433results about How to "Structural regulation" patented technology

The invention discloses a preparation method of a one-way wet conduction nano-fiber multilayer composite membrane with the wettability gradient. The method comprises the following steps that hydrophilic nano materials are dispersed in solvent, the nano materials are dispersed uniformly through ultrasound, a hydrophilic polymer is dissolved in the dispersing agent, a spinning solution A1 is obtained, and a hydrophilic nano-fiber membrane is deposited on a receiving base material through an electrostatic spinning method; hydrophilic nano materials are dispersed in solvent, the nano materials are dispersed uniformly through the ultrasound, a hydrophilic polymer is dissolved in the dispersing agent, and a spinning solution A2 is obtained; a hydrophobic polymer is dissolved in solvent, and a spinning solution B1 is obtained; the two spinning solutions are deposited on the hydrophilic nano-fiber membrane to form at least one diversion layer through the electrostatic spinning method; a hydrophobic polymer is dissolved in solvent, a spinning solution B2 is obtained, a hydrophobic nano-fiber membrane is deposited on the diversion layers through the electrostatic spinning method, and the one-way wet conduction nano-fiber multilayer composite membrane with the wettability gradient is obtained.

The invention discloses a graphene/ stannic oxide nanometer compounding resistance type film gas sensor, which takes ceramics as a basal body. The surface of the ceramic basal body is photo-etched and evaporated with multiple pairs of interdigital gold electrodes, and is coated with gas-sensitive films of graphene and stannic oxide nanometer composite, and the manufactured resistance type film gas sensor has the advantages of simple manufacturing process and low cost. The gas-sensitive film is composed of a grapheme namosheet layer in a three-dimensional nano-structure and stannic oxide crystal particle composite with an orientated growth characteristic, the introduction of the graphene can favorably reduce the resistance of sensor elements, and the formation of the three-dimensional nano-structure can obviously enhance the specific surface area of the composite, thus the absorption and the diffusion of the gas can be promoted so as to greatly enhance the room temperature gas sensitive response sensitivity of elements. The graphene/stannic oxide nanometer compounding resistance type film gas sensor has the characteristics of high response sensitivity to low concentration ammonia, fast response, favorable recovering performanc, capability of carrying out the detection at the room temperature, and the like, which can be widely applied in the agricultural and industrial production process, and the room temperature detection and control of the concentration of ammonia in the atmospheric environment.

Disclosed is an inorganic medicine, particularly modified montmorillonite, method for preparing the same and use thereof. The said modified montmorillonite means that dioctahedron of natural montmorillonite is not destroyed and basic chemical composition for the same is not changed, and the microstructure stacked from dioctahedron layer is changed to decrease the thickness of stacking layer and to expose and increase the end face charge and the interlayer charge of montmorillonite, thereby resulting in its lower degree of C axis order. The present medical use of montmorillonite is thus significantly strengthened, particularly the reversal treatment effect on chronic atrophic gastritis. Also disclosed are a medicine composition containing modified montmorillonite and the reversal treatment effect of natural montmorillonite on chronic atrophic gastritis.

The invention relates to a compound microbial organic fertilizer and a preparation method thereof. The compound microbial organic fertilizer is prepared from the following ingredients in parts by weight: 1-4 parts of trichoderma viride JUWEI002 fermentation liquor, 1-4 parts of bacillus subtilis JUWEI001 fermentation liquor, 20-30 parts of turfy soil, 33-38 parts of tobacco residue, 33-38 parts of silkworm faeces, 6-7 parts of calcium powder and 1-2 parts of potassium fulvate. The compound microbial organic fertilizer disclosed by the invention has the advantages that the quality of crops can be remarkably improved, the yield of the crops is increased, and the soil structure is improved.

