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6782 results about "Ammonium sulfate" patented technology

Ammonium sulfate (American English and international scientific usage; ammonium sulphate in British English); (NH₄)₂SO₄, is an inorganic salt with a number of commercial uses. The most common use is as a soil fertilizer. It contains 21% nitrogen and 24% sulfur.

Method for preparing aluminum oxide from aluminiferous material

The invention provides a method for preparing aluminum oxide and other products from aluminiferous materials such as bauxite, high iron bauxite, alunite, kaoline, alumina, fly ash, coal gangue, aluminum ash, nepheline, clay and the like. The method comprises the following steps: (1) crushing, grinding and mixing the aluminiferous materials with ammonium sulfate and then roasting; (2) dissolving the roasted product (clinker aggregate) in water, and filtering to obtain aluminum ammonium sulfate solution and filter residues; (3) carrying out deferrization, aluminum deposition or recrystallization on the aluminium ammonum sulfate solution with ammonia to prepare aluminum oxide, and meanwhile, recycling the ammonium sulfate; (4) preparing silicon dioxide from the filter residues, and taking the remaining residues containing ferrum as the raw material for ironmaking. The method is suitable for treating various aluminiferous materials, has the advantages of simple technical process, simple equipment, no emission of solid, liquid and gas wastes, and no secondary pollution, and realizes the high-added-value green complex utilization of the aluminiferous materials such as bauxite, high ironbauxite, alunite, kaoline, alumina, fly ash, coal gangue, aluminum ash, nepheline, clay and the like.

Process for treating sludge and manufacturing bioorganically-augmented high nitrogen-containing inorganic fertilizer

ActiveUS20080230484A1Reduce logisticsReduces liabilityByproduct vaporizationExcrement fertilisersPhosphateRetention time
The invention describes a new method for treating sludge, which can result in the production of high nitrogen organically-augmented inorganic fertilizer that incorporates municipal sludges or biosolids or organic sludges that can compete with traditional fertilizers such as ammonium phosphate, ammonium sulfate and urea on the commodity fertilizer marketplace. The method takes advantage of the thixotropic property of dewatered biosolids or organic sludge to create a pumpable paste-like material from the biosolids or organic sludge that is then treated with an oxidizer to reduce odorant effects and an acid. This mix is then interacted with concentrated sulfuric and or phosphoric acids and an ammonia source or alternatively a hot or molten melt or salt of ammonium sulfate/phosphate to form a fertilizer mix. The present invention controls the heat, atmospheric pressure and retention time of the fertilizer mix in the reaction vessel. When a fertilizer melt is formed ammoniation is subsequently completed by the specific use of vaporized ammonia. The invention can also be an add-on to commercial production of ammonium salts. The fertilizer produced by the present invention contains more than 8 wt. % nitrogen and preferably 15 wt. % nitrogen. The invention is oriented to be tailored to the biosolids production for individual municipal waste treatment plants in order to keep the fertilizer manufacturing plants of the present invention small with a minimization of logistics and liability.

Technological process for producing high concentration nitric-phosphate fertilizer

ActiveCN101486595AHigh crystallinityGood filter strengthHigh concentrationDihydrate Calcium Sulfate
The invention discloses a technique method for producing high-concentration nitric phosphate, which comprises the following steps of: adding nitric acid into phosphorus ore for acidolysis, depositing and separating acid non-soluble substance, freezing and crystallizing calcium nitrate, filtering the calcium nitrate, neutralizing the mother liquid, vaporization, pelleting and drying. The invention is characterized in that: a step of thoroughly removing the calcium of the mother liquid is arranged between the steps of filtering the calcium nitrate, and neutralizing the mother liquid. The steps comprise the following steps of: I) thoroughly removing the calcium of the mother liquid and adding sulfuric acid or ammonium sulfate; the calcium ions and the sulfate ions in the mother liquid generate dihydrate calcium sulfate crystal; II) the grading processing of reaction slurry: employing a grading device to carry out grading processing to the reaction slurry; returning the reaction slurry provided with small grain calcium sulfate to the mother liquid for thoroughly removing the calcium, and feeding the reaction slurry provided with large grain calcium sulfate to the calcium sulfate for filtering; and III) filtering and washing the filtering reaction slurry of calcium sulfate by a filter, feeding the primary filtrate and the primary lavage fluid into the working procedure of neutralizing, and returning the secondary lavage fluid to the filter. The invention has the advantage of using middle-low quality phosphorite to prepare the high-concentration nitric phosphate.

