591 results about "Oxide ceramic" patented technology

The invention discloses reflection-heat insulation dual-functional aluminum oxide ceramic and a preparation method and application thereof.The method comprises the steps that after surface silanization treatment is conducted on nanoscale hollow oxide filler, surface-modified nanoscale hollow oxide filler is prepared; and then adding the surface-modified nanoscale hollow oxide filler into a high-molecular polymer and a mixed polar solvent to obtain the thermal insulation coating. The method comprises the following steps: coating the surface of aluminum oxide ceramic with a heat insulation coating to form a primary coating, and carrying out gradient heating curing to obtain aluminum oxide ceramic with a functionalized heat insulation coating; and coating the surface of the thermal insulation coating functionalized aluminum oxide ceramic with an infrared reflection coating, and carrying out annealing treatment in a nitrogen atmosphere to prepare the reflection-thermal insulation dual-functionalized aluminum oxide ceramic. By constructing a double-layer composite structure, enhancing interface thermal resistance through chemical bonding, directionally distributing the nanofiller and designing a low-radiation layer structure, heat conduction and radiation heat transfer of the aluminum oxide ceramic-based material are synergistically reduced, and the high-temperature heat insulation performance of the aluminum oxide ceramic-based material is improved.

The invention relates to the technical field of brazing processes, in particular to a brazing process for connecting aluminum oxide ceramic and metallic titanium through low-activation brazing filler metal. According to the technical scheme, the method comprises the following steps that a to-be-welded face of the aluminum oxide ceramic is subjected to magnetron sputtering titanium film plating, the sputtering power ranges from 80 W to 150 W, the argon pressure ranges from 0.5 Pa to 1.5 Pa, the film thickness ranges from 0.5 micrometer to 5 micrometers, inert gas annealing treatment is conducted after film plating, the annealing temperature ranges from 400 DEG C to 550 DEG C, and the heat preservation time ranges from 10 min to 30 min; and the surface of the metal titanium substrate is subjected to laser micro-texture treatment, and a periodic groove structure with the depth being 10-50 microns is formed. The problems of poor wettability of the brazing filler metal and the ceramic, low joint strength and joint stress cracks are solved, meanwhile, radioactive substances generated by the brazing filler metal under the irradiation condition can be released within a short time, the equipment maintenance period is greatly shortened, and the equipment service life is prolonged.

The invention discloses an energy-saving environment-friendly spray granulation tower for aluminum oxide ceramic material processing, which comprises a bottom plate, a mixing barrel is fixedly mounted at the upper end of the bottom plate, a heating pipe is spirally wound on the outer side of the mixing barrel, a stirring assembly is arranged in an inner cavity of the mixing barrel, a granulation tower box is arranged at the rear end of the mixing barrel, and the granulation tower box is arranged in the inner cavity of the mixing barrel. And the lower end of the granulation tower box is fixedly connected with a collection hopper. According to the energy-saving and environment-friendly spray granulation tower for aluminum oxide ceramic material processing, by starting a driving motor, the output end of the driving motor drives a first stirring shaft to rotate, the first stirring shaft rotates to drive a main cone pulley to rotate, the main cone pulley rotates to drive a transmission cone pulley to rotate, and then through cooperation of a driven cone pulley, the energy-saving and environment-friendly spray granulation tower is driven to rotate. The second stirring shaft can conveniently rotate reversely, so that the materials in the mixing barrel can be fully stirred by a plurality of groups of stirring rods, and the problem that the quality and the size of formed spherical particles do not reach the standard due to the fact that the materials are not uniformly mixed can be avoided.

