The application discloses a heating transmission device suitable for in-situ detection of ultrahigh-temperature
pyrolysis reaction, comprising a heating
pipe and an adjusting
assembly; a sample outlet end of the heating
pipe is connectable to a detection device; the heating
pipe is divided into a low-temperature zone, a high-temperature zone and an annealing zone; a first water-cooled
electrode is arranged outside the low-temperature zone; and a second water-cooled
electrode is arranged outside the annealing zone; the adjusting
assembly comprises a guide rail and a sliding block; and the sliding block is connected with the first water-cooled
electrode or not. The application forms a variable-
diameter and variable-temperature zone through combination design of the heating pipe and the water-cooled electrode, guarantees contact between the heating pipe and the protective electrode, builds a relatively slow and uniform
temperature gradient in the annealing zone, guarantees generation and dispersion of product molecules and improves transmission efficiency of
macromolecular compounds. The application is convenient to connect with a
mass spectrometer, can realize in-situ analysis of ultrahigh-temperature
pyrolysis reaction and solves the problem that macromolecular products such as polycyclic aromatic hydrocarbons, fullerenes and the like cannot be detected in-situ due to aggregation caused by intermolecular forces in the
pyrolysis reaction.