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1918 results about "Spray Granulation" patented technology

Preparation method for silicon carbide ceramic tube or rod

The invention relates to a preparation method for a silicon carbide ceramic tube or rod. An extrusion moulding method is adopted to form a blank body; a normal pressure sintering method is adopted for sintering; and submicron level silicon carbide powder and additives are taken as main raw materials. The preparation method comprises the following steps: 1) carrying out ball milling on the main raw materials by a dry method, adding water, a dispersant, a plasticizer, a lubricant and a liquid state binder, and then carrying out ball milling by a wet method; 2) adopting a spray granulation process to granulate silicon carbide slurry; 3) extruding the blank body by a one-shot direct extrusion moulding method after vacuum pug, corrosion, and vacuum pug; 4) drying the molded blank body by a stage drying mechanism; and 5) placing the blank body of the silicon carbide ceramic tube or rod in a vacuum furnace and carrying out sintering for two times by taking argon gas as protective gas. The high temperature resisting strength and the corrosion resistance of the silicon carbide ceramic tube or rod prepared by the method are both better than those of a reactive sintered product. Compared with a hot press sintering method, the method has lower limit on the product shape and size, and lower cost. The method is suitable for the industrialized production.
Owner:宁波欧翔精细陶瓷技术有限公司

Method for preparing organic sustained release fertilizer synergist

The invention provides a method for preparing an organic sustained release fertilizer synergist. The synergist comprises the following components in portion by weight: 25 to 60 portions of organic component, 3 to 15 portions of synergistic component, 10 to 13 portions (solid) and 3.5 to 9 portions (liquid) of sustained release component, 0.5 to 5 portions of trace elements, 18 to 30 portions of inorganic nutrient, and 2 to 7 portions of additive. The synergist is prepared by the method of weighing, mixing, spray granulation and low-temperature drying, wherein the organic component contains 2 to 5 portions of humic acid, 25 to 45 portions of mature garbage or barnyard manure, and 2 to 5 portions of residue of monosodium glutamate and sugar; the synergistic component contains 1 to 3 portions of zeolite, 1 to 5 portions of fly ash, and 2 to 5 portions of synergistic agent; the sustained release component contains 10 to 13 portions of bentonite, 0.02 to 0.1 portion of nitrification inhibitor, and 4 to 8 portions of urease inhibitor (liquid); the trace elements contain 0.1 to 1 portion of zinc sulfate, 0.1 to 1 portion of manganese sulfate, 0.1 to 1 portion of borax, 0.1 to 1 portion of copper sulfate, and 0.1 to 1 portion of ferrous sulfate; the inorganic nutrient contains 6 to 9 portions of urea, 7 to 9 portions of ammonium phosphate, and 5 to 7 portions of potassium sulfate; and the additive contains 2 to 7 portions of plaster. The synergist is suitable for the planting of field crops and forest fruits.
Owner:新疆满疆红农资化肥科技有限公司

Spherical porous silicon/carbon composite material as well as preparation method and application thereof

The invention discloses a spherical porous silicon/carbon composite material as well as a preparation method and application thereof. The spherical porous silicon/carbon composite material is structurally characterized in that a SiOx/C matrix, graphite with small particle size and a conductive agent are dispersed in porous amorphous carbon, wherein the average particle diameter is 12-25mu m; the method comprises the following steps of carrying out first coating on a SiOx raw material with powder pitch, and performing heat treatment so as to obtain a SiOx/C material; then performing ball milling by use of a wet method so as to reduce the particle diameter of powder, adding a carbon source adhesive, the graphite with the small particle diameter and the conductive agent, and performing high-speed dispersion, thereby obtaining pulp; and finally performing spray granulation and sintering on the pulp, thereby obtaining the final spherical porous silicon/carbon composite material. According to the invention, SiOx is dispersed in cracking carbon, the graphite and the conductive agent, so that SiOx volume expansion during a charge/discharge process is buffered, and the conductibility is enhanced; by virtue of the porous structure, the imbibition rate and cycle performance of the material can be effectively improved; by virtue of bitumencarb coating and high-heat treatment performed in advance, SiOx is prevented from being directly contacted with an electrolyte, and furthermore, the stability and first efficiency of the silicon/carbon material are improved.
Owner:ZHONGTIAN ENERGY STORAGE TECH