The invention relates to the technical field of ceramic substrates, and provides a bending-resistant aluminum oxide multilayer ceramic substrate and a preparation method thereof. The bending-resistant aluminum oxide multilayer ceramic substrate comprises the following raw material components in parts by weight: 95-110 parts of aluminum oxide, 3-8 parts of a plasticizer, 6-12 parts of an auxiliary agent, 4-7 parts of a binder, 3-6 parts of a dispersant and 60-70 parts of a solvent, the preparation method of the additive comprises the following steps: A1, adding calcium oxide into ethanol, adding glucose, stirring until the materials are uniformly mixed, and concentrating to obtain a glucose coated material; a2, carrying out annealing treatment on the glucose coated material to obtain a carbon coated material; and A3, uniformly mixing the carbon-coated material with magnesium oxide and titanium dioxide, and carrying out ball milling to obtain the auxiliary agent. According to the technical scheme, the problem of low mechanical property of the aluminum oxide ceramic substrate in the prior art is solved.

The invention relates to the technical field of non-oxide ceramic-based composite materials, in particular to Fe-N-based high-entropy nitride ceramic as well as a preparation method and application thereof. The method comprises the following steps: by taking iron powder as a sintering aid, mixing (Hf < 0.2 > Zr < 0.2 > Ti < 0.2 > Nb < 0.2 > Ta < 0.2 >) N high-entropy powder with the iron powder, and carrying out ball milling treatment to obtain ball-milled powder; and under the oxygen-free condition, the ball-milled powder is subjected to sintering treatment, transformation from the loose ball-milled powder to compact and uniform solid solution ceramic is achieved in the sintering treatment process, and the Fe-N-based high-entropy nitride ceramic is obtained. According to the method, a nitride thermal reduction method sintering process is adopted, energy is provided for densification of the Fe-N-based high-entropy nitride ceramic by utilizing reaction heat release of the (Hf0. 2Zr0. 2Ti0. 2Nb0. 2Ta0. 2) N high-entropy powder and the iron powder, the sintering temperature is reduced, energy is saved, and the defect that densification needs to be carried out under a high-temperature condition in the prior art is overcome.

The invention belongs to the field of conductive aluminum oxide ceramic preparation, and particularly relates to a treatment method for performing carbon deposition infiltration on the surface of aluminum oxide ceramic to enable the aluminum oxide ceramic to have certain conductivity. According to the invention, wheat starch and corn starch are used as main raw materials and are converted into a volatile carbon source through a high-temperature carbonization process under the protection of inert gas; and placing the carbon source and aluminum oxide ceramic pre-subjected to conductive treatment in a high-temperature furnace protected by inert gas, and performing deposition carburizing treatment on the surface of the aluminum oxide ceramic at 800-900 DEG C to obtain the aluminum oxide conductive ceramic with certain conductivity. The method is low in raw material cost, low in sintering temperature of the related process, low in equipment investment, good in surface carburization uniformity of the aluminum oxide ceramic and stable in property.

The invention discloses a seawater conductivity sensor electrode material based on a copper-nickel-based nanostructure and a preparation method, the electrode material comprises: a substrate, a copper-nickel-based nanostructure layer being formed on the surface of the substrate; the substrate comprises an insulating compound and a coating coated on the surface of the insulating compound, the insulating compound comprises at least one of high-resistance silicon, silicon oxide, aluminum oxide ceramic and plastic, the coating comprises a metal coating and / or a semiconductor coating, and the copper-nickel-based nanostructure layer is in a dendritic crystal or cluster form. The copper-nickel alloy nanostructure is a core material of the electrode, so that the electrode material has high specific surface area and rich active sites, the measurement accuracy and measurement limit of the electrode material can be improved, the service life can be prolonged, the manufacturing cost can be reduced, and the application requirements of the ocean Internet of Things can be met.

