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815 results about "Magnesium fluoride" patented technology

Magnesium fluoride is an inorganic compound with the formula MgF₂. The compound is a white crystalline salt and is transparent over a wide range of wavelengths, with commercial uses in optics that are also used in space telescopes. It occurs naturally as the rare mineral sellaite.

Method for recovering polysilicon ingots, carborundum powder and polyethylene glycol from cutting waste mortar

The invention discloses a method for recovering polysilicon ingots, carborundum powder and polyethylene glycol from cutting waste mortar. The recovering method comprises the following steps shown as an attached diagram, wherein the high temperature purification comprises the following steps of: mixing the prepared silicon micro powder with a fluxing agent according to the weight ratio of 1: 0.5-5 into lumps, carrying out high temperature treatment in a high temperature vacuum furnace with the treatment temperature range of 1450-1800 DEG C and the treatment time range of 1-10h; and then carrying out directional solidification on melting-state high purity silicon subjected to the high temperature treatment to obtain the polysilicon ingots; wherein the fluxing agent is selected from one or any mixture of silica, alumina, calcium oxide, magnesium oxide, potassium oxide, sodium oxide, calcium fluoride, magnesium fluoride, sodium fluoride, sodium chloride, potassium chloride and calcium chloride. The invention has the advantages that: the yields of carborundum and polyethylene glycol are high and can reach more than 70-80 percent; and the recovered polysilicon ingots reach the purity of 6-7N and completely satisfy of the requirement for preparing silicon slices of silicon solar cell.
Owner:唐康宁

Liquid alkali-free chloride-free accelerating agent as well as methods for preparing and using same

The invention discloses a liquid alkali-free chloride-free accelerating agent and methods for preparing and using the same. Raw materials for preparing the accelerating agent include one or a plurality of the following components of aluminum sulfate, magnesium sulfate, hydramine, an early strength agent, a synergist and water. The aluminum sulfate is the purchasable industrial-grade aluminum sulfate hydrate Al2(SO4)3.18H2O and has the solid content of 51%-52%. The magnesium sulfate is MgSO4.7H2O with the solid content of 48%-49%. The hydramine is one or a plurality of mono ethanol amine, diethanolamine, triethanolamine or isopropoxide. The early strength agent is one or a plurality of calcium sulfate, calcium formate or calcium nitrite. The synergist is magnesium fluosilicate and / or magnesium fluoride. The liquid alkali-free chloride-free accelerating agent provided by the invention has the characteristics of good adaptability, low price, low mixing amount, good performance, good stability and the like; and moreover, the liquid alkali-free chloride-free accelerating agent is added into the concrete to be used as sprayed concrete, has the characteristics of low resilience, small dust pollution and the like and can satisfy the requirements of the 'JC477-2005 sprayed concrete accelerating agent' standard.
Owner:北京冶建特种材料有限公司 +1

Environment-friendly separation and recovery method of fluorine in fluorine-containing waste liquid

The invention discloses an environment-friendly separation and recovery method of fluorine in a fluorine-containing waste liquid. According to the invention, a magnesium-containing compound is added into the fluorine-containing waste liquid as a precipitation agent, such that fluorine in the waste liquid is selectively precipitated; filtering is carried out, and fluorine-removed liquid and magnesium fluoride precipitate are obtained; the fluorine-removed liquid is used in waste water recycling; the magnesium fluoride precipitate is decomposed with sulfuric acid, such that a series of compounds of fluorine are obtained; decomposition residue is subjected to a dissolution-crystallization treatment, such that magnesium sulfate crystals are obtained; the obtained magnesium sulfate crystals are returned and recycled in the fluorine selective precipitation process; the crystallization mother liquor of magnesium sulfate is returned to the dissolution-crystallization process or the magnesium fluoride precipitation decomposition process. The method has the advantages of simple process, simple operation, low production cost, and good fluorine-removing effect. With the method, fluorine resource utilization is realized. The method also has the advantages of no fluorine-containing waste production and no three-waste emission.
Owner:CENT SOUTH UNIV

Silicon solar cell front face electrode silver paste and preparing method thereof

The invention discloses silicon solar cell front face electrode silver paste. The silicon solar cell front face electrode silver paste comprises, by mass, 75-80 percent of silver powder, 3-10 percent of lead-free glass powder, 10-15 percent of organic vehicle and 0.5-3 percent of additive. The silver powder is the spherical micro silver powder with nano bismuth serving as the core, the silver content is 99.1-99.7 percent, the bismuth content is 0.3-0.9 percent, the particle size is 1-2 microns, the tap density is 4.5-5.0 g/ml, the specific surface area is 0.4-1.0 m<2>/g, and the silver powder is prepared by conducting liquid-phase chemical reduction on bismuth nitrate and silver nitrate through glyoxal or acetaldehyde. Bismuth-silicon-antimony-molybdenum lead-free glass powder serves as an adhesive, and potassium fluotitanate, potassium fluoroaluminate, magnesium fluoride and the like are added to serve as the silicon nitride antireflective film eroding additive. According to the silicon solar cell front face electrode silver paste, the contact resistance between a silver electrode and a silicon wafer can be reduced, the stripping strength of the electrode is improved, the electrical property of a solar cell is improved, the production cost of the conductive silver paste is reduced, and the requirement for nonexistence of lead and environmental friendliness are met.
Owner:天津顺御科技有限公司