Method for preparing active electrode material of lithium ion battery

The invention discloses a method for preparing an active electrode material of a lithium ion battery. The method comprises the following steps of: preparing a nano-crystal with electrochemical activity into an aqueous solution, and adding a carbon source and a surface active agent into the aqueous solution to form a uniform and stable mixture solution; and preparing the mixture solution into spherical particles under the condition that the temperature is between 200 and 900 DEG C through a spray granulation method, and performing heat treatment on the spherical particles in 400-900 DEG nitrogen gas so as to form the active electrode material of the lithium ion battery. Conductive networks are distributed in the active electrode material, and the active electrode material has a porous structure, so that the active electrode material has good lithium ion and electron transmission channels; and the lithium ion battery prepared from the active electrode material has high specific capacity, high-current charging and discharging and high cyclical stability. The method for preparing the electrode material of the lithium ion battery through a spraying method can be easily applied to mass production, and is generally used for preparing various high-performance electrode materials of the lithium ion battery.
Owner:TSINGHUA UNIV

Method for preparing rare earth-doped yttrium aluminum garnet transparent ceramic

ActiveCN101985397AHigh linear transmittanceImprove mechanical propertiesRare-earth elementSpray Granulation
The invention relates to a method for preparing rare earth-doped yttrium aluminum garnet transparent ceramic. In the invention, high-transparency polycrystalline ceramic is prepared by using commercial powdered Y2O3, Al2O3 and Re2O3, of which the purities are over 99.9 percent, as main raw materials and by spray granulation dry pressing molding process and vacuum reaction and sintering, wherein the Re may be one or several of trivalent rare earth elements such as Nd<3+>, Yb<3+>, Cr<3+>, Er<3+>, Ce<3+>, Sm<3+> and Eu<3+>; MgO or CaO or tetraethyl orthosilicate (TEOS) or SiO2 is used as a sintering assistant; a certain amount of bonding agent, plasticizer and dispersant is added; the oxides, sintering assistant and additive are mixed and added into a liquid medium, and the mixture is ball-milled and mixed for 0.5 to 100 hours; after the powder materials are mixed uniformly, the powder is made into spherical or approximately spherical grains; blanks formed by drying pressing isostatic forming are degreased; sintering the blanks in a vacuum sintering furnace; and annealing after sintering. The transmissivity at a laser wavelength of the rare earth-doped yttrium aluminum garnet transparent ceramic prepared by the method is more than or equal to 77 percent.
Owner:FUJIAN INST OF RES ON THE STRUCTURE OF MATTER CHINESE ACAD OF SCI

Method for preparing organic synergistic soil conditioner

The invention provides a method for preparing an organic synergistic soil conditioner. The soil conditioner comprises the following components in portion by weight: 30 to 60 portions of organic component, 9 to 23 portions of synergistic component, 10 to 23 portions of conditioning component, and 15 to 30 portions of inorganic nutrient. The soil conditioner is prepared by the method of weighing, mixing, spray granulation and low-temperature drying, wherein the organic component contains 2 to 5 portions of humic acid, 25 to 45 portions of mature garbage or barnyard manure, and 2 to 5 portions of residue of monosodium glutamate and sugar production; the synergistic component contains 1 to 3 portions of zeolite powder, and 8 to 20 portions of synergistic agent; the conditioning component contains 2 to 10 portions of plaster, 9 to 13 portions of bentonite, 4 to 8 portions of polyvinyl alcohol (liquid), and 0.5 to 1.2 portions of starch (liquid); and the inorganic nutrient contains 4 to 7 portions of urea, 7 to 9 portions of ammonium phosphate, 5 to 7 portions of potassium sulfate, and 4 to 6 portions of ammonium sulfate. The preparation method is scientific, reasonable, simple and easy to operate; and the preparation method solves the synergistic effect of soil conditioners, and is suitable for the planting of field crops and forest fruits, in particular suitable for the conditioning of saline-alkali soil. By the determination of the national standard GB18877-2002, various indexes satisfy the national standard, and the content of the humic acid exceeds the standard requirement.
Owner:新疆满疆红农资化肥科技有限公司

Preparation method of tungsten carbide-cobalt or tungsten carbide-cobalt-chromium thermal spraying powder