The invention provides modified zirconium silicate whisker reinforced aluminum oxide ceramic as well as a preparation method and application thereof, and belongs to the technical field of new materials. The preparation method comprises the following steps: modifying the surface of alumina powder with a silane coupling agent with sulfydryl to generate zirconium silicate in situ, uniformly mixing the zirconium silicate with zirconium silicate whiskers which are treated by hydrogen peroxide and modified by phytic acid and tannic acid and a CeO2-Y2O3-MgO-SiO2 compound, and performing spark plasma sintering to obtain the modified zirconium silicate whisker reinforced alumina ceramic. The modified zirconium silicate whisker reinforced aluminum oxide ceramic prepared by the invention has better interface bonding force, excellent mechanical properties and good wear resistance, realizes ceramic densification, and has wide application prospects.

The invention relates to the technical field of ceramics, in particular to aluminum oxide ceramic slurry as well as a preparation method and application thereof. The aluminum oxide ceramic slurry is prepared from alpha-aluminum oxide coarse powder, alpha-aluminum oxide fine powder, modified aluminum oxide powder, acrylamide, N, N '-methylene bisacrylamide and deionized water, multiple active functional groups are introduced into the surface of the modified aluminum oxide powder, interface bonding of particles with a dispersion medium and a polymer monomer is enhanced, and the surface of the particles is improved. According to the present invention, with the preparation method, the particle agglomeration tendency is reduced, such that the slurry can maintain the low viscosity under the high solid content condition so as to meet the gel injection molding process requirements, and the sintering body obtained through the gel injection molding has characteristics of high bending strength and high hardness, and can be widely used in the fields of electronic devices, mechanical sealing members, biomedical apparatuses and instruments, and the like.

The invention relates to the technical field of nuclear fusion surface plasma W materials, in particular to nano rare earth oxide ceramic-Ti microalloy composite reinforced W powder, a composite material and a preparation method of the nano rare earth oxide ceramic-Ti microalloy composite reinforced W powder. The composite powder is of a nearly spherical core-shell hierarchical structure, and the particle size is 30-50 nm; according to the composite powder, refractory metal W serves as a matrix, nano rare earth oxide ceramic particles are evenly dispersed in matrix W crystal grains, Ti mainly forms an enrichment area on the surface of the matrix or a matrix / rare earth oxide interface in a simple substance or oxide mode, the phase interface structure is effectively improved, W crystal boundary migration and dislocation motion are hindered, W crystal grains are remarkably refined, and the composite powder is prepared. Part and W form semi-coherence, fine grain and interface strengthening and toughening are achieved, and a brand new thought and a technical method are provided for synergistically improving the strength and toughness of the W composite material. The composite powder is subjected to organic reduction synthesis and low-temperature reinforced sintering to prepare the composite material, the tensile strength at the room temperature reaches 500-610 MPa, and the ductility is 5%-8%.

The invention belongs to the technical field of ceramic material preparation, and particularly relates to a high-throughput preparation method and device based on an aluminum oxide ceramic system diffusion couple. An aluminum oxide model green body containing a plurality of blind holes is prepared through the powder extrusion 3D printing technology, a diffusion material is embedded through a rivet type structure, and the layering risk is eliminated in combination with the thermal expansion coefficient gradient design (the inner layer is large, and the outer layer is small); sPS low-temperature rapid sintering is adopted, and multiple binary diffusion couples are prepared at a time. According to the method, the problems that a traditional diffusion couple is not tight in contact, easy to layer and incapable of being produced in batches are solved, the efficiency is improved by 80% or above, diffusion couple samples of different materials can be prepared at the same time, multiple binary diffusion couple systems can be obtained through subsequent sample cutting, and the preparation method is simple, efficient, easy to operate and suitable for aluminum oxide and rare earth oxide systems.

