324results about How to "Achieve densification" patented technology

The invention discloses a method for densifying wood and densified wood manufactured by the same. The method comprises: sealing the cross section of wood by using a hydrophobic material, wherein the water content of the wood is less than 12 weight percent; coating softener on the surface and/or shallow layer of the sealed wood; and performing the hot pressing of the wood of which the cross section is sealed and which is coated with the softener at a temperature above the boiling point of the softener to densify the wood. The method for densifying wood can compress the wood to different extent according to needs. The method is simple and easy to operate, requires short time and simple equipment and makes product cost low. The densified wood manufactured by the method of the invention is greatly improved in surface density, hardness and wear resistance.

The invention discloses a sintering preparation method of boron carbide ceramic, which comprises the following steps: 1. sintering: carrying out mixing and ball milling on boron carbide powder, carbon powder, metal powder, a dispersant, an adhesive and deionized water to make a slurry, carrying out spray granulation, pressing into a biscuit, presintering for debonding, and carrying out thermal-insulation sintering at lower sintering temperature (slightly higher than the melting point of metal), thereby implementing primary shrinkage sintering of the product by utilizing the surface tension of the molten metal in the system; and 2. sintering: continuing enhancing the sintering temperature, carrying out in-situ reaction to generate metal carbide, metal boride or metal boro-carbide and nano B4C which have higher sintering activity, and forming a solid solution with boron carbide granules by using the metal carbide, metal boride or metal boro-carbide and nano B4C as sintering assistants to promote the further shrinkage sintering of the system, thereby obtaining the high-performance boron carbide ceramic. The method has the advantages of both the normal-pressure sintering technique and the reactive sintering technique.

A copper base alloy, which possesses high-strength, high conductivity, oxidation resistance and contains silver of low content, is characterized in that said high-strength high-conductivity oxidation-resistance low-silver copper base alloy is composed of low-silver copper base alloy powder, diamond powder of 0.2-1.0% and graphitized nanometer carbon fibre and is prepared through a powder metallurgy technological process, wherein said low-silver copper base alloy powder contains Ag of 0.08 -0.12%, Y, La and Ce of 0.05 -0.5% or one of misch metal or mixture of several misch metal. Said alloy in accordance with the present invention possesses higher intensity and hardness, stronger anti-crackle forming and stomatic expandability, and exhibits definite puddle welding resistance and better electroconductive performances at the same time.

The invention discloses a method and device for realizing laser point cloud densification and computer equipment. The method for achieving laser point cloud densification comprises the steps that original point cloud of a target scene is obtained; projecting the original point cloud to a cylindrical surface according to a front view angle, generating a first front view, the front view angle beingrelated to an azimuth angle when the laser radar collects the original point cloud; based on a mapping relation between different resolution front views constructed by a deep learning model, mapping the first front view to obtain a second front view, the resolution of the second front view being higher than the resolution of the first front view; and projecting the second front view to a coordinate system where the original point cloud is located to obtain dense point cloud of the target scene. By adopting the method and the device for realizing laser point cloud densification and the computerequipment provided by the invention, the problem of relatively poor densification effect of the laser point cloud in the prior art is solved.

The invention relates to a preparation method of pseudo-boehmite and a microcrystalline corundum abrasive. The method comprises the steps of: hydrolyzing aluminium isopropoxide under a hydrothermal condition so as to obtain the pseudo-boehmite with a particle diameter of 3-20nm, then preparing, drying, calcinating and sintering a pseudo-boehmite gel, thus obtaining the microcrystalline corundum abrasive. With controllable technical conditions, the method of the invention is suitable for large scale production, and the obtained microcrystalline abrasive has a particle size of 50-300nm, and a compact structure, with a density of 3.9-4.0g/cm<3> and hardness of 19-23GPa. Besides used as a wear resistant material, the obtained microcrystalline corundum abrasive can also be used in high temperature materials, matrials for electronic devices, high frequency insulating materials, aerospace materials, information materials and the like.

A disclosed preparation method for high-performance WC-Co nanocrystal cemented carbide comprises: taking nanometer tungsten carbide (WC) powder, ultrafine cobalt (Co) powder and ultrafine vanadium carbide (Cr2C3) powder as raw material powders, employing an alcohol wet grinding technology, and performing vacuum sintering and hot isostatic pressing sintering to prepare the WC-Co nanocrystal cemented carbide. By employing the above method for preparing nanocrystal cemented carbide, WC crystal grain structure is complete and clearly visible, by employing a method prescribed in ISO4499-2 for calculating two hundred or more WC crystal grains and averaging, the WC average crystal grain is less than 150 nm, the hardness HV30 is 1900 or more, the strength TRS is 4000 MPa or more and the metallographic structure is A02B00C00. The technology is simple, the process control is convenient, the production cost is low, and the prepared nanocrystal cemented carbide has the advantages of high densification degree and excellent performances.

