metal coating and / or a semiconductor coating, and the copper-nickel-based nanostructure layer is in a dendritic crystal or cluster form. The copper-nickel alloy nanostructure is a core material of the electrode, so that the electrode material has high specific surface area and rich active sites, the measurement accuracy and measurement limit of the electrode material can be improved, the service life can be prolonged, the manufacturing cost can be reduced, and the application requirements of the ocean Internet of Things can be met.

The invention relates to normalized high-strength medium-carbon acid-resistant container steel and a preparation method, and belongs to the technical field of steel manufacturing. The acid-resistant container steel comprises the following chemical components in percentage by mass: less than or equal to 0.20% of C, less than or equal to 0.55% of Si, 1.20-1.70% of Mn, less than or equal to 0.025% of P, less than or equal to 0.010% of S, less than or equal to 0.050% of Nb, less than or equal to 0.050% of V, less than or equal to 0.030% of Ti, more than or equal to 0.020% of Al, less than or equal to 0.0060% of Ca and a matrix element Fe. A proper amount of Nb (niobium), V (vanadium) and Ti (titanium) alloy elements are added to replace a traditional Cu (copper) and Ni (nickel) alloy combination, and the alloy component cost is greatly reduced while high strength and acid resistance are guaranteed.

The invention belongs to the field of metal material processing, and particularly relates to a high-strength high-temperature nickel alloy welding material and a preparation method thereof.The high-strength high-temperature nickel alloy welding material comprises, by weight, 0.02%-0.05% of C, 0.10%-0.20% of Si, 18.0%-22.0% of Cr, 7.0%-9.0% of Fe, 4.0%-6.0% of Co, 2.0%-4.0% of W, 3.0%-6.0% of Mo, 0.005%-0.010% of B, 0.5%-2.5% of the total amount of Al and Ti, 0.05%-0.08% of Zr, 2.0%-2.5% of Nb, 0.30%-0.40% of RE, smaller than 0.005% of S, smaller than 0.005% of P, 1.5%-4.0% of modified boron nitride mixed powder and the balance Ni, the high-strength and high-temperature nickel alloy welding material is obtained through hot working, heat treatment, surface treatment and coating preparation, and the problem that in the prior art, deposited metal formed after welding of the high-strength and high-temperature nickel alloy welding material is poor in high-temperature mechanical property in a high-temperature environment can be effectively solved.

The invention discloses an iron-nickel metal magnetic powder core with high stable magnetic conductivity and low loss and a preparation method of the iron-nickel metal magnetic powder core. The iron-nickel metal magnetic powder core is prepared through the steps of preparing iron-nickel alloy powder through gas atomization, screening the particle size, carrying out insulation coating, carrying out compression molding, carrying out heat treatment and carrying out impregnation and spraying. Wherein in the insulating coating process, a passivation solution is adopted to form an insulating layer on the surface of the iron-nickel alloy powder, and the passivation solution comprises 0.1 wt%-0.3 wt% of phosphoric acid, 0.1 wt%-0.6 wt% of sol and the balance deionized water according to the weight part of the iron-nickel alloy powder; and the pH value of the passivation solution is 4-7. According to the technical scheme, the iron-nickel alloy powder is subjected to insulation coating through cooperation of the phosphoric acid, the sol and the coating agent, the magnetic hysteresis loss is effectively reduced, the magnetic conductivity of the iron-nickel magnetic powder core is improved, the quality factor of the iron-nickel magnetic powder core is remarkably improved to 95 or above, and after the obtained high-magnetic-conductivity low-loss iron-nickel magnetic powder core is subjected to long-term high-temperature aging, the magnetic conductivity change rate does not exceed 2%; and the safety and the performance stability are greatly improved in the application of power electronic devices.

The invention belongs to the technical field of catalytic chemistry, and particularly relates to a method for enhancing photoelectric composite catalytic reaction efficiency through self-adaptive multi-field coupling. Specifically, firstly, a closed columnar reactor composed of an LED array, a reflection / lens system, a copper-nickel alloy cathode, a Ru-doped PbO2 anode, a Ti5O7 / Ti3O4 composite photocatalytic parallel-connection multi-tube plate and the like is built, a distributed silicon photodiode and a quantum dot fluorescent probe sensor are installed, a machine learning algorithm is utilized, and according to the reactant concentration and the by-product generation condition, the quantum dot fluorescent probe sensor and the quantum dot fluorescent probe sensor are analyzed. Light field conditions (wavelength, intensity and distribution) used by photocatalysis, electric field conditions (current, voltage and power line distribution) used by electrocatalysis and flow field conditions (flow velocity, flow rate and distribution) are dynamically adjusted to optimize the chemical reaction rate, and an AI model is combined to predict an optimal multi-field coupling setting scheme, so that the efficiency is improved, the energy consumption is reduced, and the cost is reduced. Meanwhile, the effect of enhancing the catalytic conversion reaction is achieved.

