A
system and method of making a
sulfur-carbon composite are disclosed. A
nanoporous carbon
powder is placed in a container and a
sulfur source is stored in a staging tube gaseously coupled to the container, allowing delivery of the
sulfur source into the container without introducing any gases. The carbon is desorbed by cyclically heating, evacuating, and backfilling with an
inert gas until a predetermined
desorption temperature is reached, thereby forming a desorbed carbon
powder. After cooling, the sulfur source is transferred onto the desorbed
powder, the container is evacuated and sealed, and a thermal gradient is applied. Excess sulfur may be condensed away from the composite. A
system includes a container having a carbon powder and a staging tube coupled to the container through an O-ring union tee vacuum fitting. A sulfur-carbon composite includes nano-scale
porous carbon having nanometer-scale sulfur dispersed in the pores and on a surface.