The invention provides a method for metallizing a homogeneous oxide ceramic surface, and belongs to the technical field of ceramic metallization. The metallization method comprises the steps of pretreatment, primary deposition, metallization slurry preparation, coating and sintering. The primary deposition comprises the following steps: putting the pretreated ceramic into modified titanium dioxide sol, drying and calcining to obtain primarily deposited ceramic; a preparation method of the modified titanium dioxide sol comprises the following steps: adding tetrabutyl titanate into absolute ethyl alcohol, and then adding formylated alumina fibers to obtain a reaction solution A; adding deionized water and glacial acetic acid into absolute ethyl alcohol to obtain a reaction solution B; adding the reaction liquid A into the reaction liquid B, heating to 44-48 DEG C, adding 4-vinyl aniline, and carrying out heat preservation and stirring to obtain titanium dioxide sol; by adopting the metallization method disclosed by the invention, the uniformity is good, the binding force between the ceramic and the metal coating is strong, the compression-shear strength is high, and the high and low temperature cycle resistance is excellent.

The invention discloses an aluminum oxide ceramic tube shell production device and a preparation method, and belongs to the technical field of aluminum oxide ceramic tube shell preparation, the technical scheme is that the aluminum oxide ceramic tube shell production device comprises a forming mechanism, a transferring mechanism, a sintering mechanism and a surface treatment mechanism, the transferring mechanism is used for transferring the formed aluminum oxide ceramic tube shell to the sintering mechanism, the sintering mechanism is used for sintering the formed aluminum oxide ceramic tube shell, and the surface treatment is used for carrying out surface treatment on the sintered aluminum oxide ceramic tube shell. According to the scheme, the adjacent aluminum oxide ceramic tube shells can be uniformly heated, the product quality is ensured, the uniform heating time of the single aluminum oxide ceramic tube shell can be prolonged, repeated sintering is not needed, and the preparation efficiency is improved.

The invention relates to the technical field of materials, in particular to light-cured aluminum oxide ceramic slurry and a preparation method thereof. The preparation method of the light-cured aluminum oxide ceramic slurry comprises the following preparation steps: preparation of alkenyl chitosan nanofibers, preparation of modified monomers, preparation of clathrate powder, preparation of a photosensitive resin premixed solution, preparation of clathrate powder and preparation of the light-cured aluminum oxide ceramic slurry. According to the preparation method, by introducing the alkenyl chitosan nanofiber and the inclusion compound powder, the rheological property, the sintering compactness and the mechanical property of the light-cured aluminum oxide ceramic slurry are remarkably improved, meanwhile, the apparent porosity and the shrinkage rate are reduced, and the preparation method is suitable for preparing the high-performance ceramic core.

The present invention discloses a triaxially spun superelastic and high-temperature resistant composite carbon nanofiber aerogel and a preparation method thereof. The aerogel is formed by interweaving curly fibers with a core layer of carbon and a shell layer of oxide ceramic. The present invention utilizes electrostatic spinning technology to prepare composite carbon nanofiber aerogels. First, an inner layer polyacrylonitrile solution is prepared, and the water / alcohol ratio is adjusted to prepare a middle layer ceramic sol with controllable water content, thereby obtaining a spinning solution with compatibility in the initial spinning stage. The temperature and humidity of the airflow of the outer nozzle are then regulated, and the water content of the ceramic sol is further adjusted during the spinning process, so that the spinning solution becomes incompatible. The spinning solution jet is fast and solidified in advance, thereby obtaining a curly interwoven structure nanofiber aerogel precursor. Finally, the final product is obtained by changing the atmosphere and performing rapid and continuous heat treatment. The present invention solves the problems of insufficient mechanical properties and easy oxidation of carbon nanofiber aerogels. The preparation method is simple and easy to implement, and the process is continuous, and can be carried out on existing electrostatic spinning production equipment.