Preparation method of magnesium oxide foam ceramic filter for filtering magnesium and magnesium alloy melt

The invention provides a magnesium oxide ceramic foam filter for filtering a magnesium and magnesium alloy melt and a preparation method thereof, relating to the field of metallurgy. The process is as follows: a polyurethane foam template is soaked in sodium hydroxide solution (10%) for 30 minutes under the temperature of 50 DEG C and is then washed by water and dried; electric-melting magnesium oxide, magnesium fluoride and water are mixed in a ball-milling manner according to the mass ratio so as to obtain water-based dispersion slurry; the polyurethane foam template is soaked in the slurry, and bisque is obtained through repeated slurry dipping and centrifugal slurry throwing; the bisque is put into an oven; finally, the dried bisque is put into a high-temperature furnace, is heated to 1,200 to 1,300 DEG C at the speed of 1 to 3 DEG C / min, is heat-preserved for 2 hours, and is then naturally cooled in a furnace body. An obtained product of the invention has good chemical stability in the magnesium and the magnesium alloy melt, does not pollute the magnesium and the magnesium alloy melt, has good functions of absorbing and filtering nonmetallic inclusions in the magnesium and the magnesium alloy melt, and is suitable for filtering as well as purifying the magnesium and the magnesium alloy melt.
Owner:SHENYANG INSTITUTE OF CHEMICAL TECHNOLOGY

Broadband reflecting mirror

Provided is a broadband reflecting mirror that has a high reflectance in the band with wavelengths ranging from 400nm to 2,500nm, heat resistance, and flaw resistance. A broadband reflecting mirror (1) for reflecting light in a band with wavelengths ranging from 400nm to 2,500nm, is provided with a first reflecting stacked film (3) in which a first high refractive index material layer and a firstlow refractive index material layer are stacked alternately to reflect light with a band on a short wavelength side in the band with wavelengths ranging from 400nm to 2,500nm, a second reflecting stacked film (4) in which a second high refractive index material layer and a second low refractive index material layer are stacked alternately to reflect light with a band on a long wavelength side in the band with wavelengths ranging from 400nm to 2,500nm, wherein the broadband reflecting mirror is characterized in that the first reflecting stacked film (3) is arranged on the incident side of the light, while the second reflecting stacked film (4) is arranged at a position from which the light penetrating the first stacked film (3) can be reflected, and wherein the first high refractive index material layer is formed of at least one material selected from the group consisting of niobium oxide, titanium oxide, zirconium oxide, tantalum oxide, hafnium oxide, silicon nitride, yttrium oxide and indium tin oxide, the first low refractive index material layer is formed of at least one material selected from the group consisting of silicon oxide and magnesium fluoride, the second high refractive index material layer is formed of at least one material selected from the group consisting of silicon and germanium, and the second low refractive index material layer is formed of at least one material selected from the group consisting of silicon oxide and magnesium fluoride.
Owner:NIPPON ELECTRIC GLASS CO LTD

Preparation method of semiconductor nano-wire-based organic/inorganic composite solar cell

The invention discloses a preparation method of a semiconductor nano-wire-based organic/inorganic composite solar cell, belonging to the technical field of new energy resources. The method is characterized by comprising the following steps: preparing nano silicon with good light absorption performance in a visible light area by an electrochemical corrosion or hydrothermal corrosion technology; growing a zinc oxide or titanium dioxide or cadmium selenide nano-wire array on the nano silicon substrate by a high-temperature chemical vapor deposition method or low-temperature liquid phase chemical method; spinning poly-3-hexylthiophene (P3HT) or poly[2-methoxy-5-(2-ethyhexyloxy)-1,4-p-phenylene vinylene] (MEH-PPV) or poly(3-octylthiophene) (P3OT) on the nano-wire array to form a three-layer composite structure system; and finally preparing a magnesium fluoride or calcium fluoride surface anti-reflection film and metal film electrode to form a solar cell device. The process disclosed by the invention is simple, the operation is simply and easily implemented, the preparation conditions are mild, the repetition rate reaches 100%, and the prepared organic/inorganic composite material system is an important material for manufacturing a full-silicon-based solar cell device in the future.
Owner:BEIJING UNIV OF CHEM TECH

Reflective aluminum nanorod array and method for realizing color hologram by using same