The invention belongs to the field of nano-material preparation, in particular to a method for preparing a nano porous gold. In the invention, the nano porous gold is prepared by combining rapid setting and dealloying. The method comprises the following steps: firstly heating pure aluminium and gold to molten state; secondly; rapidly blowing out alloy liquid with inert gases to cause molten liquid metals to rapidly set on a copper roller which rotates at high speed to prepare alloy ribbons; and finally, carrying out dealloying treatment in acid or alkaline solution. After corrosion process, the nano porous gold is washed till neutrality in distilled water. In the method, the nano porous gold can be obtained by selecting corrosion solution with lower concentration, therefore, the nanoporous gold has simple and convenient operating process and is suitable for large-scale industrial production. In the method, the structure and size of the nanoporous gold can be adjusted according to the ingredients and corrosion solution of master alloy.

The invention belongs to the field of preparing a nanometer material, and particularly relates to a method for preparing nanometer porous silver. In the invention, the nanometer porous silver is prepared by the method combining the rapid solidification and the dealloying, wherein the method comprises the following steps: firstly, heating pure metal aluminum and silver to a molten state; secondly, utilizing inert gas to quickly blow out an alloy liquid and quickly solidifying the molten metal on a copper roller rotating at a high speed, so that an alloy ribbon is prepared; thirdly, performing dealloying treatment in acid etchant solution; and finally, after the corrosion, washing the nanometer porous silver to neutral in distilled water. The method uses the etchant solution in low concentration to obtain the nanometer porous silver, the operating process is simple, and the method is also suitable for mass industrialized production. The method can also control the structure and size of the nanometer porous silver according to compositions of the master alloy and types of the etchant solution.

The invention belongs to the field of agricultural technologies and particularly relates to a walnut rich in selenium and organic fertilizer rich in selenium for the walnut rich in selenium. The walnut and the organic fertilizer are mainly used for solving the technical problems that the fertilization amount of existing fertilizer for producing subsidiary agricultural products rich in selenium is difficult to control, the environment is polluted, dependence of crops is prone to generation, land is barren, and cost is high. According to the technical scheme, the walnut rich in selenium is obtained through fertilization of the self-made organic fertilizer rich in selenium, the selenium content of a walnut kernel ranges from 200 microgram per kilogram to 800 microgram per kilogram, and the walnut and the organic fertilizer have the advantages of being environmentally friendly, free of pollution and low in cost.

A suspended microbe carrier with high microbial affinity, adsorption and hydrophilicity is a macroreticular skeleton and millipore skeleton combined structure. Its preparing process includes such steps as preparing the aqueous solution of polyvinyl alcohol, proportionally adding sulfuric acid and formaldehyde solution, reaction, adding powdered imorganic filler, high-speed stirring, filling it in a mould, foaming by filling the pre-heated air via millipore air distributor, and treating at 40-80 deg.C for 4-24 hr.

The invention discloses a nitrile resin monomer, a nitrile resin polymer and a preparation method of the nitrile resin monomer and the nitrile resin polymer, belonging to the technical field of organic polymer materials. The nitrile resin monomer is a tetraphthalonitrile resin monomer containing benzoxazine cycle, and the nitrile resin polymer is a product obtained by heating polymerization of the nitrile resin monomer. The nitrile resin monomer has a low viscosity, a good mobility and the processing performances of low-temperature curing and the like at a low temperature. The nitrile resin polymer has the good curing performances of self-flame resistance, adhesion, heat stability and the like. The resin monomer has the good processing performances of benzoxazine resins, and the resin polymer has the high-temperature resistance of nitrile resins, thus reducing the curing processing temperature and being capable of being used in a high-temperature temperature, namely, having the advantages of low temperature processing, medium temperature formation and high temperature use; and the resin monomer and the resin polymer can be used in the fields of coatings, adhesives, electronic packaging materials, aeronautics, astronautics, ships, resin matrix composites and the like. The preparation method is simple and easy to control, low in reaction temperature, energy-saving, and suitable for industrialized production.

The invention relates to a preparation method for a finely structured POSS hybridization low dielectric material. The method takes a POSS monomer containing an active group and dual functional group organic micromolecules capable of having a click chemical reaction as the precursor of the finely structured hybridization low dielectric material, and makes use of an environmentally friendly click chemical synthesis method to connect the finely structured POSS molecules and the organic micromolecules onto the low dielectric material structure orderly. Through changing the composition, structure and performance of the organic molecular chain connected with POSS, the method realizes the adjustment and control of the structure, porosity, thermal property, mechanical property and dielectric constant of the finely structured hybridization low dielectric material.

