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46results about How to "The preparation process is practical" patented technology

Method for preparing tungsten carbide nano-powder

The invention discloses a method for preparing tungsten carbide nano-powder. The method comprises the following steps of: dissolving ammonium paratungstate and citric acid in deionized water, and performing complexation in water bath; filtering and drying to obtain a precursor of tungsten oxide, and calcining under air atmosphere to obtain tungsten oxide powder; putting the obtained tungsten oxide powder in a tube furnace, introducing ammonia and nitriding to obtain tungsten nitride powder; mixing the obtained tungsten nitride powder and carbon black, performing ball milling, performing rotary evaporation drying and performing heat treatment under the air pressure of less than 200 Pa or inert atmosphere; or putting the obtained tungsten nitride powder in the tube furnace, and introducing the mixed gas of methane and hydrogen and carbonizing to obtain the tungsten carbide nano-powder. The preparation process of the method is simple, practical, and high in controllability and can easily realize large-scale production; the particle size of the prepared powder is small, the particle size distribution is uniform and the aggregation degree is low; and the method has high sintering activity, and densification can be realized by performing hot pressing sintering at the temperature of 1,700 DEG C.
Owner:SHANGHAI INST OF CERAMIC CHEM & TECH CHINESE ACAD OF SCI

Traditional Chinese medicine contrast medium adjuvant used for B ultrasonic and preparation method thereof

The invention provides a traditional Chinese medicine contrast medium adjuvant used for B ultrasonic, which comprises the following materials in part by weight: 10-20 parts of bighead atractylodes rhizome, 10-20 parts of poria cocos, 10-20 parts of turmeric, 10-20 parts of tangerine peel, 10-20 parts of cortex magnoliae officinalis, 10-20 parts of radix aucklandiae, 10-20 parts of Rhizoma atractylodis, 10-20 parts of cuttlebone, 10-20 parts of calcined oyster shell, 10-20 parts of Chinese yam, 10-20 parts of charred triplet, 10-20 parts of myristica fragrans, 10-20 parts of gizzard pepsin, 10-20 parts of rhizome cyperi, 10-20 parts of codonopsis pilosula, 10-20 parts of combined spicebush root, 10-20 parts of eclipta, 10-20 parts of jasmine, 10-20 parts of baical skullcap root and 10-20 parts of field pennycress. The traditional Chinese medicine contrast medium adjuvant used for B ultrasonic provided by the invention not only can adapt to stomach hyperfunction type, but also can adapt to decreased stomach function type, and also can be applied to the mixed type of various flatulence and mucinosis, check time is short, imaging rate is high, and preparation process is simple and practical. The contrast medium adjuvant has no obvious toxic side effect and has prospect on further development research.
Owner:张洪英

Self-polishing antifouling coating excluding cuprous oxide and organic tin and preparation method thereof

InactiveCN107841216APrevents marine life from accumulatingContinuous antifouling effectAntifouling/underwater paintsPaints with biocidesSolventSeawater
The invention belongs to the technical fields of antifouling coatings and underwater coatings, and discloses a self-polishing antifouling coating excluding cuprous oxide and organic tin and a preparation method thereof. Problems that an existing antifouling coating is not environment-friendly, and the like, are solved. The coating provided by the invention is prepared from a film-forming substance, a capsaicin raw material, an environment-friendly antifouling agent, porous powder, a pigment, a filling material, an additive and a solvent. The preparation method comprises the following steps ofdispersing through multiple-time agitation. According to the antifouling coating provided by the invention, a compound antifouling agent is stored by utilizing the micron, the nanometer and a hole ofthe porous powder; afterwards, the porous powder and the compound antifouling agent are wrapped and isolated by utilizing silica and the compound antifouling agent; the irritation action, on production and construction personnel, of the compound antifouling agent can be decreased to some extent; the rate that capsaicin and the environment-friendly antifouling agent are released into seawater is effectively controlled; thus, the long-time and continuous favorable antifouling effect is more easily obtained; the self-polishing antifouling coating is safe and friendly to a marine environment. Thepreparation method provided by the invention is simple in process and practical and basic raw materials to which the preparation method relates can be all purchased on the market.
Owner:ARMOR ACADEMY OF CHINESE PEOPLES LIBERATION ARMY

