The invention belongs to the technical field of
manganese slag treatment, and provides a method for preparing heavy
manganese carbonate from
manganese slag washing
water based on a
microreactor. The method comprises the following steps: mixing manganese
slag washing water and an additive, and carrying out
solid-liquid separation to obtain filter residues and filtrate; and mixing the filtrate and the alkali liquor to obtain a manganese
ion solution, and respectively introducing the manganese
ion solution and
carbon dioxide mixed gas into the
microreactor for reaction to obtain the heavy manganese
carbonate. The manganese slag washing water and the
carbon dioxide react in the
microreactor, and the pH value of the manganese
ion solution, the flow of the manganese ion solution and the
carbon dioxide, the
reaction temperature, the reaction pressure and the reaction time are controlled, so that the yield of manganese in the obtained heavy manganese
carbonate is high, the purity is high, and the manganese content in the
effluent filtrate is low; the obtained heavy manganese carbonate can be directly used as a
raw material for electrolytic manganese
metal, and the purposes of
effective treatment of manganese residue washing water and comprehensive recycling of resources under mild conditions are achieved.