The invention relates to a manufacturing method for a high-copper-silicon magnesium powder metallurgy aluminum alloy, and belongs to the field of material forming with a traditional powder metallurgy forming-sintering process combined with aluminum alloy machining. The manufacturing method includes the steps that an aluminum alloy ingot blank is manufactured through indoor temperature pressing-sintering; then, the aluminum alloy ingot blank is subjected to hot extrusion to obtain an aluminum alloy section; the aluminum alloy section is subjected to solid-solution quenching treatment; and finally, the aluminum alloy section obtained after quenching treatment is subjected to aging treatment. The performance of the material is significantly improved through proper low-temperature sintering assisted by heat machining and heat treatment matched with the temperature of low-temperature sintering, and particularly, an unexpected effect on increase of elongation is achieved. The manufacturing process is simple, the obtained product is excellent in performance, and large-scale industrialized application is facilitated.

The invention discloses a method for preparing tungsten carbide nano-powder. The method comprises the following steps of: dissolving ammonium paratungstate and citric acid in deionized water, and performing complexation in water bath; filtering and drying to obtain a precursor of tungsten oxide, and calcining under air atmosphere to obtain tungsten oxide powder; putting the obtained tungsten oxide powder in a tube furnace, introducing ammonia and nitriding to obtain tungsten nitride powder; mixing the obtained tungsten nitride powder and carbon black, performing ball milling, performing rotary evaporation drying and performing heat treatment under the air pressure of less than 200 Pa or inert atmosphere; or putting the obtained tungsten nitride powder in the tube furnace, and introducing the mixed gas of methane and hydrogen and carbonizing to obtain the tungsten carbide nano-powder. The preparation process of the method is simple, practical, and high in controllability and can easily realize large-scale production; the particle size of the prepared powder is small, the particle size distribution is uniform and the aggregation degree is low; and the method has high sintering activity, and densification can be realized by performing hot pressing sintering at the temperature of 1,700 DEG C.

The invention relates to a method for extruding and molding metal powder gelatin, which belongs to the field of metal part preparation in powder metallurgic production technology. The method is characterized by comprising the steps: firstly, premixed liquid with finite concentration is prepared; then, metal powder is added into the premixed liquid to prepare a stable gelatin system; the stable gelatin system is extruded and molded to prepare a blank body; and finally, the blank body is sintered into a part. The invention breaks through the traditional molding technology and can prepare metal products with large sizes and complicated shapes. Compared with the pressure molding, the invention solves the problems of complicated shape limitation and energy consumption caused by overlarge pressure needed by molding, and greatly improves the molding condition. Compared with the injection molding and the hot pressure casting molding which need to be added with a lot of organic binding agents, the method does not need a special degreasing step, has simple technology and can greatly reduce the production cost.

The invention relates to a method for preparing dense fluoride ceramic films on a magnesium surface and a magnesium alloy surface and belongs to the technical field of metal surface treatment. The method comprises the following steps of: chemically passivating a magnesium alloy; preparing a single-pulse ceramic film; and preparing a double-pulse ceramic film. In a chemically passivating process, solution such as hydrofluoric acid, phosphoric acid, hydrogen fluoride amine and the like are used; the preparations of the single-pulse ceramic film and the double-pulse ceramic film are mainly performed in a fluoride electrolyte-containing system, wherein potassium fluoride (sodium) is taken as a main salt; phosphate is taken as an additive; and citrate or tartrate is taken as a main stabilizing agent. The fluoride ceramic film obtained by the method is complete and dense, has high hardness, is firmly combined with a substrate, can be separately used as a protective layer and can be prepared into a composite surface functional layer which has higher corrosion resistance, higher wearing resistance and high hardness after subsequent processing treatment. The overall process of the method has the advantages of simple flow, low equipment cost, environment friendliness and the like.

The invention relates to a Y2O3-MgO nano-composite ceramic and a preparation method thereof. The Y2O3-MgO nano-composite ceramic is shown as xY2O3.(1-x)MgO, wherein x is the percentage of the mole number of Y2O3 to the total mole number of Y2O3 and MgO; the value of x is more than or equal to 0.01 and less than or equal to 0.99. The method comprises the following steps: preparing Y2O3-MgO nano-composite powder by adopting a sol-gel method; sintering the sieved composite powder by virtue of discharge plasma sintering or hot isostatic pressing sintering to obtain the infrared transparent Y2O3-MgO nano-composite ceramic.