The invention relates to the technical field of ceramic manufacturing processes, and particularly discloses a preparation method of a 96 aluminum oxide ceramic substrate, which comprises the following steps: slurry preparation: carrying out ball milling treatment on high-purity aluminum oxide powder, a sintering aid, a binder, a plasticizer, an organic solvent and a dispersing agent, and fully mixing to obtain tape casting slurry; forming a green body, coating a carrier film with the tape casting slurry through a tape casting machine with a wet film which is uniform in thickness and flat in surface, and drying the carrier film through a drying box in a partitioned manner to obtain a cured green body; and sintering densification treatment: carrying out glue removal treatment on the green body, and carrying out stepped heating sintering to obtain the 96 aluminum oxide ceramic substrate. According to the 96 aluminum oxide ceramic substrate prepared by the scheme, a large number of uniform crystal cores can be formed, small crystal grains can be dissolved, large crystal grains grow at a constant speed, and the uniformity of the crystal grain size is ensured, so that scattering of phonons on a crystal boundary can be reduced, and a structural foundation is laid for improvement of heat conductivity.

The invention discloses a manufacturing method of a small-spacing lamp panel. The manufacturing method comprises the following steps: pressing; drilling is conducted, specifically, through holes are mechanically drilled, and the hole diameter is 0.2-0.3 mm; copper deposition: the thickness of a hole wall copper plating layer is 0.3-0.5 [mu] m; electroplating through holes, wherein the copper thickness in the holes is greater than or equal to 18 microns; the through holes are filled with epoxy resin with the shrinkage rate smaller than 0.5%, and curing is conducted; ceramic board grinding is conducted, an aluminum oxide ceramic grinding wheel is adopted for board grinding, the resin surface in the hole is flush with the surface of the outer layer copper foil of the multi-layer circuit board, the surface roughness Ra is smaller than 0.1 micrometer, and board grinding technological parameters are as follows: the pressure is 5-8 N / cm < 2 >, the rotating speed is 200-300 rpm, and the linear speed is 1-2 m / min; secondary copper deposition: copper deposition is carried out on the surface of the hole plugging resin to form a copper plating layer, and the thickness of the copper plating layer is 0.3-0.5 [mu] m; the whole board is electroplated, and the copper thickness on the resin is larger than or equal to 12 micrometers; and manufacturing an outer-layer circuit. The manufacturing method of the small-spacing lamp panel has the advantages of being low in cost, high in yield, simple in process and the like.

The invention discloses a preparation method of high-density aluminum oxide ceramic and the high-density aluminum oxide ceramic, and the preparation method comprises the following steps: adding a silane coupling agent ethanol solution into alpha-Al2O3 powder for modification treatment to obtain modified powder; the modified powder is subjected to doping treatment, doped powder is obtained, and the mass percent of the modified powder in the doped powder is larger than 97.5%; the method comprises the following steps: filling doped powder in a preset range of a key area of a graphite mold, filling pure modified powder on the outer layer of the doped powder, and wrapping carbon felt after pre-pressing and compacting to obtain a pre-pressed sample; the pre-pressed sample is put into a rapid hot-pressing sintering furnace, O2 / Ar mixed atmosphere is introduced, the temperature is gradually increased to a first sintering temperature, and meanwhile, the pressure applied to the mold is gradually increased to the sintering pressure according to the temperature increasing progress; keeping the temperature for a period of time at the first sintering temperature and the sintering pressure; after heat preservation is finished, the sintering pressure is kept, the temperature is reduced to a second sintering temperature, natural cooling is conducted to the room temperature, and the target high-density aluminum oxide ceramic is obtained.

The invention discloses a preparation method of a high-strength aluminum oxide ceramic substrate, which comprises the following steps: firstly, modifying aluminum oxide powder by a liquid phase method, and coating a layer of nano magnesium oxide on the surface of the aluminum oxide powder; then carrying out ball milling treatment on the modified powder, rare earth metal oxide, metal oxide, an organic solvent, a binder, a plasticizer and a dispersing agent together, then carrying out defoaming, tape casting, drying and laminated hot pressing to obtain a ceramic green body, and finally carrying out sintering molding in an air atmosphere to obtain the ceramic. The nano magnesium oxide active coating layer constructed in situ and the added exogenous sintering aid act together, so that uniform growth of isometric crystals is promoted, development of a small amount of dominant oriented grains is directionally induced, a composite enhanced microstructure is formed, atomic scale super-uniform distribution and optimal interface combination of the nano magnesium oxide and the exogenous sintering aid are realized, and the nano magnesium oxide / exogenous sintering aid composite material is prepared. The bending strength of the obtained alumina ceramic can reach up to 881 MPa.