The invention discloses a zirconium-nickel dissimilar metal welding method based on active regulation and control of a temperature field. The zirconium-nickel dissimilar metal welding method comprises the following steps that S1, base metal is cleaned; the butt-joint end faces and the welding surfaces of the zirconium and nickel alloy pipes are polished and cleaned, and clean zirconium and nickel base materials are obtained; s2, a to-be-welded part is assembled; the to-be-welded end face of the clean base metal is assembled in a protective gas cavity of the rotary clamping device; s3, welding is conducted; a laser scanner is adopted for welding at a preset welding position, heat source gradient distribution of base metal at the two ends of a welding seam is controlled by regulating and controlling laser power, welding seam temperature field feedback is established through an infrared temperature sensor, and real-time monitoring and laser power regulating and controlling are conducted; s4, postweld heat treatment; and the laser power is adjusted in real time according to welding seam temperature field feedback so as to adjust and control the welding seam cooling process. According to the method, effective connection of zirconium-nickel indissolvable metal is achieved by controlling the regional welding temperature field, the temperature range for forming brittle compounds is avoided, the uniformity of a molten pool between Zr and Ni materials is ensured, and welding defects such as hot cracks and air holes are reduced.

The invention discloses an ultrasonic impregnation preparation method of a nickel alloy type electrolytic catalyst. The ultrasonic impregnation preparation method comprises the steps of substrate pretreatment, precursor preparation and catalyst film preparation. Through the mode, the ultrasonic impregnation preparation method of the nickel alloy type electrolytic catalyst can replace a Pt-based catalyst which is high in cost, a synergistic effect is generated through interaction of two or more metal elements, the catalytic performance, stability and corrosion resistance of the alloy catalyst under high-concentration alkaline large current are improved, HER reaction is facilitated, and the nickel alloy type electrolytic catalyst can be used for preparing a high-efficiency electrolytic catalyst. And moreover, the dependence on single noble metal is reduced, the production cost of the catalyst can be remarkably reduced, and the resource utilization efficiency, the energy efficiency and the environmental friendliness are improved.

The utility model discloses a heat treatment furnace which comprises a base and a furnace body, the furnace body is fixedly installed at the top of the base, a clamping assembly is fixedly installed at the top of the base and comprises a fixing frame and a threaded rod, the fixing frame is fixedly installed at the top of the base, and the threaded rod is connected to one side of the fixing frame through threads. One end of the threaded rod is connected with a movable frame through a bearing, a sliding rod is fixedly installed on one side of the movable frame, the side wall of the sliding rod is sleeved with a spring, a first clamping plate and a second clamping plate are slidably connected to the side wall of the sliding rod, a stop rod is fixedly installed at the top of the fixed frame, and a round rod is fixedly installed on one side of the movable frame and slidably connected with the fixed frame. According to the heat treatment furnace, through the arranged clamping assembly, iron-nickel alloy can be clamped, meanwhile, the iron-nickel alloy can be conveniently stretched into the furnace body for heat treatment, the iron-nickel alloy can be conveniently taken out after heat treatment, the iron-nickel alloy can be automatically loosened after being taken out, use is more convenient, and the use effect can be improved accordingly.

The present invention belongs to the fields of electrical and electronic engineering and advanced nonferrous metal additive manufacturing. Specifically, it relates to a method for preparing copper alloy-tungsten-copper composite electrical contacts using laser additive manufacturing. The method uses coaxial powder feeding laser cladding to prepare a nickel or nickel alloy coating as an intermediate layer on a copper alloy substrate. This is followed by laser cladding to prepare a tungsten-copper coating. The composite electrical contact consists, in sequence, of a pure copper or copper alloy substrate layer, a pure nickel or nickel alloy coating, and a tungsten-copper coating. The resulting electrical contact has high electrical and thermal conductivity and good resistance to arc erosion. Using laser cladding technology to prepare copper alloy-tungsten-copper electrical contacts can effectively reduce production costs, improve production efficiency, and facilitate subsequent maintenance and repair, making it environmentally friendly.

A high-Ni alloy steel plate excellent in weld hot cracking resistance includes in mass %: C≤0.15%, Si: 0.05-1.0%, Mn: 0.05-2.0%, P≤0.035%, S≤0.0015%, Cr: 16-28%, Ni: 18-65%, Al: 0.01-1.0%, Ti: 0.15-1.5%, B: 0.0002-0.0030%, N≤0.05%, O≤0.003%, Mo: 0.01-10%, Cu: 0.01-4.0%, Co: 0.01-3.0%, V: 0.01-0.5%, Mg≤0.0050%; and a balance consisting of Fe and impurities, in which a grain size number G defined by JIS G0552 is 1.0 or more and a standard deviation of a concentration distribution of solid solute Ti in a thickness direction is 0.045% or less. A manufacturing method of a high-Ni alloy steel plate excellent in weld hot cracking resistance includes conducting a high-temperature long-time heat treatment at a temperature of 1200 degrees C. or more for eight hours or more in a step prior to a final hot rolling.

