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4960 results about "Ice water" patented technology

Gas pipeline drag reduction agent and preparing method thereof

The invention relates to a gas line drag reduction agent and a preparation method thereof, relating to the technical field of the composite of high-molecular compound and piping systems. The drag reduction agent consists of carbon bisulfide, hydrazine hydrate and long chain acid, the mol ratio of which is 1.8:1:1 to 2.2:1:1. The preparation method comprises the following steps: step one, CS2 is taken according to proportional quantity, dripped into the mixed liquor of the hydrazine hydrate and water with proportional quantity under agitation, reflowed for certain time in the temperature range of 90 to 95 DEG C, then cooled for 30 to 60 minutes in ice water bath and pumped and filtered, the mother liquor continues to react for two times, products of the third time are merged, washed by using ethanol and ether sequentially, and recrystallized by using boiling water so as to obtain symmetrical diaminothiourea clear crystal; and step two, symmetrical diaminothiourea with proportional quantity and the long chain acid with proportional quantity are dissolved in a pyridine solvent with nitrogen protection, reflowed at the temperature of 140 to 220 DEG C by adopting a temperature programming method, and react for 3 to 4 hours, then the mixture is cooled to the room temperature and recrystallizated by using the ethanol of 95 percent to obtain the brown product.
Owner:PIPECHINA SOUTH CHINA CO

Process for producing absorbent charcoal loading titanium dioxide photocatalyst

The invention relates to a preparation method of activated carbon supported titanium dioxide photocatalyst, belonging to the preparation technical field of titanium dioxide photocatalyst, comprising a plurality of steps as followings: pretreating, washing and drying the activated carbon; at the condition of ice-water bath, adding meta-titanic acid and ammonia according to a molar ratio of 1:2 into 20 to 40 milliliter hydrogen peroxide with a concentration of 30%, and agitating for 50 to 70 minutes to obtain a yellowish green sol; then adding the pretreated activated carbon into the yellowish green sol and agitating for 3 to 5 hours, filtering the activated carbon after standing for 12 to 24 hours, then calcining with the protection of inert gas to obtain the activated carbon supported titanium dioxide photocatalyst. The weight ratio of the pretreated activated carbon and the meta-titanic acid is 1:1 to 3:1. The preparation method has the advantages of simple technology, cheap raw material, mild preparation conditions, easy operation, granular shape, good organic pollutant degradation effect, easy separation, regeneration and long service life of the supported photocatalyst prepared by the preparation method, nonuse of organic solvent, non-pollution in the whole production process, accordance with the requirement of sustainable development and environment-friendly integrated technology.
Owner:TONGJI UNIV

Self-adhesive long-acting slow-release essential oil microcapsule and preparation method and application thereof

The invention discloses a self-adhesive long-acting slow-release essential oil microcapsule and a preparation method and an application thereof. The method comprises the following steps of: uniformly mixing essential oil, a reaction monomer, an auxiliary emulsifying agent, oil-soluble initiator and a newly-added oil-soluble crosslinking agent to obtain an essential oil/monomer mixed solution; adding an aqueous solution of an emulsifying agent; pre-emulsifying in a shearing and stirring state for 10-20 minutes; performing ultrasonic dispersion in an ice-water bath to obtain a fine emulsified liquid; and performing a polymerization reaction on the fine emulsified liquid in a nitrogen atmosphere in a shearing and stirring state at the temperature of 65-70 DEG C for 3-6 hours, and cooling after finishing reaction to obtain self-adhesive long-acting slow-release essential oil microcapsule rubber latex. The preparation method has the advantages of ready availability of raw materials, simple process, high good controllability over the morphological structure of the microcapsule, no relevance to organic solvents and suitability for industrial production; and the prepared microcapsule has high structural strength, a good slow release effect, and high self-adhesive properties on substrates such as fibers and the like. The invention further discloses a self-adhesive long-acting slow-release essential oil microcapsule and an application thereof.
Owner:HANGZHOU WENSLI SILK DIGITAL PRINTING CO LTD +1

Preparation method for taste base peptide for steamed savory flavoring

The invention discloses a preparation method for taste base peptide for steamed savory flavoring, and belongs to the field of food additives. The method comprises the following steps: performing enzymolysis on defatty grouts to prepare raw material peptide; performing maillard reaction on the raw material peptide and sugar to prepare the taste base peptide; taking the raw material peptide and reducing sugar as raw materials, common salt and / or cysteine as accessories, and 6 to 16g / 100ml raw material peptide, 0.5 to 4.5g / 100ml reducing sugar, 2 to 10g / 100ml common salt, and 1 to 5g / 100ml cysteine as ingredients of the maillard reaction, controlling the temperature to 80 to 130 DEG C, and reacting for 0.5 to 3.5 hours; and cooling a reaction solution by ice water, and spray drying the reaction solution to obtain the taste base peptide. The taste base peptide is a light yellow powder base, and the content of taste potentiating peptide with 1,000-5,000 Da is as high as 20 to 30 percent; compared with a product prepared by the conventional method, the content of amino acid with bitterness of a product prepared by the method is decreased by 10 to 60 percent, and the browning rate is decreased by 40 to 80 percent; and the taste base peptide can be taken as an additive, applied to the steamed savory flavoring, and effectively overcomes the disadvantages of dark color, strong and pungent top note, inadequate mouthfeel, and the like of national savory flavoring products.
Owner:JIANGNAN UNIV