The invention relates to a preparation method of tungsten carbide-cobalt or tungsten carbide-cobalt-chromium thermal spraying powder. The preparation method includes: proportionally mixing tungsten carbide powder with cobalt powder or tungsten carbide powder, cobalt powder and chromium powder, compounding slurry, performing spray granulation, screening and degreasing granulated powder prior to rapidly sintering the granulated powder in a vertical high-temperature sintering furnace, enabling the powder to continuously and uniformly pass through a heating area and a cooling area in a free-falling motion mode, completing sintering in the heating area for 0.1-5s at the sintering temperature of 1000-1700 DEG C in the nitrogen protective atmosphere, and performing classified screening for the sintered powder as required finally. The preparation method solves the problems of long production cycle, low production efficiency, high energy consumption and the like when tungsten carbide based composite spherical thermal spraying powder is prepared by a traditional method, is simple in technological process, capable of achieving continuous production, energy-saving and environment-friendly and can be widely applied to the fields of aerospace, machine manufacturing, petrochemical engineering and the like, and the obtained powder is uniform in component, high in sphericity degree and good in fluidity.
Owner:CENT SOUTH UNIV

Acidating agent for newborn piglet feed and preparation method thereof

The invention discloses an acidating agent for newborn piglet feed and preparation method thereof, relating to the feed additive field. The acidating agent is composed of the following raw materials by parts by weight: 40-55 parts of L-lactic acid, 20-25 parts of boletic acid, 2-4 parts of citric acid and 21-38 parts of auxiliary material, wherein the auxiliary material comprises the following components: 2-3% of dextrin, 7-8% of carboxymethyl cellulose cellulose sodium, the balance white carbon black; the raw materials added with water, mixing and spray granulation are carried out, so as to produce liquidity uniform granules. Pure organic acid composition is adopted, not only pH value of gastrointestinal tract can be reduced, but also sterilization anticorrosion can be realized, so as to regulate and control flora balance of gastrointestinal tract, thus being beneficial to breeding and growth of beneficial fungus such as lactic acid bacillus, inhibiting quantity of harmful fungus such as colibacillus and the like, improving animal anti-stress effect and improving animal immunity; and the acidating agent can directly participate in internal supersession, release energy, promote absorption of mineral substance, vitamin and nutritive material and improve animal production performance.
Owner:JINAN TIANTIANXIANG

Broadband wide temperature range high-power density low-loss manganese-zinc soft magnetic ferrite material and preparation method thereof

The invention discloses a broadband wide temperature range high-power density low-loss manganese-zinc soft magnetic ferrite material. The material comprises main ingredients, an auxiliary ingredient A and an auxiliary ingredient B, wherein the main ingredients comprise the following components in percentage by weight: Fe2O3, MnO and ZnO; based on the weight of the main ingredients, the auxiliary ingredient A comprises at least three of CaCO3, Nb2O5, NiO, SnO2 and Co3O4; and the auxiliary ingredient B comprises at least three of SiO2, Y2O3, K2CO3, Al2O3, CuO, MoO and Bi2O3. The preparation method of the material sequentially comprises the following steps: primary batching, primary sanding, pre-sintering, secondary batching, secondary sanding, performing component analysis, performing spray granulation, molding and sintering. The material disclosed by the invention has low loss in a temperature range from 20 DEG C below zero to 120 DEG C under the conditions of 100-500KHz and 100-200mT, and has high magnetic conductivity and high high-temperature saturation flux density. Compared with the conventional material, the material disclosed by the invention is energy-saving and can enable a switching power module to be miniature and efficient.
Owner:郴州市久隆旺高科电子有限公司

Super low-loss and small-line width microwave ferrite material and preparation method for microwave ferrite material

The invention relates to a super low-loss and small-line width microwave ferrite material and a preparation method for the microwave ferrite material and belongs to the field of microwave communication and magnetic materials. The main phase of the material is of a johnstonotite structure, and the chemical formula of the material is Y3-2x-yCa2x+yFe5-x-y-zVxZryAlzO12, wherein x is not less than 0.02 but is not more than 0.25, y is not less than 0.05 but is not more than 0.25, and z is not less than 0.01 but is not more than 0.25. The preparation method comprises the following steps of: calculating according to chemometry and weighing a raw material, vibratory milling, presintering, vibratory grinding and coarse crushing, sanding fine crushing, spray granulation, compression moulding and sintering. Proved by testing, the ferromagnetic resonance line width deltaH of the obtained material is not more than 1.27KA/m, the dielectric loss tgdeltae is not more than 0.5*10-4, and the insertion loss of an assembled microwave device is not more than 0.21dB, and thereby, the stability and the reliability of the obtained material are greatly enhanced, and the application range is broadened. The manufactured microwave ferrite device has the advantages of wide working band and low insertion loss.
Owner:TDG HLDG CO LTD

