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154 results about "Non oxide ceramics" patented technology

Method for preparing ultra-fine diamond grinding wheel of vitrified bond

The invention discloses a method for preparing an ultra-fine diamond grinding wheel of a vitrified bond, belongs to the technical field of ultra-precision machining of hard brittle and soft brittle photoelectric crystals, and in particular relates to the method for preparing an ultra-fine diamond grinding wheel of photoelectric semiconductor hard brittle and soft brittle photoelectric crystals. The method is characterized by comprising the following steps of: taking ultra-fine diamond powder which has a particle size of a fixed valve from #10,000 to #300,000 as an ultra-fine diamond grinding material; taking three or four ultra-fine non-oxide ceramics as bonding agents, taking one or two of chlorides or nitrates of potassium, calcium, sodium and magnesium as a dispersant and a refiner; taking one or two of dextrine, carbonates and hydrocarbonates as a foaming agent; pressing and molding by a cold-press molding method; uniformly heating to the temperature of between 480 and 530 DEG C from a room temperature; keeping the temperature for 30 to 60 minutes; uniformly heating to the temperature of between 580 and 610 DEG C; keeping the temperature for 40 to 60 minutes; uniformly heating to the temperature of between 640 and 680 DEG C; keeping the temperature for 100 to 150 minutes; and naturally cooling to the room temperature so as to sinter and mold the ultra-fine diamond grinding wheel. The method has the effects and the advantages of high-efficiency ultra-smooth low-damage grinding and high-efficiency ultra-precision grinding machining effect.
Owner:DALIAN UNIV OF TECH

Carbon-based polymer composite material capable of being ceramized and preparation method thereof

The invention relates to a carbon-based polymer composite material capable of being ceramized and a preparation method thereof. The carbon-based polymer composite material is formed by mixing and pressing carbon-based resin, a fiber-reinforced material, a high temperature-resistant coupling agent, aluminium silicate mineral powder and non-oxide ceramic powder, and the carbon-based polymer composite material specifically comprises the following components in parts by weight: 20-50 parts of the carbon-based resin, 10-40 parts of the fiber-reinforced material, 0.5-2 parts of the high temperature-resistant coupling agent, 10-50 parts of the aluminium silicate mineral powder and 1-10 parts of the non-oxide ceramic powder. Compared with the prior art, the composite material disclosed by the invention has the advantages of good thermal protection performance and anti-scour performance; a forming process of the composite material is simple, and aerobic thermal protection and ceramic formationare integrated; the ceramization temperature is lower and the ceramic conversion rate is higher; and the polymer composite material further has the advantages of capability of being formed by the polymer composite material process, strong designability, good mechanical properties at medium and low temperature, high ceramic conversion rate, low thermal weight loss rate, high retention rate of high-temperature strength and the like.
Owner:WUHAN UNIV OF TECH

High-entropy brazing filler metal for brazing non-oxide ceramics and non-oxide ceramic composite material and preparation method of brazing filler metal

The invention relates to a high-entropy brazing filler metal and a preparation method thereof, and particularly relates to a high-entropy brazing filler metal for brazing non-oxide ceramics and the composite material of the non-oxide ceramics and the preparation method of the brazing filler metal, aiming to solve the problem that the brazing filler metal at the joint of the non-oxide ceramics and the ceramic composite material which are soldered together is unreliable in performance at a temperature higher than 500 DEG C in the prior art. The brazing filler metal comprises the following components in parts by weight: 18 to 24 parts of Ni, 14.3 to 19 parts of Cr, 16.8 to 22.5 parts of Co, 15.9 to 21 parts of Fe, 10.1 to 13.5 parts of Cu, and 0 to 24.9 parts of Ti or TiH2. The preparation method comprises the following steps of: carrying out vacuum melting on the weighed components at the temperature of 1200 to 1800 DEG C, performing linear cutting and carrying out foiling or composite tabletting on the components, so as to obtain the brazing filler metal; or the preparation method comprises the following steps of: carrying out ball-milling on the components in a ball material mass ratio of (12-16):1, and then tabletting and cleaning the components to obtain the brazing filler metal. The strength of the alloy joint obtained by using the method reaches 35 to 71 MPa, and the strength retention of the alloy joint at a high temperature of 800 DEG C exceeds 67%.
Owner:HARBIN INST OF TECH

Inorganic binder, preparation method and its application in preparation of porous ceramics

ActiveCN101182231AIncreased grain boundary bonding areaHigh strengthNon oxide ceramicsFoaming agent
The invention relates to an inorganic bond, a preparation method thereof and an application for the preparation of a porous ceramic thereof. The bond consists of alumina and/or aluminum hydroxide, phosphoric acid and boric acid, wherein, the weight percentage content of the alumina and/or the aluminum hydroxide is 70 percent to 99.5 percent, the weight percentage content of the phosphoric acid is 30 percent to 0.5 percent, and additionally the weight percentage content of the boric acid is 0 percent to 15 percent. The weight percentage content of the aluminum hydroxide is converted into Al2O3. The mol ratio of phosphor and aluminum is less than one. When the bond is used for preparing for the porous ceramic, firstly the granular diameter of the alumina or the aluminum hydroxide used for preparing for the bond is confirmed, and the granular diameter of the alumina or the aluminum hydroxide for using is 0.01 time to 0.5 time of the granular diameter of ceramic powder material; non-oxide ceramic powder material is mixed uniformly and mixed uniformly with pore-forming agent or vesicant to be molded and sintered, the sintering temperature is between 900 DEG C to 1600 DEG C. The sintering atmosphere is processed in air or under the inert atmosphere.
Owner:江西高环陶瓷科技股份有限公司

Method for preparing titanium nitride ceramic powder

InactiveCN101462701AWell mixedWith wet chemical methodNitrogen compoundsSucroseReaction rate
The invention relates to a method for preparing titanium nitride ceramic powder, which belongs to the field of the preparation of ceramic powder. A titanium source comprises soluble titanium salt, namely titanium tetrachloride or titanium tetrabromide, and a carbon source comprises glucose, sucrose, citric acid and soluble starch. Nitric acid is used as an oxidizing agent, and urea is used as a fuel; and ammonium nitrate is used as a preparing agent. The mol ratio Ti ;C of the titanium source to the carbon source is 1 to (4-16), and the mol ratio of the nitric acid with the ammonium nitrate to the urea with the ammonium nitrate is (1-12) ;2. Various raw materials are dissolved in water and then are heated at a temperature of between 100 and 600 DEG C, and a solution undergoes a combustion reaction to generate precursors; the precursors are pulverized and then are pretreated for 0 to 10 hours at a temperature of between 200 and 800 DEG C, and then a carbon thermal reduction is carried out for 1 to 10 hours in the atmosphere of flowing nitrogen at a temperature of between 800 and 1,800 DEG C. Follow-up treatment is carried out on products to obtain titanium nitride powder. The titanium source and the carbon source in the precursors of the invention have fine granularity and are uniformly mixed; therefore, the method has good reaction activity and also has the advantages of lowering the temperature of the carbon thermal reduction reaction and improving the reaction rate. The method can prepare nanometer-level non-oxidized ceramic powder with good decentrality.
Owner:UNIV OF SCI & TECH BEIJING
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