63results about How to "No temperature gradient" patented technology

Belonging to the technical field of molybdenum metallurgy, the invention relates to a method for microwave roasting of molybdenite concentrate to produce high-purity molybdenum oxide. The method includes: firstly conducting crushing and ball milling on molybdenite concentrate, then spreading the crushed molybdenite concentrate to a thickness of 1-4cm, and placing the product in a microwave cavity; turning on a microwave output switch, blowing in compressed air, regulating the microwave output power, and carrying out pre-oxidation on the crushed molybdenite concentrate; heating the pre-oxidized molybdenite concentrate to a sublimation temperature and performing thermal insulation for 30-60min, in the process, letting the molybdenum trioxide steam generated by oxidizing roasting overflow through a microwave reactor top, performing water-cooling and then conducting collection by a bag dust collector, thus obtaining high-purity molybdenum trioxide reaching the nonferrous metal industry grade 2 standard. The method provided by the invention has the advantages of short technological process, low energy consumption, and high product purity, etc.

The invention discloses a preparation method of a SnS2/SnO2 lithium ion battery anode material in hollow-sphere structure. The method includes: 1) adding SnCl4.5H2O in a mixed liquid of deionized water and anhydrous ethanol to fully dissolve the component for forming a solution A, and dissolving NaOH in the solution A to prepare a solution B; 2) under stirring, adding urea to the solution B and continuously stirring the solution to prepare a uniform mixed solution C, and performing a homogeneous hydrothermal reaction on the mixed solution C; 3) after the reaction is finished, washing and drying a product to obtain a SnO2 precursor; 4) heating the SnO2 precursor to burning to prepare SnO2 powder; 5) dispersing the SnO2 powder in ethanol with stirring to prepare a uniform mixed suspension D;6) adding SnCl4.5H2O and TAA to the suspension D with stirring until the components are completely dissolved to obtain a homogenous suspension E; 7) performing a microwave thermal reaction on the suspension E, when the reaction is finished, moving-out and washing and drying the product to prepare the SnS2/SnO2 lithium ion battery anode material in hollow-sphere structure.

The invention provides a hydroxy modification method for a low-pressure microwave radiation carbon nanometer tube, it relates to the hydroxy modification method of the carbon nanometer tube and solves the problems of the existing modification technology on nanometer tube that the technical process is complex, the reaction time is long, and the energy consumption and the cost are high. The modification method includes the steps of: 1. soaking carbon nanometer tube into alkali solution, then heat by microwave under low pressure, and remove the upper layer of alkali solution after the cooling and precipitation to obtain the precipitate; 2. cleaning and dry the precipitate to obtain the hydroxy-modified carbon nanometer tube. The invention greatly shortens the reaction time and has the advantages of simple technique, low energy consumption and low cost.

The invention relates to the field of methanol-to-olefin catalysts, discloses a high-silicon ZSM-5 molecular sieve and a preparation method and application thereof, in particular to a preparation method of the high-silicon ZSM-5 molecular sieve. The preparation method comprises the following steps: mixing a solid silicon source, an aluminum source, a ZSM-5 molecular sieve seed crystal, a template, an alkali, urea and water uniformly in sequence, and carrying out aging and hydro-thermal synthesis crystallization, wherein urea is added in the stage of uniformly mixing the raw materials, the liquid silicon source is SiO2, the aluminum source is Al2O3, and the mixing ratio of the raw materials meets that the molar ratio of the solid silicon source, the aluminum source, the template, the alkali, the urea to the water is 1: (0.001 to 0.01): (0.025 to 0.25): (0.02 to 0.2): (0.3 to 4): (2 to 50), and the weight ratio of the ZSM-5 molecular sieve seed crystal to SiO2 in the solid silicon source is (1 to 10): 100. The invention also relates to the high-silicon ZSM-5 molecular sieve prepared by the invention and application thereof. When the prepared flaky high-silicon ZSM-5 molecular sieve is used for reactions for catalyzing methanol to propylene and/or butane, the selectivity of C3 and/or C4 olefin products is improved.

The invention discloses a convenient-to-integrate device for achieving a PCR (polymerase chain reaction) and an operating method. The device comprises a temperature control module, a semiconductor cooler module, a heat conduction module, a sample injection module, a power module and a reaction pipeline module, wherein the temperature control module is used for outputting two channels of control signals according to the set temperature parameters to achieve connection or disconnection of forward and reverse currents of a semiconductor cooler; one side of the semiconductor cooler clings to a heat radiating block and the other side of the semiconductor cooler clings to the heat conduction module; and the reaction pipeline module is embedded in the heat conduction module. During experiments, the sample injection module sucks reaction liquid into a reaction pipeline to reach the heat conduction module, and valves at the two ends are closed to complete sample injection and sealing; the temperature control module is started to heat the heat conduction module when the forward current of the semiconductor cooler is connected and to refrigerate the heat conduction module when the reverse current of the semiconductor cooler is connected; and temperature control of the reaction pipeline is achieved through variation of the temperature of the heat conduction module and the PCR is finally achieved in the reaction pipeline.

