Preparation method and application of magnetic chitosan nanometer material
A chitosan nano, chitosan technology, applied in chemical instruments and methods, alkali metal oxides/hydroxides, inorganic chemistry, etc., can solve difficult separation, poor mechanical strength, chemical resistance of chitosan Weak and other problems, to achieve the effect of solving the phenomenon of agglomeration, strong electrophilicity, and strong adsorption
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example 1
[0014] Example 1: Preparation of Magnetic Chitosan Nanomaterials
[0015] (1) Chitosan modification treatment: first add 3g of chitosan powder into the sulfuric acid solution with pH 2 and submerge, soak for 8 hours under magnetic stirring, stop stirring until the chitosan powder is precipitated, and carry out solid-liquid separation. The powder was washed three times with deionized water, then the chitosan powder was put into an oven and dried at 60° C. to form a cake, and pounded into a powder to obtain the modified chitosan.
[0016] (2) Preparation of ferroferric oxide: prepared by co-precipitation method, first put 7.13g FeCl in a beaker 3 ·6H 2 O and 5.56 g FeSO 4 Mix and add deionized water to form a mixed solution of 500ml. Then put the beaker containing the mixed solution into a water bath with a temperature of 60°C, and slowly add ammonia water with a concentration of 3% by mass under stirring until the pH of the mixed solution is 11. After 1 hour of reaction, 1 ...
example 2
[0018] Example 2: Preparation of Magnetic Chitosan Nanomaterials
[0019] The step (1) in Example 1 was omitted, that is, the chitosan was not modified, and the rest of the steps were exactly the same as in Example 1, to prepare magnetic chitosan nanomaterials without chitosan modification.
example 3
[0020] Example 3: The adsorption and removal experiment of phosphorus by magnetic chitosan nanomaterials
[0021] (1) Using a 100ml conical flask as a reactor, add 0.3g of the magnetic chitosan nanomaterial prepared in Example 1.
[0022] (2) Take 50ml of KH with an initial concentration of 5mg / L 2 PO 4 solution, adjust its initial pH to 6 with NaOH solution, add it to the Erlenmeyer flask, then place the Erlenmeyer flask into a full-temperature shaker for oscillating adsorption for 45min, the temperature is set at 25°C, and the speed is set at 180r / min.
[0023] (3) The magnetic chitosan nanomaterials were separated and collected with a magnet, and the supernatant liquid was taken, and the phosphorus content was determined to be 1.97 mg / L, and the removal rate of phosphorus was 61%.
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