This invention relates to the field of
fertilizer production technology, specifically to a segmented
ripening preparation process for low-free-acid, high-water-soluble superphosphate; the process includes the following steps: feeding
phosphate rock
powder into a
ball mill for
grinding to a particle size ≤120 mesh, preparing 93%±0.5% industrial
sulfuric acid; adding
phosphate rock
powder at a
molar ratio of available P2O5 to
sulfuric acid of 1:1.05~1:1.07, adding 0.3%~0.5% (by weight of
phosphate rock
powder) of a modifying agent, and reacting at 65~70℃ for 40~50 minutes. In the later stage of the reaction, low-pressure steam of 0.2 MPa is introduced; staged maturation is carried out, first in a
closed chamber at 55~60℃ for 24 hours, and then in a ventilated chamber at 45~50℃ and a
wind speed of 0.8~1.0 m / s for 48 hours;
granulation and screening are carried out, with the
granulation drum rotating at 14~16 r / min and tilted at an angle of 3°~5°; through the above methods, the problems of high
free acid, low proportion of water-soluble
phosphorus and insufficient production efficiency in traditional processes are solved, and the product quality and production capacity are synergistically improved.