The invention relates to the field of metal materials, in particular to a preparation method of an ultra-high-speed laser cladding Al2O3 metal ceramic coating. The method comprises the following steps that iron-based metal powder, aluminum oxide ceramic powder and silicon powder are prepared according to the design proportion, the iron-based metal powder, the aluminum oxide ceramic powder and the silicon powder are evenly mixed and then subjected to ultra-high-speed laser cladding, the mass percent of aluminum oxide in the obtained composite powder is 6-10%, the mass percent of silicon powder in the obtained composite powder is 0.5-5%, and when ultra-high-speed laser cladding is carried out, the thickness of the composite powder ranges from 0.5 mm to 5 mm; the laser power ranges from 1500 W to 2400 W, the scanning speed ranges from 12 m / min to 20 m / min, the defocusing amount is + 1 mm, the powder feeding amount ranges from 22 g / min to 30 g / min, the lap joint rate ranges from 60% to 65%, and powder feeding and protective gas is argon. The component design is reasonable, the cost is low, and the obtained product is high in hardness, resistant to corrosion and convenient for industrial application.

The invention discloses a method for preparing an aluminum oxide coating on the surface of neodymium iron boron for a new energy automobile motor, which comprises the following steps: (1) pretreating the surface of a base material: firstly, carrying out corner passivation, degreasing, sand blasting and other pretreatments on a neodymium iron boron magnet, cleaning the surface of the neodymium iron boron magnet by using compressed air after the sand blasting pretreatment is completed, and drying the surface of the neodymium iron boron magnet; removing loose neodymium-iron-boron particles or sand grains on the surface of the neodymium-iron-boron magnet; (2) preheating treatment: respectively preheating the neodymium iron boron magnet and the powder; (3) plasma spraying: coating the surface of the neodymium-iron-boron magnet with the powder by adopting a plasma spraying technology; and (4) hole sealing is conducted, specifically, the sprayed neodymium-iron-boron magnet is soaked with hole sealing agent epoxy resin, redundant glue is wiped away with propyl alcohol, and the neodymium-iron-boron magnet is placed in a vacuum drying box to be dried. The aluminum oxide ceramic coating and the yttrium oxide ceramic coating prepared by the method have good coating uniformity, corrosion resistance, adhesive force and lower porosity.

The invention discloses a high-corrosion-resistance yttrium oxide coating for semiconductor equipment and a preparation method of the high-corrosion-resistance yttrium oxide coating, and belongs to the technical field of coatings. According to the high-corrosion-resistance yttrium oxide coating for the semiconductor equipment and the preparation method of the high-corrosion-resistance yttrium oxide coating, a SiC transition layer is formed on the surface of a carbon-containing matrix; and an yttrium oxide ceramic coating is deposited on the SiC transition layer in an SPPS plasma spraying mode. The SiC transition layer is firstly formed on the carbon-containing substrate, then the Y2O3 coating is deposited through solution precursor plasma spraying, and a structure with both interface stability and surface protection is formed. SiC is thermally compatible with a substrate, so that undercut, warping and stripping can be inhibited; the dense Y2O3 layer can form a non-volatile protective phase in fluorine-containing / chlorine-containing plasma, thereby reducing the material removal rate and reducing particle release.