Composite organism slow release fertilizer product and producing method

InactiveCN101054314AOvercome the disadvantages of easy exceeding the standardOvercoming pollutionAgriculture gas emission reductionOrganic fertilisersMoisturePollution
The present invention relates to a chemical fertilizer and a manufacturing method thereof, specifically to a composite biological slow-release fertilizer product and its manufacturing method. Said composite biological slow-release fertilizer product in accordance with the present invention comprises granular fertilizer cores and coatings packing outside of the fertilizer cores, wherein said fertilizer cores are grains formed by a mixture of ternary compound fertilizer and the slow-release components which are mixture of urea and humic acids. Said coatings comprises at least animal oil and fat, bone meal and bacillus components. By replacing steam for heat spraying granulation with urea and humic acids melting complexing liquor, the manufacturing method in accordance with the present invention resolves the problem of moisture exceeding standard in 'three (organics, inorganics and bilogies) in one' fertilizer production and achieves the goal of nitrogen slow-release. At the same time, by adopting animal oil and fat and bone meal which can provide food such as lipids to animalcules and are easy to degrade as bacillus preparation carrier, said method overcomes the problems that the mixing of bacillus preparation and other fertilizer components leads to bacterial agent pollution and bacterium poisoning phenomenna. The present invention provides a 'three (organics, inorganics and bilogies) in one' composite biological slow-release fertilizer product which exhibits quick results, slow results and long results integrally, and a manufacturing method thereof.
Owner:王怀欣

Preparation method of normal pressure-sintered silicon carbide ceramics

The invention discloses a preparation method of normal pressure-sintered silicon carbide ceramics, which adopts a solid normal pressure sintering method and takes submicro silicon carbide powder, graphite powder and boron carbide powder as main materials. The method comprises the following steps: 1) material grinding is carried out by adopting a staged ball milling mode, firstly, the main raw materials are ball-milled by adding water under the environment of the pH value being 10-12 to lead the agglomerated silicon carbide micro powder and other main raw materials to be evenly dispersed; then a plasticiser, a lubricant and water soluble phenol resin are added and ball-milled for a period of time; and finally a caking agent is added for ball milling; 2) spray granulation technology is adopted for carrying out granulation on the silicon carbide slurry; (3) the materials after granulation are maintained under constant temperature and humidity; (4) double-sided compression moulding is carried out on the maintained materials; (5) a staged drying mechanism is adopted for drying the molded body; and (6) the silicon carbide body is put in a vacuum firing furnace for being subjected to two times of sintering by taking the argon as protective gas. The silicon carbide ceramics prepared by the method have superior performance, corrosion resistance and long service life, and are applicable to commercial process.
Owner:宁波欧翔精细陶瓷技术有限公司

Amino acid fermentation bacteria utilization method

The invention discloses an amino acid fermentation bacteria utilization method, which belongs to the technical field of amino acid production. The method comprises the steps that by taking glutamic acid fermentation as an example and adopting the isoelectric point of fermentation broth, a disc separator is utilized to separate mycoprotein in the fermentation broth, and a moderate amount of compound enzyme is added into the mycoprotein serum, so that the walls of bacteria are broken and the bacteria are enzymetically hydrolyzed. The enzymatic hydrolysate is separated by the high-speed disc separator, and the cell walls are removed, the obtained clarified enzymatic hydrolysate is concentrated under low temperature to produce the enzymetically hydrolyzed mycoprotein extract, or the clarified enzymatic hydrolysate is dried by a gunite granulation fluidized bed drier, a spray granulation drier and the like to produce the enzymetically hydrolyzed mycoprotein powder. In the method, the utilization value of the mycoprotein is greatly increased, so that the mycoprotein is changed from cheap feed into high value-added yeast extract and yeast powder substitute, the product can be used as fermentation ingredient and in other fields, the resources can be sufficiently utilized in the whole process, the purposes of energy saving and consumption reduction are achieved, and the invention has a broad application prospect.
Owner:HULUNBEIER NORTHEAST FUFENG BIOTECHNOLOGIES CO LTD
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