The invention discloses a polysaccharide composition capable of adjusting the structure of intestinal floras and applications thereof. The composition is composed of konjak polysaccharide and ginseng polysaccharide according to a weight ratio of 1-99:1-99. The results of a large amount of tests show that konjak polysaccharide and ginseng polysaccharide are combined according to a specific ratio, the composition can change the intestinal floras specifically, the structure of intestinal floras is regulated, the health of intestinal tracts is improved; the konjak polysaccharide and ginseng polysaccharide are used together to generate a synergistic effect on regulating the structure of intestinal floras; and the composition can be used to treat enteric flora disturbance, is safe, and does not have any side or toxic effect.

The invention belongs to the field of health-care products, and particularly relates to a probiotics and Chinese herbal medicine compound preparation with a hypoglycemic function. The preparation is formed by mixing the components in parts by weight as follows: 25-30 parts of dioscorea roots, 15-25 parts of pueraria roots, 20-30 parts of cinnamon, 20-40 parts of lycium berries and 30-40 parts of freeze-dried probiotics powder, wherein probiotics comprises bacteria in percentage by weight as follows: 40% of bifidobacterium adolescentis, 40% of bifidobacterium longum, 10% of lactobacillus plantarum and 10% of lactobacillus rhamnosus. The preparation has the hypoglycemic function.

The invention belongs to the technical field of semiconductor optoelectronic materials, and in particular relates to a BeZnOS compound semiconductor material, its preparation method and application. The BeZnOS material provided by the present invention is a quaternary compound semiconductor material obtained by solid solution of BeO and ZnS in a certain proportion. Through the synergistic effect of compound substitution of Be and S, not only can the bandgap of ZnO be adjusted more freely, but also play a role Increase the solubility of the substituting elements Be and S in ZnO and eliminate the effect of mutual restraint between the band gap of the solid solution and the adjustment of the lattice constant. The BeZnOS quaternary compound is a wide bandgap semiconductor with freely adjustable bandgap, and can be used for light-emitting devices or photodetection devices in ultraviolet to solar blind regions. The BeZnOS compound semiconductor material provided by the invention can be grown by various methods such as pulse laser deposition, magnetron sputtering, electron beam evaporation, etc., and the equipment and operation process are simple. The BeZnOS single crystal thin film material provided by the invention is successfully synthesized for the first time in the world, and has very important significance for the development of ZnO-based optoelectronic devices with adjustable wavelength.

The invention discloses a method for synthesizing a highly directional nano flake Bi2Fe4O9 crystal at a low temperature. The method mainly adopts the hydrothermal preparation method and comprises the following steps that: Bi(NO3)3.5H2O and Fe(NO3)3.9H2O with the same mol ration are dissolved in a dilute nitric acid, a sodium hydrate aqueous solution is titrated into the mixed solution until the precipitation is complete, and the mixture is filtered and washed by water until the solution is neutral. The method is characterized in that the obtained precipitation is dissolved in a sodium hydrate aqueous solution with a concentration of between 8 and 20 mol per liter, 2 milliliters of H2O2 solution against 40 milliliters of the H2O2 solution are added, the mixture is put in a reaction kettle and reacts for 12 to 72 hours at a temperature of between 160 and 200 DEG C, the product is washed by de-ionized water and alcohol and is dried in an oven, and the obtained final product is the directionally growing nano flake Bi2Fe4O9.