The invention discloses a method for producing triuranium octoxide by calcining ammonium uranyl tricarbonate with microwaves, which comprises the following steps: putting ammonium uranyl tricarbonate into a microwave reactor, turning on a microwave heating switch, adjusting the microwave output power to 5-60kW, heating the materials to 400-700 DEG C from room temperature at the speed of 20-100 DEG C/minute, preserving heat for 5-30 minutes, and then naturally cooling to the room temperature to acquire a triuranium octoxide product. The production method has low energy consumption as well as uniform product ingredients and granularity, and the calcining time in the whole technical process is only one third of a conventional method.

The present invention discloses device and method of controlling optical cavity length of annular laser. The device consists of mainly a heat insulated container, a heat insulted elastic diaphragm and a piezoelectric ceramic chip. The heat insulted elastic diaphragm is fixed onto the heat insulated container, and the piezoelectric ceramic chip has its two ends connected separately with the heat insulted elastic diaphragm and the heat insulated container. The method includes connected the device with annular laser, filling the capillary of the annular laser with dry air, altering the voltage applied onto the piezoelectric ceramic chip to change the refractive index of dry air, to change the compensation amount of the optical cavity length of annular laser for being near to the variance in the optical cavity length of annular laser caused by outer environment change, and to realize the control on the optical cavity length of annular laser. The present invention has the advantages of fast response, high sensitivity, low power consumption, etc.

The invention provides a preparation method of manganese oxide yttrium semiconductor photocatalytic powder. The method comprises dissolving yttrium nitrate, potassium permanganate and manganese nitrate into deionized water in accordance with a Y/Mn mole ratio of 1 : 1.5 and a Mn<7+> : Mn<2+> mole ratio of 1 : 4; adding sodium hydroxide into the solution in drops, adjusting a pH value to 8 to 14 and forming a uniform precursor solution; pouring the precursor solution into a hydrothermal reactor and sealing; putting into a microwave digestion system for microwave hydrothermal synthesis, cooling to room temperature, washing the product for several times with the deionized water and absolute ethyl alcohol, and then calcining under 1100 DEG C. By using a microwave hydrothermal method in addition to a solid-phase method, the preparation method can effectively reduce reaction temperature and improve powder activity. The manganese oxide yttrium powder prepared by the method has a narrow optical band gap (Eg=1.55 eV), and meanwhile, has an absorption wavelength of more than 800 nm, thereby being of great significance for exploring new types of semiconductor photocatalytic materials capable of responding to visible light.

The invention discloses a quasi-temperature isostatic pressing forming method and a die. An outer die comprises a female die and male dies arranged at the two ends of the female die, the female die is of a transparent cylinder structure, exhaust holes are evenly and symmetrically formed in the wall face of the female die, and a cavity defined by the female die and the male dies is filled with an inner die; a first cavity used for containing a sample is formed in the inner die, the first cavity is in a cuboid shape, the inner die comprises a plurality of inner die blocks, the inner die blocks comprise contact inner die blocks and supporting inner die blocks, and the orthographic projection range from each face of the first cavity to the inner wall face of the outer die is provided with the contact inner die blocks used for making contact with the surface of the sample; and the sizes of the contact inner die blocks corresponding to the two opposite faces in the first cavity are the same, and the area, outside the contact inner die blocks, of an inner cavity of the outer die is filled with the supporting inner die blocks. According to the quasi-temperature isostatic pressing forming method and the die, through reasonable arrangement of the component structure, uniform and compact forming of a green body is achieved, the quasi-temperature isostatic pressing forming method and the die are suitable for the conditions with and without gas product discharging in the forming process, and the application range is wide.

A reference volume for use with pressure change flow rate measurement apparatus has an internal structure comprising elements with cross section and length comparable to the cross section and length of adjacent interstitial fluid regions. The reference volume may have one or more heat conduction elements exterior to and in good thermal contact with a corrosion resistant material that defines the internal fluid holding region.

The invention relates to a tunnel-type constant-temperature heating furnace. According to the tunnel-type constant-temperature heating furnace, a constant-temperature tunnel is formed by an upper heating plate, a lower heating plate and two side plates connected with the upper heating plate and the lower heating plate, and the front end and the rear end of the constant-temperature tunnel are provided with openings. Two gates are separately mounted at the openings in the front end and the rear end of the constant-temperature tunnel. Two wheels are located on the front portion and the rear portion of the constant-temperature tunnel correspondingly. A conveying belt penetrates through the constant-temperature tunnel and surrounds the two wheels. The portion, located in the constant-temperature tunnel, of the conveying belt is attached to the lower heating plate. The temperature in the tunnel is uniform, and a temperature gradient hardly exists; heat convection is avoided, and air can be isolated to prevent material contamination; heat conduction is rapid, and the heat efficiency is high; continuous material work is achieved, and a reliable guarantee is provided for an automatic production line; and the tunnel-type constant-temperature heating furnace can be widely applied to the food industry, the medical industry, the fine chemical engineering industry and the electronic industryand particularly to automatic production lines for liquid crystal screen hydrosol OCR and has irreplaceable functions for pre-curing hydrosol on adhesive-coated screens.

