Liquid ammonia modified method of cotton fibriia and yarn

A cotton and linen fiber, liquid ammonia technology, applied in fiber treatment, plant fiber, removal of liquid/gas/vapor by centrifugal force, etc., can solve the problems of long processing time, small batch, long process, etc., and improve the level of bright dyeing , The effect of reducing drying cost and improving softness

Inactive Publication Date: 2009-04-22
上海业安纺织科技有限责任公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in the existing methods, there is no focus on energy conservation and environmental protection.
Mainly reflected in: First, the measures for removing the liquid ammonia existing on the fiber after soaking ammonia are not perfect, so that energy is required to make the liquid ammonia do liquid-gas-liquid cycle recovery, the amount of energy required becomes larger, and the processing time becomes shorter. Long; the second is the current liquid ammonia recycling method, because the generated ammonia contains air, which must be absorbed by water to remove the air, and then the ammonia components are rectified from the ammonia water out, and then condensed into liquid ammonia, the process is long, consumes a lot of energy, and equipment investment is large; third, it is processed in an unsealed container, and the drying and deodorization of fibers and yarns is not thorough, polluting the environment; fourth, the production batch is small and cannot Meet the needs of mass production

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] Liquid ammonia modification method of fiber (taking flax fiber roving before scouring as an example). Wind the flax roving (3Nm) on a special roving bobbin with a winding density of 0.33g / cm 3 , first drying, the drying temperature is 70 ° C, so that the moisture content of the raw material after drying is lower than 6%; then put the roving bobbin into a sealed processing tank, and fix it on a creel that can rotate slowly. Before feeding liquid ammonia, first vacuumize the treatment tank to 0.005Mpa, then fill the ammonia gas to a pressure of 0.3Mpa, then pass liquid ammonia into the treatment tank, control the pressure below 0.5Mpa, and control the rotation speed of the creel to 4r / min, soaking the roving for 180 seconds. Then spin dry, and the roving rotation line speed on creel is more than 30m / s when spin dry. Then dry in a hot ammonia airflow at 60°C. During drying, the pressure in the tank is kept at 0.28-0.32Mpa, and the average ammonia flow rate per kilogram ...

Embodiment 2

[0032] The liquid ammonia modification method of skein (with cotton yarn 60 s / 2 as an example). Wind the cotton yarn on the spinning machine into a form with a length of 1550mm and a weight of four strands of 200g (the weight of a single strand is 50g). The drying temperature is 70°C, so that the moisture content of the raw material after drying is lower than 6%. Then put the skeined yarn into a sarong with holes, and put the sarong into a sealed treatment tank on a slowly rotating creel. Before feeding liquid ammonia, the container is evacuated to 0.005Mpa, then filled with ammonia gas to a pressure of 0.2Mpa, then liquid ammonia is passed into the treatment tank, the pressure is controlled to 0.25Mpa, and the rotation speed of the creel is controlled to 6r / min , soak the skein for 120 seconds. Then spin dry, and the rotary linear speed of skein in the sarong is more than 30m / s when spin dry. Then dry in the hot ammonia airflow below 80°C. During drying, the pressure in t...

Embodiment 3

[0034] Liquid ammonia modification method for bobbins (taking 36Nm hemp yarn as an example). Wind the hemp yarn on the loose winder to form a cone yarn with a winding density of 0.32g / cm 3 The net weight of each bobbin yarn is 1.0kg, and it is firstly dried at a temperature of 70°C so that the moisture content of the raw material after drying is lower than 6%; then the bobbin is fixed in a sarong with holes, and the The sarong is placed on a slowly rotating creel in a sealed treatment tank. Before feeding liquid ammonia, the container is evacuated to 0.004Mpa, then filled with ammonia gas to a pressure of 0.7Mpa, and then liquid ammonia is passed into the treatment tank, the pressure is controlled at 0.8Mpa, and the rotation speed of the creel is controlled at 5r / min , soak for 250 seconds. Then spin dry, and the rotary line speed of bobbin yarn on creel is controlled at 30r / min when spin dry. Then dry it in a hot ammonia airflow at 65°C. During drying, the pressure inside ...

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Abstract

The invention provides a method for modifying cotton and long vegetable fiber or yarn by ammonia liquid, which comprises the following steps: firstly, drying pre-treatment of raw materials; secondly, ammonia leaching of the raw materials in a hermetical treatment tank; thirdly, spin-drying of the raw materials subjected to ammonia leaching when a creel is twirled; fourthly, drying of the raw materials subjected to spin-drying by ammonia flow when the creel rotates slowly; fifthly, flushing of the raw materials which are dried by the ammonia flow by airflow when the creel rotates slowly; and so on. The method keeps the inherent advantages of the cotton, the long vegetable fiber and the yarn, overcomes the defects of the cotton, the long vegetable fiber and the yarn, increases softness, crimp tendency and fluffiness of the cotton, the long vegetable fiber and the yarn, improves the dye-uptake rate, the leveling property and the showy dye level, and further solves the problems of energy conservation, efficiency improvement and environmental protection.

Description

technical field [0001] The invention relates to a method for processing textile raw materials, in particular to a method for modifying cotton and linen fibers and yarns with liquid ammonia. Background technique [0002] Existing cotton, hemp fiber and yarn are a large class of natural textile materials. Under the guidance of today's green, environmental protection and return to nature concepts, it has been paid more and more attention by the market and consumers. However, compared with synthetic fibers, cotton and hemp fibers and yarns are difficult to spin, weave, and dye poorly, and the textiles made of them have defects such as shrinkage and easy wrinkling. Liquid ammonia treatment is an important means to remove the disadvantages while retaining the inherent advantages of cotton and hemp fibers and yarns, making them fibers and yarns with special properties. However, in the existing methods, energy saving and environmental protection are not considered in key aspects. ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M11/61D06B1/04D06B15/10D06M101/04
Inventor 郎金成孙以泽刘运峰
Owner 上海业安纺织科技有限责任公司
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