The application provides a cotton
fiber dyeing method of a polar / non-polar binary non-
aqueous medium system. The method comprises the following steps: S1, placing cotton fabric, a dye, water, an alkali agent and a polar
solvent A in a sealed
dyeing tank and filling CO2 for dye
dissolution to obtain a mixed
system; S2, regulating parameters of the sealed
dyeing tank for dyeing; S3, adding a non-polar
solvent B to the sealed dyeing tank for fixation treatment; and S4, after cooling to
room temperature, taking out the cotton fabric, washing,
drying and completing the dyeing. By introducing a CO2 responsive polar
solvent, the polarity is enhanced when CO2 is filled, so that high-concentration reactive dyes are fully dissolved at low temperature and almost no
hydrolysis occurs, the
dosage form is reduced after CO2 is released, the dyes are uniformly precipitated and quickly adsorbed on the cotton
fiber, so that the high-concentration dyeing build-up is significantly improved, the dye
hydrolysis rate is significantly reduced, the
dye uptake is improved to more than 95%, the medium and CO2 can be recycled, and the efficient, green and low waste
discharge of cotton
fiber deep and thick color dyeing is realized.