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Microwave preparation method of anti-oxidation coating made of carbon-based material

The invention relates to a microwave preparation method of an anti-oxidation coating made of a carbon-based material, in particular to a substrate material which may be a carbon material, a C/C composite material or a C/SiC composite material. In the invention, slurry prepared by using Si compounds is coated on the carbon-based material, which is subjected to surface treatment, by a brush or immersion, then the carbon-based material is buried in graphite powder in a corundum crucible, the corundum crucible is placed in microwaves to be heated, the pre-heating, heating and temperature preservation are performed by stepwise regulating the power of a microwave oven, and thus, an anti-oxidation single-layer coating is obtained; on this basis, a composite coating of oxides, silicides and the like can be obtained. In the invention, microwaves act directly on the carbon-based material and the carbon-based material, after absorbing the microwaves, generate heat raises the temperature to a required temperature, so that the coating and a substrate are bonded and a protective coating with high protective performance is obtained; and as aluminum powder is added as a SiC sintering aid, the compaction of the SiC is promoted by the silicon aluminum alloy produced by the low-melting-point aluminum and part of molten silicon.
Owner:UNIV OF SCI & TECH BEIJING
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