4results about How to "Good crystal form" patented technology

The application provides a preparation method of black phosphorus arsenic material, comprising the following steps: mixing gray arsenic, red phosphorus and an additive, and then placing the mixture in a high-temperature area to react in a closed container in a protective atmosphere or vacuum, and synchronously depositing in a low-temperature area to crystallize, so as to obtain black phosphorus arsenic material; wherein the additive comprises tellurium iodide; the temperature of the high-temperature area is not lower than 550 DEG C, and the temperature of the low-temperature area is 450-530 DEG C; and the black phosphorus arsenic material is black phosphorus arsenic single crystal. The application realizes controllable synthesis of flaky black phosphorus arsenic single crystal, and has excellent applicability in semiconductor devices.

This invention belongs to the field of methoxyamine hydrochloride preparation technology and discloses a method for separating methoxyamine hydrochloride and ammonium chloride. The method involves cooling a mixed solution containing ammonium chloride and methoxyamine hydrochloride to selectively crystallize out ammonium chloride, which is then separated to obtain ammonium chloride crystals and a mother liquor enriched with methoxyamine hydrochloride. The mother liquor is then concentrated or dissolved by heating, followed by ultra-low temperature crystallization, separation, and drying to obtain methoxyamine hydrochloride crystals. This invention uses ultra-low temperature segmented crystallization to selectively precipitate ammonium chloride, resulting in methoxyamine hydrochloride crystals with a purity ≥99.9% and ammonium chloride crystals with a purity ≥98%.

This invention relates to the field of wastewater treatment technology, and more particularly to a method for enhancing anaerobic ammonia oxidation (AAO) denitrification using iron-loaded polyurethane porous materials. The method includes the following steps: Anaerobic ammonia oxidation sludge, iron-loaded polyurethane porous materials, and wastewater containing ammonia nitrogen and nitrite nitrogen are thoroughly mixed in an anaerobic reactor and reacted under anaerobic conditions at a temperature of 31-35°C. The iron-loaded polyurethane porous materials are prepared as follows: polyurethane sponge is selected as a carrier, cut and cleaned, and then immersed and stirred in a mixed iron salt solution for a period of time. The pH of the mixed solution is adjusted to alkaline, resulting in the formation of a red precipitate. The iron-loaded polyurethane porous materials are then hydrothermally synthesized. The mixed iron salt solution includes ferric chloride and ferric nitrate. The carrier material prepared by this invention, when applied to an anaerobic ammonia oxidation system, can effectively shorten the process start-up time, promote the enrichment and biofilm formation of anaerobic ammonia oxidizing bacteria, and achieve a high total nitrogen removal rate.