Special organic-inorganic composite biological pesticide-fertilizer for flowers and preparation method thereof

The invention provides a special organic-inorganic composite biological pesticide-fertilizer for flowers. The special organic-inorganic composite biological pesticide-fertilizer for flowers comprises the following raw materials in parts by weight: 80-90 parts of municipal sludge, 10-20 parts of fruit peel, 10-20 parts of fallen leaves, 10-15 parts of poultry manure, 10-14 parts of bagasse, 20-30 parts of iron ore slag, 10-12 parts of animal feathers, 10-15 parts of tree ash, 10-15 parts of monoammonium phosphate, 20-25 parts of urea, 10-12 parts of ammonia sulfate, 8-10 parts of ammonium hydrogen carbonate, 8-10 parts of potassium chloride, 5-7 parts of carboxymethyl chitosan, 20-30 parts of modified bentonite, 5-8 parts of lignite, 2-4 parts of black dye tree, 9-11 parts of celastrus angulatus, 9-11 parts of common carpesium fruit, 9-11 parts of radix sophorae flavescentis, 4-6 parts of lilac daphne flower bud, 3-5 parts of coptis root, 10-12 parts of powder of root of stellera chamaejasme, 2-4 parts of vegetable oil, 1-3 parts of zinc sulfate, 3-4 parts of ferrous sulfate, 0.8-1.2 parts of borax, 20-26 parts of potassium fulvate and 0.3-0.4 part of EM (effective microorganism) strain. The pesticide-fertilizer disclosed by the invention has the advantages of scientific ratio of nitrogen, phosphorus and potassium, easiness in absorption by crops, obvious yield-increasing benefit and the like. By applying the pesticide-fertilizer, the nutrient absorption of plants can be balanced, the quality of flowers can be effectively improved, plants are green in leaves and bright in flower, and the flowering phase is also prolonged.
Owner:东至县神山化肥有限责任公司 +1

Ammonia process flue gas treatment method for acidic tail gas and device

ActiveCN103223292AIncreased self-concentrationGood desulfurization absorptionDispersed particle separationAmmonium sulfatesEnvironmental resistanceAmmonia storage
The invention relates to an ammonia process flue gas treatment method for acidic tail gas. The method includes the steps of: 1) controlling the sulfur dioxide concentration of tail gas entering an absorption tower at a level of less than or equal to 30000mg/Nm<3>; 2) arranging process water in an absorption tower entrance flue or in the absorption tower or cooperating with a ammonium sulphate solution to perform spray cooling; 3) disposing an oxidation section in the absorption tower, setting an oxidation distributor at the oxidation section to achieve oxidation of a desulfurized absorption liquid; 4) arranging an absorption section in the absorption tower, utilizing an absorption liquid distributor in the absorption section to realize desulfurization spray absorption by an ammonia-containing absorption liquid, which is fed through an ammonia storage groove; 5) arranging a water washing layer at an absorption section upper part in the absorption tower, washing the absorption liquid in the tail gas by the water washing layer and reducing the absorption liquid escape; and 6) setting a demister at the upper part of the water washing layer in the absorption tower to control the mist drop content in the purified tail gas. Employment of the Claus sulfur recovery and ammonia process desulfurization integrated desulfurization technology in the coal chemical industry can reduce the investment cost of after-treatment, the process can be simpler, and factory environmental protection treatment can form an intensive advantage.

Preparation method of high-purity vanadium pentoxide

The invention discloses a preparation method of high-purity vanadium pentoxide. The preparation method comprises the following steps of: returning and dissolving coarse vanadium in aqueous alkali, and filtering the solution to remove metal impurities, which are subjected to precipitation reaction with the aqueous alkali, in the coarse vanadium, thus obtaining a primary returned solution; slowly pouring the primary returned solution into a sulfuric acid solution, adjusting the pH value of the solution to be 1.0-2.0 to obtain a liquid-solid mixture, and performing solid-liquid separation on the liquid-solid mixture; filtering and washing precipitates obtained from the solid-liquid separation of the mixture, and returning and dissolving the mixture into the aqueous alkali, thus obtaining a secondary returned solution; adding ammonium sulfate into the secondary returned solution for precipitating vanadium, and filtering the solution to obtain ammonium metavanadate; and processing the ammonium metavanadate to obtain the high-purity vanadium pentoxide. The preparation method adopting multiple stages of returned dissolving can be used for effectively removing the metal canon impurities of the vanadium pentoxide, and further obtaining the high-purity vanadium pentoxide with the metal canon impurity contents of less than 0.001% and the vanadium pentoxide content of 99.99%.