The invention discloses nanostructured lithium orthosilicate ceramic spheres used for tritium propagation and a preparation method thereof. The nanostructured lithium orthosilicate ceramic spheres are made by preparing precursor powder with uniform particle size through a solvothermal method, obtaining a lithium ceramic sphere blank with a uniform microstructure through wet moulding, and carrying out two-step sintering. The prepared lithium orthosilicate ceramics is high in purity, good in sphericility, small in hole size and uniform in hole dispersion, has a crystal grain size in nanometer order and allows the radiation resistance, mechanical properties and tritium release properties of tritium propagation ceramics to be improved at the same time.

The invention provides a method for preparing a high density nanocrystalline hard alloy by step sintering, and belongs to the technical field of novel materials and novel powder metallurgy. The method comprises the following steps: firstly determining the dosage of the raw materials according to the requirements on the content of Co in the final hard alloy based on nanoscale purple tungsten oxide, cobaltous oxide, carbon black and mixed powder of vanadium oxide and chromic oxide as raw materials, mixing the raw materials and performing ball milling, then pressing the raw materials to blocks and conveying the pressed raw materials into a vacuum pump to perform a in-situ reaction to prepare nanometer composite powder with uniform distribution and good dispersity; filling the nanometer composite powder into a high density hard alloy mold, performing discharge plasma sintering, and performing segmented heating, heating up and heat preservation processes to obtain a pre-sintered block with controllable length and size of crystalline grain; finally, putting the pre-sintered block in a high-strength graphite mold to perform high temperature instant discharge plasma quick sintering densification to finally obtain a dense nanocrystalline hard alloy block material. The method provided by the invention can be used for effectively improving the density and mechanical properties of the hard alloy block material.

The invention discloses a method for quickly preparing an Ag2Se block thermoelectric material through self-homogenization for the first time. Ag powder and Se powder are used as raw materials; firstly the raw materials are easily mixed, and then the mixed raw materials are directly subjected to plasma activated sintering (PAS), so compact Ag2Se block thermoelectric material can be prepared in several minutes. The process dissolved by the method is super easy, the preparation time is super short, the obtained product is uniform in component distribution, and an obvious effect of self-homogenization is shown. The prepared Ag2Se block thermoelectric material is superior in performance, the room temperature ZT exceeds 0.6, and a good foundation is laid for large-scale preparation and large-scale application of the Ag2Se compound.

In the thermally conductive grease of the present invention, etc., the particles of the inorganic powder have a polyhedral shape, and 0.2 to 2.0 wt% of a nonionic surfactant is added with respect to 40 to 90 volume % of the mixed powder, and 10 to 90 wt % of the nonionic surfactant is mixed. 60% by volume of base oil (resin), the mixed powder is composed of 40-90% coarse particles with an average particle diameter of 5-17 μm and 10-60% with an average particle diameter of 1/3-1/3 of the coarse particles Composed of 40 particles.

The invention discloses a method for rapidly preparing high heat conduction Si3N4 ceramic with low cost. The method is characterized in that Si powder is taken as a raw material, ZrO2 powder is taken as a nitridation catalyst, ZrO2-MgO-Re2O3 is taken as a sintering aid, wherein Re2O3 is taken as a rare earth oxide, Si, ZrO2 and MgO-Re2O3 are mixed according to mass fraction and then dried to obtain a Si-ZrO2-MgO-Re2O3 mixing powder; the mixing powder is subjected to a two-step insulation method and a pressureless sintering process to obtain the high heat conduction Si3N4 ceramic; According to the ceramic material, the relative density is higher than 95%, hardness is 8-20 GPa, fracture toughness is 3-8MPa.m<1/2>, bending strength is 200-1000Mpa, and the thermal conductivity is 20-100W.m<-1>,K<-1>. By introducing a ZrO2 catalyst, Si powder nitridation IS accelerated, the introduction of ZrO2-MgO-Re2O3 can improve the densification of Si3N4, and the high heat conduction Si3N4 ceramic can be rapidly prepared with low cost.

The invention provides a preparation method of solid spherical metal powder for additive manufacturing, and belongs to the field of additive manufacturing. According to different requirements of different additive manufacturing technologies for powder, atomized powder is subjected to mechanical ball milling and plasma balling, through the compatibility of milling balls with different diameters andthe synergistic effect of ball milling parameters, ball-milling powder within the required particle size range is obtained through ball milling, then, ball-milling powder is subjected to balling treatment through plasma balling, and powder which is uniform in particle size distribution, solid, free of defect, high in degree of sphericity and good in fluidity is obtained and completely meets the additive manufacturing requirements.

