Traditional Chinese medicine gastrointestinal developing agent for B ultrasound and preparation method thereof
A technology of contrast agent and traditional Chinese medicine, used in echo/ultrasonic imaging agents, etc., can solve the problems of strong gastric acid reaction, inability to use, no therapeutic effect, etc., and achieve the effects of simple preparation process, short inspection time, and no allergic reaction.
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[0043] The present invention further provides a method for preparing the above-mentioned traditional Chinese medicine gastrointestinal contrast aid for B-ultrasound, the dosage form of the traditional Chinese medicine contrast aid is granule, which comprises the following steps:
[0044] Step 1: Mix the raw medicinal materials according to the stated ratio, add ethanol with an alcohol concentration of 80% to 90% that is 3 to 5 times that of the mixture, heat to boiling and reflux for 2 to 4 hours, filter, and use percolation to remove Slowly percolate at a speed of 1-2ml per minute, collect the percolation liquid, then concentrate under reduced pressure at a vacuum of 0.06-0.09Mpa to a paste with a relative density of 1.00-1.10 at 50-60°C, spray dry, spray dry The air inlet temperature of the machine is 160-175°C, and the outlet air temperature is 80-85°C, and then crushed into powder to make dry cream powder;
[0045] Step 2: adding 0.3-0.5 times of sucrose powder and 0.2-0.4...
Embodiment 1
[0052] Embodiment 1: Granules
[0053] Take 320g white snail lion shell, 240g sea white stone, 340g phoenix tree, 110g water hyacinth fruit, 140g thorn rose, 180g Tangli branch and leaf, 120g multi-spike stone fruit, 70g green sheep ginseng, 180g cold berry root, 60g Agrimony, Horse tooth seven 70g, Tianshui antsweed 160g, golden thread bag 80g, black root 210g, snake white scorpion 120g, tangut green orchid 70g and yellow violet 60g.
[0054] Its preparation method comprises the following steps:
[0055] Step 1: Mix the raw medicinal materials according to the stated ratio, add ethanol with an alcohol concentration 3 times that of the mixture and 80% ethanol, heat to boiling and reflux for 2 hours, filter, and use percolation method at a rate of 2ml per minute to slowly Percolation, collect the percolation liquid, then concentrate under reduced pressure at 0.09Mpa to a paste with a relative density of 1.10 at 60°C, spray dry, the air inlet temperature of the spray dryer is 1...
Embodiment 2
[0057] Embodiment 2: syrup
[0058] Take 340g of white snail shell, 210g of sea white stone, 320g of phoenix seed, 140g of water hyacinth, 120g of thorn rose, 160g of Tangli branch and leaf, 140g of multi-spike stone fruit, 80g of green sheep ginseng, 160g of cold berry root, 70g of Agrimony, 80g horse tooth seven, 180g tianshui antweed, 60g gold thread bag, 230g black root, 140g snake white scorpion, 60g tangut green blue and 80g chrysanthemum violet.
[0059] Its preparation method comprises the following steps:
[0060] The first step is to press the fruit of chrysanthemum, green sheep ginseng, cold berry root, agrimony, horse tooth seven, Tianshui antweed, golden thread bag, black bark root, snake white scorpion, tangut green orchid and yellow violet Mix the ratios, add ethanol with an alcohol concentration 3 times that of the mixture and be 95% ethanol, heat and reflux for extraction 4 times, and extract for 3 hours each time, combine the extracts, and use a tube centrif...
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