The present application relates to high-temperature alloy smelting technical field, specifically relates to a kind of high-aluminum titanium cast nickel-based high-temperature alloy purification smelting method.The pure smelting method, step one, low calcium nickel alloy preparation;Step two, pure smelting: batching and furnace charging, melting period, refining period, alloying period, calcium treatment purification period and casting period;Pure smelting process is carried out in vacuum induction melting furnace, 2 / 3 low calcium nickel alloy is directly loaded into magnesium oxide crucible when furnace charging, and the remaining 1 / 3 low calcium nickel alloy is added in calcium treatment purification period.The present application prepares a kind of component accurately controllable "low calcium nickel alloy" as master alloy by pre-preparation, is added in key smelting stage, solves the problem of calcium element direct addition, realizes the deep deoxidation denitrogenation desulfurization of alloy melt, significantly reduces the oxygen, nitrogen, sulfur impurity content in alloy, to improve the purity and comprehensive mechanical properties of alloy.

The invention belongs to the field of electromagnetic shielding material manufacturing, and particularly relates to a foam nickel alloy blackening process for an electromagnetic shielding material. The foam nickel alloy blackening process for the electromagnetic shielding material comprises the following steps: forming an alloy blackening layer by adopting an alloy electrodeposition blackening step; alloy forming the alloy blackening layer comprises Ni and S, and further comprises one or more of Zn, Sn and Mo. Further, the alloy blackening layer is composed of any one of an alloy Ni-Zn-S, an alloy Ni-Sn-S, an alloy Ni-Mo-S, an alloy Ni-Zn-Sn-S, an alloy Ni-Zn-Mo-S, an alloy Ni-Sn-Mo-S, an alloy Ni-Zn-Mo-S, and an alloy Ni-Sn-Mo-S. Further, the process comprises a pretreatment step, a nickel pre-plating step, an alloy electrodeposition blackening step, a post-treatment step and a drying step. The alloy blackening foamed nickel finished product has excellent conductivity, can improve the absorption capacity of electromagnetic waves, further improves the electromagnetic shielding performance, and has high application value in the field of electromagnetic shielding materials.

Disclosed is a copper foil to which a carrier foil is attached, which has favorable peel strength under high-temperature pressing conditions, the copper foil to which the carrier foil is attached comprising: a carrier foil; a release layer on the carrier foil; a heat-resistant layer on the release layer; and an ultra-thin copper foil on the heat-resistant layer, in which a buffer layer of a nickel alloy is interposed between the release layer and the heat-resistant layer.

The invention provides a conductive paste and a preparation method and application thereof, and the conductive paste comprises 84-91 wt% of a conductive phase, 0.8-5.2 wt% of a glass phase, 4-11 wt% of an organic carrier, 0.1-3 wt% of a dispersant, and the balance of a solvent. The conductive phase comprises 5-60 wt% of nickel alloy powder and 40-95 wt% of silver powder, the nickel alloy powder comprises at least one nickel alloy compound, the nickel alloy compound has a general formula of Ni-alpha-beta-gamma, alpha, beta and gamma are three non-nickel elements which are different from one another, and the sum of the alpha, the beta and the gamma is 100%. The elements alpha, beta and gamma are respectively selected from any one of transition metal, rare earth metal, alkaline earth metal and other non-nickel elements, the mass content of the nickel element is 10-99 wt%, and the sum of the mass content of the elements alpha, beta and gamma is 1-90 wt%. Nickel elements and non-nickel elements alpha, beta and gamma in a proper mass ratio are screened to form nickel alloy powder, so that the physical and chemical properties of the nickel alloy powder are improved, the ratio of the nickel alloy powder for replacing silver powder is increased, the electrical properties in the conductive slurry can be guaranteed, and the cost of the slurry is remarkably reduced.

The invention provides a production process of a high-low tooth screw, relates to the technical field of screw production, and solves the problems of poor skid resistance, low fastening efficiency, unbalanced mechanical properties, insufficient corrosion resistance and the like of a traditional screw through innovative design and process optimization. SCM435 alloy steel is selected, spaced anti-skid teeth are pressed within the range of 270 degrees in the circumferential direction of the head of the screw through a four-station cold header, high-low alternating tooth forms are twisted on the rod portion, the gradient hardness of the surface and the core portion is achieved through isothermal quenching, surface treatment is combined with zinc-nickel alloy electroplating and a polytetrafluoroethylene coating, and the corrosion resistance and the assembly smoothness are improved; full-process intelligent detection is realized through machine vision, three-coordinate measurement and torsion test. The local layout of the anti-skid teeth reduces material consumption and improves meshing efficiency, the high-low tooth form reduces assembly torque and stabilizes pre-tightening force, gradient heat treatment enhances fatigue resistance, the composite coating improves corrosion resistance, and intelligent detection guarantees product consistency.