Photochemical advanced oxygenation-based simultaneous desulfuration and denitration system

The invention discloses a photochemical advanced oxygenation-based simultaneous desulfuration and denitration system. The system is provided with a burning and exhausting system consisting of a burner, an electrostatic dust collector, a heat exchanger, a spray tower, a liquid adding tower and a chimney, wherein fume generated by the burner enters the electrostatic dust collector, fume particles are removed from the fume by the electrostatic dust collector, the fume enters the heat exchanger and is cooled by the heat exchanger, and then the fume enters the spray tower; an UV light tube is arranged in the spray tower; hydrogen peroxide solution from the liquid adding tower is pumped by a circulating pump, sprayed into the spray tower through an atomizing nozzle and is activated by ultraviolet light to decompose hydrogen peroxide and then generate hydroxyl radicals (.OH) with strong oxidizing property; after being contacted with the fume in the spray tower, the hydroxyl radicals undergoes a gas-liquid absorption reaction with the fume to oxidize and remove NOx and SO2 in the fume; the fume, after being absorbed and washed, enters the chimney from the top of the spray tower and is exhausted; and sulfuric acid solution and salpeter solution generated in the spray tower are pumped into the separating column by the circulating pump and are reacted with added ammonia water to generate agricultural fertilizers including ammonium sulfate and ammonium nitrate.

Desulphurization method for acid gas

The invention provides a desulphurization method for acid gas, which comprises the following steps: firstly, carrying out heat combustion reaction on the acid gas and fuel in a combustion chamber; secondly, carrying out catalytic reduction reaction on the obtained combustion product; thirdly, combusting tail gas obtained by the catalytic reduction reaction; and fourthly, carrying out ammonia elution on sulfur dioxide in gas obtained after combustion to obtain ammonium sulphate. The desulphurization combined process for the acid gas has no strict requirement on the Claus combustion, does not need multistage Claus reaction, and even does not control the Claus reaction strictly; and wastewater subjected to ammonia washing in the acid gas containing ammonia is not discharged to a sewage treatment center of a factory, and a fussy device is not needed to add for ammonium refining and recovery. The method can balance the ammonia and the Clause reaction according to the yield of the ammonium sulphate, and does not have sewage discharge; heat required by the process can be balanced through by-product steam, so that the method greatly saves the investment and operation cost, and has short flow and simple operation; and the gas emission can be far lower than the national emission standard.

Disease-resistant compound biofertilizer special for corn and preparation method thereof

ActiveCN104003817AImprove the micro-ecological environmentPromote growthFertilizer mixturesDiseasePhosphate
The invention belongs to the technical field of fertilizer, particularly relates to disease-resistant compound biofertilizer special for corn and further relates to a preparation method of the disease-resistant compound biofertilizer special for the corn. The disease-resistant compound biofertilizer special for the corn comprises carbamide, compound microbial agents, bran, chitosan, furfural residues, ammonium sulfate, potassium sulfate, monoammonium phosphate, rape seed cakes, manure, humic acid, sesame seed cakes, microelements, calcium superphosphate and plant ash. The nutrient elements of the disease-resistant compound biofertilizer special for the corn are balanced, microelement compositions are abundant, soil productivity and soil fertility can be improved effectively, addition of compound microbial agents can remarkably restrain main corn diseases occurring universally, the disease-resistant compound biofertilizer special for the corn is long in fertilizer efficiency, corn yield can be improved by 25 to 30 percent effectively, the corn diseases can be prevented and cured effectively, soil can be improved effectively through long-term utilization of the disease-resistant compound biofertilizer, and the disease-resistant compound biofertilizer special for the corn can play a role in the whole growth period of the corn.

Method for innocent treatment and comprehensive utilization of manganese slag

InactiveCN101691633AHigh recovery rateThe comprehensive effect of harmless treatment is goodProcess efficiency improvementManganese sulphateSlag
The invention provides a method for innocent-treatment and comprehensive utilization of manganese slag, which comprises the steps of: (1) washing and pressure-filtering the manganese slag, and separating manganese sulphate from ammonium sulphate which cause environmental pollution from leaching residue; (2) performing a reaction of slag washing water and a precipitator, ensuring that 5 to 10 percent of excessive precipitator is added, the reaction time is between 0.5 and 3 hours and the reaction temperature is between 30 and 100 DEG C, converting manganese ions in the slag washing water into manganese hydrate or manganese carbonate to precipitate the manganese ions, and then performing solid-liquid separation to realize the recovery of manganese; and (3) reacting a solution obtained by recovering the manganese and lime milk, wherein the reaction temperature is between 60 and 100 DEG C, reaction time is between 0.5 and 3 hours and reaction pressure is between 0 and 200mmHg, ensuring that the ammonium sulfate is converted into ammonia and calcium sulphate, absorbing the ammonia into ammonia water through an absorption device, filtering a solid-liquid mixture, separating out solid calcium sulphate, and recycling a filtrate in the slag washing process in the step (1). The method has the advantages of less equipment investment, low energy consumption and production cost, high recovery rate of valuable compositions and good comprehensive effect of innocent treatment of the manganese slag.

