The invention provides high-filling silver
powder and a preparation method thereof, and belongs to the field of
metal powder.The preparation method comprises the steps that a nano-silver solution is prepared, a dispersing agent and a first
reducing agent are mixed to obtain a
mixed solution, the nano-silver solution and the
mixed solution are mixed in a constant-temperature stirring state to obtain a base solution, a second
reducing agent solution and a
silver nitrate solution are prepared respectively, and the high-filling silver
powder is prepared. And under the constant-temperature stirring state, the second
reducing agent solution and the
silver nitrate solution are synchronously added into the base solution, a silver powder solution is obtained through reaction, the silver powder solution is subjected to washing,
solid-liquid separation,
drying and
depolymerization shaping treatment, and the high-filling silver powder is obtained. Controllable preparation of the large-size
sphericity silver powder is achieved by controlling the particle size and the adding amount of the nano-silver, regulating and controlling heterogeneous
nucleation and growth sites of silver ions and inhibiting formation of multistage dendritic crystals,
surface charges and steric hindrance effects of
silver particles are optimized through the surface
adsorption effect of the dispersing agent, the agglomeration phenomenon of the silver powder in the growth process is reduced, and the silver powder is prepared. And meanwhile, the silver powder is endowed with excellent flowability.