The invention discloses a preparation method and application of ultrahigh-temperature-resistant tantalum carbide ceramic aerogel, and belongs to the field of ultrahigh-temperature ceramic aerogel preparation. The preparation method of the ultrahigh-temperature-resistant tantalum carbide ceramic aerogel comprises the following steps: mixing a complexing agent and tantalum alkoxide in a polyol solvent for reaction, then adding organic acid for catalytic polymerization, then adding phenolic resin and a gel catalyst to obtain a tantalum carbide precursor solution, and carrying out sol-gel reaction to obtain tantalum carbide precursor wet gel; performing drying treatment on the tantalum carbide precursor wet gel to obtain tantalum carbide precursor aerogel, and performing pyrolysis to obtain the tantalum carbide ceramic aerogel. The tantalum alkoxide is modified by using the complexing agent, the polyhydric alcohol and the organic acid, the precursor solution in which the raw materials can stably coexist at room temperature is obtained, an oxide ceramic gel network does not need to be synthesized in the preparation process, normal-pressure drying can be performed, and the obtained tantalum carbide ceramic aerogel has the characteristics of high purity and low residual carbon content.

The invention relates to the technical field of surface strengthening treatment and coating preparation, in particular to a micro-arc oxidation electrolyte, a preparation method of the micro-arc oxidation electrolyte and a preparation method of an oxide ceramic coating on the surface of a magnesium-copper dissimilar metal material component. The invention provides a micro-arc oxidation electrolyte. The micro-arc oxidation electrolyte comprises a main film-forming agent, an arcing aid, a pH regulator, a corrosion inhibitor and water, the main film-forming agent comprises ammonium fluozirconate and / or potassium fluozirconate; the arcing aid comprises one or more of disodium hydrogen phosphate, sodium dihydrogen phosphate, ammonium dihydrogen phosphate and diammonium hydrogen phosphate; the corrosion inhibitor comprises one or more of hexamethylenetetramine, ammonium bifluoride and triethanolamine. The micro-arc oxidation electrolyte breaks through the problem that valve metal and non-valve metal cannot be subjected to arc discharge at the same time for micro-arc oxidation treatment in the micro-arc oxidation process.

The invention provides porous alumina ceramic and a preparation method thereof, and relates to the technical field of ceramic materials. The invention relates to a preparation method of porous alumina ceramic. The preparation method comprises the following steps: dispersing alpha-cellulose powder in deionized water to form a cellulose suspension; stirring to fully swell the cellulose and form uniform gel, and freeze-drying to obtain a template; dissolving aluminum nitrate hexahydrate, magnesium nitrate hexahydrate and yttrium nitrate hexahydrate in absolute ethyl alcohol to obtain a precursor solution; putting gamma-Al2O3 micro powder and ammonium fluoride into a ball milling tank, adding the precursor solution and a dispersing agent, adding zirconium oxide balls and absolute ethyl alcohol into the ball milling tank, and performing ball milling to obtain ceramic slurry; dipping a template into the ceramic slurry, and performing dipping treatment under a vacuum condition to form a composite green body; and sintering to obtain the porous alumina ceramic. According to the porous aluminum oxide ceramic, the process stability is improved, and the problem that the strength is sharply reduced when the porosity is too high is solved.

The invention discloses a method for preparing oxide eutectic ceramics in an ultrafast high-temperature furnace. Proportioning the raw material powder according to the eutectic components, and sequentially carrying out ball milling, drying, sieving and compression molding; putting the green body into a thin-wall graphite crucible, and putting the thin-wall graphite crucible into an interlayer hole of a heating carbon felt element; and heating to a set temperature in an ultrafast manner, keeping the temperature for an extremely short time, and cooling to obtain the oxide eutectic ceramic. According to the method, the eutectic structure of the oxide ceramic is rapidly formed by adopting ultrafast heating and Joule heat radiation heating at the furnace temperature far lower than the eutectic temperature, and the structure morphology of the eutectic ceramic can be regulated and controlled by adjusting temperature parameters. The obtained eutectic structure is fine in size and excellent in mechanical property; the problems that an existing oxide eutectic ceramic preparation method is long in consumed time, high in cost, complex in bulk material preparation process and the like are solved.