The invention discloses suckling pig feed which comprises the following components in parts by weight: 35-40 parts of corn, 20-25 parts of extruded corn, 10-15 parts of bean pulp, 5-10 parts of fermented miscellaneous meal, 1-5 parts of syrup, 0.1-0.5 part of acidifying agent, 0.03-0.08 part of phytase, 0.1-0.5 part of zinc oxide, 0.1-0.5 part of lysine, 0.1-0.5 part of choline, 0.1-0.5 part of threonine, 0.01-0.05 part of tryptophan, 0.1-0.5 part of methionine, 0.1-0.5 part of calcium citrate, 0.5-1 part of monocalcium phosphate, 1-5 parts of plasma protein powder, 1-5 parts of lactose, 2-6 parts of low-protein whey powder, 1-5 parts of white sugar, 5-10 parts of glucose and 0.1-0.5 part of microecological preparation. The suckling pig feed has the beneficial effects that the immunity of suckling pigs is improved, the feed conversion ratio is reduced, the nutritional requirements of the suckling pigs within two weeks from feeding to weaning can be met, the suckling pig feed is high in palatability and high in digestibility, the diarrhea rate of the suckling pigs is reduced, and the production performance of the suckling pigs is improved.

A method for rapid in-situ detection of object surface pollutants is characterized in that a flexible and semi-transparent surface enhanced Raman substrate is used and is composed of a Raman active nanoparticle assembly body and a flexible polymer; by a way that the substrate is directly affixed to the surface of an object to be detected, or the substrate is rubbed back and forth on the surface of the object to be detected, or the substrate is coiled into a capillary, the adsorption and enrichment capacity of the substrate on the pollutants on the surface of the object to be detected is enhanced, then the on-site rapid in-situ detection of the pollutants on the surface of the object is achieved by a surface enhancing Raman technique. Compared with other detection methods, the method is simple, rapid, low in cost, and beneficial for on-site casual inspection, and has wide application prospects in the fields of environmental monitoring, food safety, medical treatment and health care and the like.

The invention discloses a pollution-free paddy rice planting method. The method comprises the following steps: A, planting milk vetch as green manure in a rice field, and applying a basic manure, wherein 500-800 kg of the basic manure is applied to each mu of the rice field; B, after the rice field is subjected to exposure, performing rotary tillage, ridge separation, irrigation and rice transplanting; C, applying a compound fertilizer to seedlings after the seedlings are inserted; D, grazing 8-15 7-10-day-old ducks to each mu of the rice field after 15-20 days of rice transplanting, evicting the ducks from the rice field after 25-40 days, spraying a biological pesticide, draining for 7-10 days, topdressing 30-100 kg of the compound fertilizer used in the step C to each mu of the rice field, irrigating till the depth of water is 8-10 cm, grazing 5-10 7-10-day-old ducks to each mu of the rice field again, and evicting the ducks from the rice field before 15-20 days of rice mature. According to the pollution-free paddy rice planting method, the yield is high, pollution is avoided, produced rice tastes good, and meanwhile, high-quality duck is obtained.

The present invention discloses a visible-light-responsive BiVO4/TiO2/graphene tri-material composite light catalyst and a preparation method thereof. The preparation method comprises the steps of (1) preparing a suspension system A containing BiVO4 nano particles, and a suspension system B containing a TiO2 sol-gel and graphene oxide; (2) proportionally mixing up the suspension system A and the suspension system B, conducting the heating treatment, separating and drying to obtain a BiVO4/TiO2/graphene oxide composite material; (3) suspending the BiVO4/TiO2/graphene oxide composite material in short-chain alcohol, adding a reducing agent, conducting the hydrothermal reaction and drying to obtain the visible-light-responsive BiVO4/TiO2/graphene tri-material composite light catalyst. The preparation method is simple and easy to operate, and low in cost. Based on the preparation method, the structure and the properties of the composite light catalyst can be regulated and controlled through simply changing the conditions of reactions and heat treatments.