Process for removing smoke dust by wet ammonia flue gas desulphurization and device thereof

The invention provides a process for removing smoke dust by wet ammonia flue gas desulphurization. The smoke dust removing process comprises two processes, namely, smoke dust removal and ammonium sulfate post-treatment, wherein the ammonium sulfate post-treatment process is that desulfurated ammonium sulfate slurry which is generated by a desulphurization system is delivered to a cyclone separator, a lower overflow vent of the cyclone separator is connected with the inlet of a centrifugal machine, and a solid outlet of the centrifugal machine is connected with a drier; and the smoke dust removing process is that liquid of an upper overflow vent of the cyclone separator and a liquid outlet of the centrifugal machine are connected with filtering separation equipment, and liquid enters a recirculating tank or a liquid tank for next circulation after dust in the liquid is removed by the filtering separation equipment. A device for removing dust by wet ammonia desulphurization comprises the cyclone separator, a centrifugal machine, the drier, the filtering separation equipment, an ash settling pond, a circulating tank or the liquid tank with a stirring device, is used for combining theammonium sulfate post-treatment and dust removal, and has simple process and system, small occupied area and low operation cost.

Rice fertilizer capable of improving resistance, quality and yield of rice

The invention relates to rice fertilizer capable of improving the resistance, quality and yield of rice. The rice fertilizer consists of the following raw materials in percentage by weight: 20.0 to 27.0 percent of urea, 7.0 to 20.0 percent of ammonium sulfate, 5.0 to 13.0 percent of monoammonium phosphate, 9.8 to 17.5 percent of potassium chloride, 10.0 to 18.5 percent of calcium superphosphate, 3.0 to 6.0 percent of calcium-magnesium phosphate, 2.0 to 8.0 percent of soluble silicon, 0.1 to 0.9 percent of amino acid, 5.0 to 30.0 percent of humic acid, 0.5 to 6.0 percent of other trace elements (zinc, manganese, boron, ferrum, copper, molybdenum, selenium and the like), 0.2 to 0.5 percent of activating agent and less than or equal to 2.5 percent of water. The rice fertilizer has the advantages of comprehensively providing the nutrient required by growth of rice, improving the yield and the quality of rice, activating the nutrient of soil, enhancing the capacity of absorbing nutrient by crops, improving a soil structure, enhancing soil fertility, promoting development, and improving the resistance of the crops (disease resistance, pest resistance, drought resistance, flooding resistance, cold resistance, saline-alkaline resistance, lodging resistance and the like).

Method for recovering lead oxide by waste lead-acid storage battery

A method for recovering lead oxide by a waste lead-acid storage battery is disclosed. The waste lead-acid storage battery is crushed together with lead slime subsequent to acid cleaning, a grid plate and a filler comprising the lead slime are obtained by screening, the grid plate is fused-cast to an alloy ingot, the filler and the lead slime are ball-milled, and fine stuff is added with saturated oxalic acid solution for reaction at 25-65 DEG C and then for filtering and depositing; the deposition is then treated by excessive 30% nitric acid at the temperature of 40-45 DEG C for subsequent filtration and deposition, and the deposition is reacted with 4wt% sal volatile at the temperature of 25-65 DEG C for subsequent filtration and deposition; the deposition is added into recovered HNO3 to be dissolved at the temperature 40-45 DEG C until no bubble is generated, the filtered filtrate is added with 25% ammonia for reaction, filtration, washing and deposition to be neutral, and the lead oxide is obtained by drying and roasting. Recoverable nitramine and ammonium sulfate are recycled in all the filtrates in the technologies; thereby discharging no waste liquid. The utilization rate of raw material is 90.1-92.1%, the yield is 95.0-96.7%, and the content of PbO is 98.0-98.9%.

Method for extracting aluminium oxide from coal ash

The invention provides a method to extract aluminum oxide from a fly ash, and relates to a technological method which is to extract aluminum oxide from the fly ash and comprehensively utilize the residue after extracting aluminum oxide. The invention is characterized in the method which is as follows: ammonium sulfate is mixed into the fly ash to sintering, and the solid is dissolved to obtain the solution containing aluminum-ammonium sulfate; the solution is crystallized to form solid aluminium-ammonium sulfate; solid aluminium-ammonium sulfate reacts with ammonia gas to obtain aluminium hydroxide and ammonium sulfate, and aluminium hydroxide and ammonium sulfate are washed and filtrated to obtain solid aluminium hydroxide; solid aluminium hydroxide is calcined to obtain aluminum oxide; ammonium sulfate can be circularly used after being evaporated in the liquid phase. The ammonium sulfate which is used by the method of the invention is weak acidic, the corrosiveness on the equipment is small, and the ammonium sulfate can be used circularly. The whole process is easy to industrial application. The requirement of the corrosion resistance on the equipment is low. The amount of the residue is small which is beneficial to the comprehensive utilization of the residue after extracting the aluminum oxide.
Owner:河南华慧有色工程设计有限公司 +1
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