The invention belongs to the technical field of medium-entropy ceramic materials, and relates to a preparation method of a yttrium-zirconium-cerium ternary medium-entropy oxide ceramic material, which comprises the following steps: weighing Y2O3 powder, ZrO2 powder and Ce02 powder according to a molar ratio of 1: 2: 2, carrying out ball-milling mixing to obtain mixed powder, drying the mixed powder, prepressing into a blank, carrying out microwave sintering, and carrying out sintering to obtain the yttrium-zirconium-cerium ternary medium-entropy oxide ceramic material. Synthesizing a yttrium-zirconium-cerium ternary medium-entropy oxide (Y1 / 3Zr1 / 3Ce1 / 3) O2 ceramic material with an equal molar ratio; according to the invention, the raw materials are simple, the preparation steps are simple, the production efficiency is high, the microwave sintering technology is low in sintering temperature and short in sintering time, microwave is utilized to reduce activation energy of substances to accelerate sintering and generate uniform fine grains, and internal pores of the fine grains are small and round, so that the sintered material has good stability and reprocessability; according to the process, green and continuous production is easy to realize, the production scale and efficiency are further improved, and a new way and thought are provided for industrial microwave sintering preparation of the medium-entropy oxide ceramic material.

The invention belongs to the technical field of aluminum electrolysis, and relates to preparation and application of a metal ceramic inert anode material for aluminum electrolysis. The material for the metal ceramic inert anode is formed by compounding a high-entropy alloy phase and a ceramic phase; according to the preparation method disclosed by the invention, the AlCrFeNiV high-entropy alloy and the NiFe2O4 spinel ceramic are compounded to prepare the metal oxide ceramic. The manufacturing method of the metal ceramic inert anode is easy to operate, efficient and beneficial to application and popularization. And in an electrolytic test with the electrolyte being a cryolite-aluminum oxide system at 960 DEG C, good high-temperature conductivity, electrochemical stability, corrosion resistance and thermal shock resistance are achieved.

The invention discloses a one-dimensional heat flux density measuring device based on the Fourier law, and relates to the technical field of object heat flux density measurement. Comprising a heating unit, a sealing heat insulation unit, a cooling unit, a temperature acquisition unit and a data processing unit. The sealing heat insulation unit comprises a heat insulation material, an aluminum oxide ceramic tube, a sealing air layer, an outer layer supporting plate and a rubber or silica gel sealing ring. The heating unit comprises a high-temperature copper plate heating platform; the cooling unit comprises a water cooling head, a cooling water jacket and a cooling water tank, and is nested at the top of the sealed heat insulation unit; according to the temperature acquisition unit, a thermocouple is attached to the surface of a measured object and is connected with an external thermodetector; the data processing unit comprises an acquisition terminal and a computer, the acquisition terminal is connected with a USB interface of the computer and a USB interface of the thermodetector, and data acquired by the thermodetector is transmitted to the computer. The invention provides the heat flux density measuring device which is simple and convenient to assemble, low in construction cost and simple and convenient to calculate, and the measuring efficiency is improved.

The invention discloses a method for preparing silicon dioxide doped yttrium oxide ceramic by adopting green gel casting, which comprises the following steps: firstly modifying yttrium oxide powder, then doping silicon dioxide in the yttrium oxide powder, finally carrying out green gel casting by adopting an Isobam gelling agent, and sintering to obtain the yttrium oxide doped silicon dioxide ceramic. According to the preparation method, the modified yttrium oxide powder is prepared by adopting the surfactant, hydrolysis of the yttrium oxide powder is effectively prevented through modification, silicon dioxide is doped in the yttrium oxide powder, the sintering activity of yttrium oxide is improved, and an adopted Isobam gel system is environmentally friendly, high in production efficiency, good in blank quality and lower in cost; the prepared yttrium oxide doped silicon dioxide ceramic is good in wear resistance, high in density and high in strength.