Preparation method for paraffin microcapsule phase-change material modified by graphene oxide

The invention discloses a preparation method for a paraffin microcapsule phase-change material modified by graphene oxide. A technical scheme is that the preparation method comprises the following steps: adding concentrated acid and a strong oxidant in low-temperature ice-water bath to oxidize graphite; successively adding deionized water, hydrogen peroxide and hydrochloric acid, carrying out vacuum filtration, drying and grinding to obtain graphene oxide, adding the graphene oxide into the deionized water to prepare the graphene oxide liquor; adding paraffin, a non-ionic emulsifier and an ionic emulsifier into a stirring kettle, heating and adding graphite to stir to obtain paraffin emulsion; and adding an initiator into the paraffin emulsion to dissolve and dropwise adding monomers, carrying out vacuum filtration after the dropwise adding, carrying out petroleum ether washing and water washing, drying in vacuum and crushing to obtain paraffin microcapsule powder. The preparation method has the beneficial effect that the thermal stability, and the thermal conductivity of the paraffin microcapsule phase-change material are improved by virtue of reaction of multiple oxygen-containing groups on the graphite oxide and the polymer; and moreover, the paraffin microcapsule phase-change material is simple to prepare, environmentally friendly, and has market prospect in the fields such as building energy conservation, thermal insulation products and floor heating.
Owner:江苏节霸新能源材料有限公司

Method for processing frozen minced fillets of java tilapia

The invention relates to the technical field of foods, in particular to a method for processing the frozen minced fillets of java tilapia. The method comprises the following steps: the fish head, the fish scales and the viscera of java tilapia are removed by preprocessing, the java tilapia is washed cleanly and made into minced fish, then the minced fish is dewatered and finely filtered after ice water with the weight of 2-3 times of the weight of the minced fish and 0.15-0.2% of NaCl solution are sequentially used for rinsing the minced fish fully, a compound antifreeze with the weight of 7-9% of the weight of the minced fish is added, and minced fillets are obtained by fully mixing evenly, subpackaged at the temperature of -40 DEG C to -80 DEG C for quick freezing and put for freezing preservation at -18 DEG C; the moisture content of the minced fillets is smaller than 79%, and the gel strength and the folding resistance degree are used as indexes for judging the quality of the minced fillets. In the frozen minced fillets made and obtained according to the method, the gel strength of the minced fillets before freezing storage exceeds 800 (g.cm) by the detection of the gel strength and the folding resistance degree, the gel strength of the minced fillets after the freezing storage for 2 months still reaches more than 600 (g.cm), and the folding resistance degree reaches an AA level. The quality of the frozen minced fillets is equivalent to that of the SA level minced fillets of marine products, such as nemipterus virgatus, red sea bream and the like.
Owner:GUANGDONG OCEAN UNIVERSITY

Preparation method of highly pure quartz sands

The invention discloses a preparation method of highly pure quartz sands. The method comprises the following steps: 1, roughing: cleaning a raw material, and crushing the cleaned raw material; 2, carrying out calcining and water quenching: calcining the crushed raw material, taking out particles, and quenching the particles in an ice-water mixture; 3, carrying out electric separation and magnetic separation: milling the quenched particles, carrying out electric separation and magnetic separation twice, and carrying out pulse magnetic field treatment; 4, pickling: immersing a material obtained in step 3 in a hydrochloric acid solution, filtering the immersed material, dialyzing the obtained first filtrate to recover hydrochloric acid, preparing a first mixed acid by using the recovered hydrochloric acid and a sulfuric acid solution, immersing quartz sands in the first mixed acid, filtering the immersed quartz sands, dialyzing the obtained second filtrate to obtain recovered mixed acid, preparing a second mixed acid by using the recovered mixed acid and a nitric acid solution, immersing the quartz sands in the second mixed acid, adding the immersed quartz sands to a sodium carbonate solution, and flushing the quartz ands; 5, floating the flushed quartz sands; and 6, drying the floated quartz sands. The preparation method allows highly pure quartz sands with the SiO2 content to be not lower than 99.995% to be produced, and takes a greatly lower acid amount than traditional methods.
Owner:江苏凯达石英股份有限公司
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