ActiveCN105068396ASimple processGood processing error toleranceNanoopticsInstrumentsDielectric substrateMagnesium fluoride
Provided is a reflective aluminum nanorod array. Each nanorod and a magnesium fluoride layer, an aluminum reflective layer and a dielectric substrate layer corresponding to the nanorod constitute a unit structure. The unit structures have narrow band response to red, green and blue light respectively, and the unit structures are recorded as a unit structure R, a unit structure G and a unit structure B respectively. The three unit structures are alternately arranged in sequence in the length direction of the unit structures. A method for realizing color hologram by using the reflective aluminum nanorod array comprises the steps of determining the main wavelength of response, finding out the side length of the unit structures, the thickness of the magnesium fluoride layers and the width, height and length of the nanorods, calculating the arrangement period size, the number of units and the orientation angle, and arranging the three unit structures alternately for color hologram. The advantages are as follows: the process is simple and has high stability and reliability; the aluminum nanorod corresponding to each structure parameter modulates the phase of light of only one color, and there is no crosstalk between light of different colors; and the reflective aluminum nanorod array and the method can be widely used in true color 3D display, information storage and other fields.
Owner:CHINA INFORMATION COMM TECH GRP CORP

9Ni steel sintered flux and preparation method thereof

The invention belongs to the field of welding material production, and discloses a 9Ni steel sintered flux and a preparation method thereof. The sintered flux comprises the following components in percentage by weight: 20 to 30 percent of dead-burned magnesite clinker, 8 to 18 percent of fluorite, 20 to 30 percent of corundum, 1 to 3 percent of elpasolite, 10 to 20 percent of grammite, 2 to 8 percent of strontium carbonate, 1 to 5 percent of rutile, 1 to 3 percent of silicon iron, 1 to 3 percent of ferrotitanium, 1 to 5 percent of manganese metal, 1 to 5 percent of magnesium fluoride and 1 to 3 percent of chromium oxide green. The preparation method comprises the following steps of: performing dry-mixing on mineral materials and iron alloy in a formula for 5 minutes; adding water glass to perform wet-mixing; then pelleting the mixture; drying pellets for 3 hours under the atmospheric environment; baking the pellets in a baking oven at a low temperature of 150 DEG C for 2 hours; then baking the pellets at a high temperature of 800 DEG C for 1 hour; performing furnace cooking, and crushing and screening the pellets to obtain a 12-60-mesh finished product of the flux. When the flux disclosed by the invention is matched with an ERNiMo-8 welding wire to perform welding, the flux has the following characteristics that: 1) a welding seam process has high performance, electric arcs during welding are stable, the surface of a welding seam is white and bright without an oxide color, molten slag is turned up automatically and can be taken off with a slight contact, the welded seam is formed to have a beautiful appearance, the welding bead height is moderate, and the welded same infiltration angle is moderate; 2) the flux can be matched with the ERNiMo-8 welding wire in use, and the comprehensive mechanical property is high; and 3) the flux can be matched with the ERNiMo-8 in use, and the chemical components of a deposited metal are easy to control.
Owner:LUOYANG SHUANGRUI SPECIAL ALLOY MATERIALS

Long-range surface plasma resonance sensor and preparation method thereof

The invention discloses a long-range surface plasma resonance sensor and a preparation method thereof. The sensor is formed by bonding a BK7 prism and a glass slide through cedar oil, wherein the outer surface of the glass slide is plated with a magnesium fluoride thin film, a silver film and a gold film in turn; the gold film is directly contacted with biological solution to be detected and is used for detecting the biological solution in a mode of angle modulation; magnesium fluoride with the refractive index of about 1.38, which is close to that of the biological solution, can form approximatively symmetric structures on two sides of a metal conductive layer so as to ensure that surface plasmas on the two sides of the metal conductive layer are coupled to form the long-range surface plasma; compared with other metals, the metal silver used as the conductive layer has a narrower half band width of a resonance absorption peak, but has unsteady chemical properties; a conductive layer gold film can make a resonance angle generate a greater transition along with the change of the refractive index of the biological solution to be detected; simultaneously, the conductive layer gold film has stable chemical properties and high biological affinity. The specific multilayer film structure can integrate the advantages of each film and effectively improve the sensitivity of biological sensors.
Owner:EAST CHINA NORMAL UNIV

Method for extracting valuable metal from cobalt metallurgical waste

The invention provides a method for extracting valuable metal from cobalt metallurgical waste. The method comprises the following steps of S1, calcium removal, S2, copper separation, S3, calcium and magnesium removal, and S4 zinc separation. The method has the beneficial effects that 1, impurity removal liquid generated by the impurity removal procedure of cobalt wet metallurgy P204 or the valuable metal in manganese-rich slag after the impurity removal liquid is precipitated can be sufficiently utilized; 2, the metal recovery rate of the method is high, the recovery rate of calcium can reach 85% or over, and the recovery rates of copper, cobalt, manganese and zinc can reach 90% or over; 3, the technological process of the method is short and only has four steps, and applied raw and auxiliary materials are easy to obtain and low in cost; and 4, the technological process does not involve high temperature or high pressure, reaction conditions are mild, and the number of potential safety hazards is small. Calcium sulfate generated through the method can serve as a raw material for production of cement, a small amount of generated calcium fluoride slag and a small amount of generated magnesium fluoride slag can be sent to a fluorination plant to serve as raw materials, and environmental friendliness is achieved.
Owner:青海快驴高新技术有限公司
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