The invention discloses a reaction apparatus of a microwave pyrolysis biomass. The reaction apparatus comprises a microwave pyrolysis unit, the microwave pyrolysis unit comprises a microwave thermal decomposition furnace, and at least a feed inlet arranged outside the microwave thermal decomposition furnace, the microwave thermal decomposition furnace comprises a solid-phase pyrolysis part and a gas-phase pyrolysis part connected in order from down to up, the solid-phase pyrolysis part comprises a solid-phase hollow circular column composed of metal mesh, and the solid-phase hollow circular column is filled with a solid-phase microwave absorbent and a catalyst. The reaction apparatus increases the pyrolysis heating rate, reduces the generation amount of solid carbon residue, increases theproportion of pyrolysis gas in products, and optimizes the pyrolysis reaction process, has the advantages of simple equipment, less land occupation, and convenient operation, can complete operation ofcontinuous feeding and deslagging, and is convenient for operation and management.

A method for preparing lanthanum cuprate (La2CuO4) powder by means of the microwave-hydrothermal method includes the following steps: lanthanum nitrate is added into distilled water, so that solution A is obtained; copper nitrate is added into the solution A, so that solution B is obtained; citric acid is added into the solution B, so that solution C is obtained; the pH of the solution C is regulated to 1.5 to 7, so that solution D is obtained; the solution D is added into a microwave-hydrothermal reactor, the reactor is sealed and then put into a microwave-hydrothermal instrument to carry out hydrothermal reaction, and after reaction is finished, the reactor is naturally cooled to the room temperature; sample is collected by centrifugal separation and then repetitively washed by distilled water and acetone, and after drying, the La2CuO4 powder is obtained. Since the method adopts the microwave-hydrothermal method to prepare the La2CuO4 powder, the electric field and the magnetic field can be changed in the space, so that molecular motion can be intensified, as a result, heat energy can be obtained, and thereby the synthesis of the La2CuO4 powder becomes highly efficient, simple and highly repetitive. Moreover, the heating speed is high, heating is uniform and does not have the temperature gradient and the hysteresis effect, consequently, the defect of ununiform heating of a hydrothermal container is overcome, the reaction time is shortened, energy consumption is reduced, and the working efficiency is increased.

The invention discloses a transition Sn-based heterojunction material@spherical high polymer, and a preparation method thereof and application thereof. The preparation method comprises the following steps: adding a spherical high polymer obtained by hydrothermal reaction of glucose into ethanol, adding SnCl4.5H2O, stirring for a certain time, and adding thioacetamide; and heating, adding ethanol at intervals, taking out a precursor after the reaction is finished, and carrying out centrifugal washing and vacuum drying to obtain a composite material. The preparation method is low in preparationcost, simple to operate and short in preparation period, and the prepared material is high in purity, high in crystallinity and uniform in morphology and has certain charge-discharge cycle performancewhen applied to a negative electrode of a sodium-ion battery.

The invention provides a vacuum tube type microwave heating carbon furnace, relates to the technical field of high temperature vacuum coating equipment, and solves the technical problems that a heating temperature field inside the furnace is non-uniform and the resistance value of a resistor carbon film is not inconsistent. The vacuum tube type microwave heating carbon furnace comprises a furnacebody, a magnetron, a double-layer vacuum quartz tube with a jacket, and a microwave absorbing heating material, wherein the magnetron is arranged on a furnace body, and the magnetron can emit microwaves inside an inner cavity of the furnace body after being electrified; the vacuum quartz tube is arranged inside the furnace body in a rotating manner, and treated workpieces are placed inside the vacuum quartz tube for carbon coating film treatment; and the microwave absorbing heating material inside the jacket of the vacuum quartz tube can emit heat after absorbing microwaves, and the furnace body is further internally provided with a heat insulation layer made of a microwave-transmitting material. A novel material sintering method has the characteristics of high heating rate, high energy utilization rate, high heating efficiency, uniform material temperature field, good technological controllability, short technological period, good product uniformity and high rate of finished products.

The invention discloses a device and a method for a microwave heating and concentrating of a tobacco extract. The device comprises a microwave heater used for heating the tobacco extract, an evaporating tank used for collecting the heated tobacco extract, a vapor-liquid separator used for collecting vapor generated in the evaporating tank and carrying out vapor-liquid separation on the vapor, a condenser used for condensing the vapor generated at the vapor outlet of the vapor-liquid separator, and the like. The concentrating method comprises the following steps: a forced circulation pump, themicrowave heater and the vacuum pump are turned on, the tobacco extract enters the microwave heater through the forced circulation pump, and is heated to a preset temperature, the heated tobacco extract enters the evaporating tank, the vapor generated in the evaporating tank enters the vapor-liquid separator, and vapor free from water drops enters the condenser. The tobacco extract is heated and then evaporated in the evaporating tank under a vacuum condition at a low temperature through microwave energy, the structure is simple, and the concentrating temperature is low, so scaling of the tobacco extract is greatly reduced, growth of bacteria is inhibited through microwaves, and the product quality is improved.