The invention discloses a density enhancing method of piezoelectric ferroelectric ceramic materials with bismuth layer structure. According to a chemical formula: (Am-1BmO3m+1) <2-> (Bi2O2) <2+>; and molar ratio A: B: Bi = m-1: m : 2, materials are calculated and weighted, wherein, the A is univalent, bivalent, trivalent or quadrivalent metal ion that is suitable for dodecahedral coordination; the B is trivalent, quadrivalent, pentavalent or sexivalent metal ion that is suitable for octahedral coordination; the production processes are that: mixing, pre-synthesizing, grinding, forming and sintering; the sintering process is that: the temperature of the obtained material from the last step is raised to 1100 to 1250 DEG C at a speed of 2 to 5 DEG C per minute, and is lowered to 50 to 150 DEG C within 1 to 5 minutes; under the temperature of 950 to 1150 EDG C, insulation at the low temperature is done for 5 to 20 hours; then the temperature is lowered to 500 DEG C at a speed of 3 to 7 DEG C per minute, and the obtained material is naturally cooled with a furnace. The invention can obtain the piezoelectric ferroelectric ceramic materials with grain-refining and density bismuth structure.

The invention discloses a method for preparing an MnZn ferrite magnetic core by multi-physical field coupling. The method comprises the following steps of filling MnZn ferrite powder having particle sizes of 0.7 to 2.0 micrometers into a mold, directly powering on the mold with the MnZn ferrite powder to fast heat the mold at a heating rate of 5 to 200 DEG C/s under the pressure of 10<-2> Pa, simultaneously, applying an acting force of 50 to 100MPa to two ends of the mold, heating to a temperature of 600 to 1200 DEG C under the action of a continuous electric field, carrying out heat preservation for 2 to 10min so that the MnZn ferrite powder undergoes a solid-phase reaction in the mold and is molded fast, interrupting power supply, and taking out a sintered body. The method has the advantages that a heating rate is greatly improved so that diffusion between atoms is promoted; and through the pressure on the two ends of the mold, a MnZn ferrite magnetic core solid-phase reaction, compaction molding and compact sintering are carried out simultaneously so that performances of a molded magnetic core are guaranteed.

The invention relates to a preparation method of an ablation resistant C/SiC ceramic matrix composite material. The method includes the steps of: (1) providing a porous C/C composite preform; (2) making the preform into a C/SiC composite material; (3) mixing polysilazane, boron powder and a solvent, with the mass percentage of polysilazane in the mixture being 30-40% and the mass percentage of boron powder in the mixture being 10-30%, and mixing the mixture uniformly to obtain a SiBCN precursor solution; and (4) using the SiBCN precursor solution for impregnation curing and cracking of the composite material, thus obtaining the ablation resistant C/SiC ceramic matrix composite material. The method provided by the invention can acquire the composite material with high density, low ablationrate and excellent comprehensive properties.

The invention discloses a method for preparing a carbon/carbon composite material. The method comprises the steps of: uniformly mixing a biomass capable of being hydrolyzed with water to obtain a biomass dispersing liquid; immersing a carbon fiber prefabricated body in the biomass dispersing liquid to obtain a reaction system Al; then reacting the reaction system A in a hydrothermal kettle under the heating condition, after the reaction is ended and the reaction system is cooled, taking the carbon fiber prefabricated body deposited with the biomass out and washing with water to obtain the carbon/carbon composite material. The method is green and environmental-friendly, efficient and feasible, is low in cost and reaction temperature and is capable of realizing rapid densification of the carbon/carbon composite material. The prepared carbon/carbon composite material is a carbon fiber reinforced composite material using the biomass carbon as a matrix, and is rich in hydroxide groups and carbonyl groups on the surface, thereby being good in biological activity.

The invention belongs to the technical field of ceramic substrates, and particularly relates to a high-power LED (Light-Emitting Diode) heat dissipation ceramic substrate. The ceramic substrate comprises the following materials in percentage by mass: 70-80 percent of alumina powder, 3-8 percent of melamine, 3-6 percent of hydroxymethyl cellulose, 6-10 percent of deionized water and 5-10 percent of composite sintering aid, wherein the composite sintering aid comprises the following materials in percentage by mass: 40-60 percent of silicon powder, 5-10 percent of aluminum powder, 20-30 percent of kaolin powder and 10-30 percent of calcium fluoride. The ceramic substrate has the advantages of high heat conductivity coefficient, excellent heat resistance, high bending strength and avoidance of the phenomena of bending, wrapping and the like. Through adoption of an appropriate sintering method and selection of an appropriate sintering aid, denseness of an alumina ceramic sintered body is realized, and the heat conductivity of alumina ceramics is increased greatly.