Method for preparing zirconia gradient porous ceramics with ice as template

The invention relates to a method for preparing zirconia gradient porous ceramics with ice as a template. The method comprises: taking ice as a pore-forming template, adding distilled water, a Na2SiO3.9H2O binder, a yttrium oxide sintering aid and a ceramic powder water system dispersant into zirconia powder, conducting ball milling and mixing so as to obtain a stable suspending liquid, which, after vacuum pumping, is injected into a die for low temperature rapid freezing, carrying out vacuum freeze drying to a frozen sample, performing demoulding and then put it into a high temperature furnace for sintering, thus obtaining zirconia porous ceramics. The pore structure of the porous ceramics is completely decided by appearance characteristics of ice crystals. Compared with other porous preparation technologies, ice is an ideal template for making porous ceramics, and the process of the invention is characterized by environmental protection and low cost. The prepared zirconia porous ceramics have obvious gradient porous structures. The use of a binder in the invention can prevent a green body from cracking and deforming during drying, thus enhancing the mechanical strength of products. And adding of a yttrium oxide sintering aid can lower the sintering temperature. The prepared zirconia porous ceramics has compressive strength up to 8MPa.
Owner:SHAANXI UNIV OF TECH

Type-B ultrasonic traditional Chinese medicinal gastroenterography assistant and method for preparing same

The invention provides a type-B ultrasonic traditional Chinese medicinal gastroenterography assistant and a method for preparing the same. The traditional Chinese medicinal gastroenterography assistant comprises egg shells, asteroid, clam shells, elaeagnus pungens, hairyvein agrimony, licorice, calcined dragon bone, hyperforin, purple lythrum herbs, kadsura longipedunculata, rhubarb, roots of yellow Himalayan raspberry, cornu cervi degelatinatum, red umbilicaria, hop, amomum aromaticum, wampee, rhizoma nardostachyos, areca peels, pugionium and curcuma zedoaria. The type-B ultrasonic traditional Chinese medicinal gastroenterography assistant and the method have the advantages that the type-B ultrasonic traditional Chinese medicinal gastroenterography assistant is safe in use, free of allergic reaction, short in examination time, high in developing rate, convenient to use and low in cost and is painless, noninvasive and non-toxic, a novel technology and a novel method are provided for early and accurate diagnosis of diseases, a powerful basis for clinical diagnosis is provided, the type-B ultrasonic traditional Chinese medicinal gastroenterography assistant is perfect and novel, and a process for manufacturing the type-B ultrasonic traditional Chinese medicinal gastroenterography assistant is simple and practical.
Owner:王发芬

Polyethylene terephthalate and polyurethane composite artificial blood vessel and preparation thereof

The invention discloses a polyethylene terephthalate and polyurethane composite artificial blood vessel and a preparation method thereof, belonging to the field of biomedical engineering. The artificial blood vessel is prepared from polyethylene terephthalate and polyurethane by means of an electrostatic spinning device with a stirrer. The prepared artificial blood vessel is a tubular object witha microporous structure. The polyurethane added in the artificial blood vessel can improve the elasticity of the blood vessel under the condition of not damaging the strength of the polyethylene terephthalate material, increase the compliance of the artificial blood vessel and achieve the requirements of clinical use. The polyethylene terephthalate and polyurethane composite artificial blood vessel has the advantages of high strength, large elasticity and compliance, good biocompatibility, strong anticoagulant property and large cell adhesion, and can meet the requirements of the clinical useof the artificial blood vessels with large diameter and small diameter. The preparation process is simple and practical, and applicable to preparing the artificial blood vessels with various different requirements on mechanical properties.
Owner:宁波贝昂生物材料有限公司

Aluminum sulfate-ferric chloride-poly dimethyl diallyl ammonium chloride ternary complex coagulant as well as preparation and application methods thereof

The invention discloses an aluminum sulfate-ferric chloride-poly dimethyl diallyl ammonium chloride ternary complex coagulant as well as preparation and application methods thereof. The preparation method comprises the following steps of: putting AS (Aluminum Salt) dry powder or solution in a mixed reactor, adding water to blend into an AS saturated solution, stirring the solution, adding FC (FeCl3) dry powder or solution, stirring while continuously adding water to blend so as to obtain a binary mixed solution; and stirring the binary mixed solution, adding PDMDAAC (Poly Dimethyl Diallyl Ammonium Chloride) colloid or dry powder to obtain a ternary mixed solution and continuously stirring the mixed solution until the PDMDAAC colloid is fully dissolved to obtain a stable AS-FC-PDMDAAC ternary complex coagulant which is diluted with water in any proportion or directly added for various kinds of raw water. The series of ternary complex coagulant provided by the invention can be used for various raw water coagulation treatments and waste sewage flocculation treatments as well as dewatering process of sludge and silt in single dosage mode according to the direct dosage amount requirement, and the use method is extremely convenient and simple.
Owner:NANJING UNIV OF SCI & TECH
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