The invention relates to the field of composite fertilizers, and in particular to a whole-element composite fertilizer and a preparation method thereof. The whole-element composite fertilizer consists of the following raw materials in parts by weight: urea, triple superphosphate, potassium sulfate, monoammonium phosphate, potassium chloride, ammonium molybdate, boric acid, polypeptide alkali chelate zinc, citrate chelate copper, long-lasting additives, illite powder, attapulgite powder and humic acid ammonium. The preparation method comprises the following steps: preparing pretreated raw materials, mixing and stirring, crushing cakes, pelletizing by using a pelletizer, drying granules, cooling the granules, screening, coating finished granules so as to obtain a finished product, and the like. The invention provides the whole-element composite fertilizer which is capable of effectively replenishing organic matters and various medium-trace elements which are urgently required by soil, improving soil structures, improving permeability, and promoting nutrient absorption of crops, and the invention further provides the reasonable preparation method for the whole-element composite fertilizer.

The invention provides a biological water flushing fertilizer. The biological water flushing fertilizer is prepared by mixing a microorganism strain and an organic fertilizer, wherein the microorganism strain is obtained by carrying out strain liquid fermentation on bacillus subtilis, brevibacillus laterosporu and bacillus mucilaginosus; the biological water flushing fertilizer is composed of the following components in percentage by mass: 10%-20% of the microorganism strain, 20%-30% of humic acid, 30%-60% of calcium nitrate or phosphorus nitrate, 5%-10% of boric acid, 5%-12% of magnesium sulfate, 5%-8% of ferrous sulfate, 1.5%-5% of organic matters, 2%-6% of sulfur powder, 0.5%-1.0% of bentonite and 1%-5% of an inductive agent. The preparation method comprises the following steps: liquid fermentation of the strain, adsorption of fermented strain liquid, and preparation of the biological water flushing fertilizer. According to the biological water flushing fertilizer, the nutritional value of fertilizer raw materials is obviously improved and the fertilizer effect is rapidly improved; the fertilizer utilization efficiency effect and the effect of preventing diseases and increasing the output are improved. Meanwhile, the soil physical and chemical properties are also improved; the hardening is eliminated, the soil is loosened, the pH value of the soil is adjusted and the soil structure is improved.

The invention provides a method for remedying soil heavy metal pollution, improving saline and alkaline land and recycling microalgae for resource utilization through a multi-pond-alga water circulation irrigation system, and belongs to the field of soil remediation and resource utilization. Through the interaction of man-made ponds, microalgae and soil, a pond-microalga combined remediation system is adopted as the core, the soil is prepared and domesticated to remedy the microalgae, the multiple ponds are used for collecting rainwater, the microalgae are cultivated and subjected to expandingpropagation, and the microalgae are sprayed to the field; through circulation irrigation, multi-time spraying and alga water recycling, heavy metal in the polluted soil is taken away, the salinity ofthe soil is reduced, the nutritional ingredients of the soil are improved, and the soil fertility is restored; the microalgae are harvested through the method of pond enrichment and flocculation andaeration, the alga charcoal preparation process is utilized through combination, and resource utilization is achieved; and the system achieves automatic control through a sensor, a PC and a control component. The remediation method comprises a heavy metal/saline and alkaline land remediation microalga cultivation system, a water collection system, an intelligent spray irrigation unit, a microalgarecycling system and a microalga resource utilization system.

The invention relates to a novel method for extracting a seaweed intermediate by an enzyme process, which comprises the following steps: sufficiently cleaning and immersing dry Laminaria digitata, adding into an acidic solution, and stirring uniformly to obtain a mixture A; dissolving a composite acidic enzyme in water, and adding into the mixture A to perform primary stirring extraction, thereby obtaining a mixture B; dissolving an inorganic alkaline compound and a composite alkaline enzyme in water, and adding into the mixture B to carry out secondary stirring extraction, thereby obtaining the mixture C; and dissolving a preserving agent in water, adding into the mixture C, and stirring uniformly to obtain the seaweed intermediate. The method for preparing the seaweed intermediate is efficient, quick, mild, comprehensive, safe and harmless. Compared with the traditional acid-alkali extraction technique, the extraction efficiency is enhanced by 50% above, the algal polysaccharides content is enhanced by 50-100%, the alginic acid content is 3.5-4.0, the effect of the seaweed intermediate product is obviously enhanced, and all the effective components in the seaweeds are reserved in the product, thereby implementing complete-effect addition in deed.