404 results about "Sodium salt" patented technology

The invention relates to a preparation method of a rice leavening with a scalp care effect and a product and application thereof, the preparation method comprises the following steps: mixing a rice raw material, a plant raw material, water, a magnesium salt, a sodium salt and Tween, sterilizing to obtain a fermentation medium, inoculating a compound microbial agent into the fermentation medium, and fermenting to obtain the rice leavening with the scalp care effect. After the fermentation liquid is finished, sterilizing and filtering to obtain a rice leavening; wherein the compound microbial agent comprises a first microbial strain and a second microbial strain; the strains in the first microbial strain comprise a combination of streptococcus thermophilus, bifidobacterium breve and a plant lactobacillus YK-L002 strain; and the second microbial strain comprises a trichosporon YK-S004 strain. According to the invention, specific strains are subjected to compounding and combined fermentation, and the fermentation product filtrate obtained after fermentation treatment of four bacteria has excellent hair care and nourishing effects, and can effectively condition the scalp micro-ecological environment and nourish the hair quality.

The invention discloses a method for preparing a NaFeO2 material and leaching copper, zinc and molybdenum from copper slag, and relates to the technical field of metallurgical solid waste resource utilization. The method comprises the following steps: grinding the copper slag, mixing the ground copper slag with a sodium salt, roasting the mixture in a muffle furnace at a proper temperature, and finally carrying out ultrasonic washing and filtering on the roasted product to obtain filter residues and filtrate; and drying filter residues to obtain a high-purity NaFeO2 material, and recovering valuable metals such as copper, zinc and molybdenum from filtrate. In the washing process, valuable metal elements copper, zinc and molybdenum in the copper slag are efficiently leached into the solution, the leaching rate reaches 96% or above, and synchronous recovery of the valuable elements is achieved; according to the method, the industrial waste residue copper slag is successfully converted into the NaFeO2 product with the high additional value, meanwhile, valuable metal is efficiently extracted, the method has the advantages of being simple in process, low in cost, high in recycling degree and environmentally friendly, a new way is opened up for high-value utilization of the copper slag, and the method has good industrial application prospects.

The invention relates to the technical field of battery sodium supplementation agents, in particular to a sodium supplementation agent with a core-shell structure, a preparation method and a positive pole piece. The preparation method comprises the following steps: providing a core material containing sodium salt; a first coating process: providing a first coating material containing organic fluorine, mixing the core material containing the sodium salt with the first coating material, and performing first sintering to obtain a primary coating coated with a first coating layer; and a second coating process: providing a second coating material containing a carbon source, mixing the second coating material with the primary coating, and carrying out second sintering to obtain the sodium supplement which is coated with a first coating layer and a second coating layer and has the core-shell structure. The invention provides the sodium supplementing agent with the core-shell structure, the preparation method and the positive pole piece, so that the problem of poor sodium supplementing performance of the sodium supplementing agent in the related technology is solved.

The application discloses a meat protein emulsion with low-sodium and low-oil phase characteristics for 3D printing and a preparation method and application thereof. The application utilizes anionic polysaccharide xanthan gum and L-arginine to synergistically stabilize the low-sodium and low-oil phase meat protein emulsion, and improves the 3D printing performance thereof. The xanthan gum and L-arginine enhance the stability and rheological properties of the emulsion by inducing the unfolding of meat protein structure and reducing the oil-water interfacial tension. The xanthan gum can also prevent the aggregation of droplets by constructing a weak gel network in the water phase and providing negative charges. Therefore, the meat protein emulsion stabilized by the synergistic action of the xanthan gum and L-arginine overcomes the problems of poor emulsion stability and inability to print caused by partial replacement of sodium salt and low oil phase, and endows the meat protein emulsion with good viscoelasticity, thixotropic recovery performance and self-supporting property, thereby realizing high-fidelity printing. The application recommends the dual use of the xanthan gum and L-arginine, which can not only reduce the intake of sodium and oil to ensure health, but also help produce high-quality or personalized muscle protein food.

The application belongs to the technical field of gene detection, and particularly relates to a biological sample nucleic acid rapid extraction method and kit based on a magnetic bead method. The method comprises the following steps in sequence: S1, liquefying a biological sample by using a liquefying solution; the liquefying treatment is to add 1-4 times the volume of the liquefying solution to the biological sample, shake and mix, and then place at room temperature for 15-30 minutes; the liquefying solution comprises guanidine salt, potassium salt and / or sodium salt, Tris-HCl, EDTA and isopropyl alcohol; S2, lysing the biological sample; adding a lysing solution and magnetic beads to the system obtained in S1, and heating at 90-100 DEG C for 3-20 minutes to lyse the biological sample; S3, cleaning the biological sample; and S4, eluting the nucleic acid. The method does not need centrifugal separation in the operation process, and can realize automatic and efficient extraction of the nucleic acid.

The invention provides a sodium ion specific fluorescence labeled transparent soil sample as well as a preparation method and application thereof, and belongs to the technical field of rock soil and geological engineering. The method comprises the following steps: firstly, sequentially carrying out hydrophilization treatment, solvent evaporation and dissolution on a sodion combined benzofuran isophthalate probe to obtain a probe mother solution; mixing the probe mother solution, a buffer solution, an inorganic sodium salt solution and a solvent to prepare a fluorescence labeling pore solution; and finally, mixing the sodium polyacrylate particles and the fluorescence labeled pore liquid, and performing vacuum saturation treatment to obtain the transparent soil sample. The transparent soil sample provided by the invention still keeps excellent optical transparency while having sodium ion specific response capability, so that a stable and reliable experimental medium is provided for in-situ, real-time and full-field observation of sodium ion migration.

The application provides a preparation method of a precursor pre-adsorption sodium-supplemented sodium iron phosphate pyrophosphate positive electrode material, uses hydrated iron phosphate as a precursor, and places the precursor in a sodium salt of an organic weak acid sodium supplement solution for impregnation adsorption, and after drying, is mixed with a sodium source, a phosphoric acid source, a pyrophosphoric acid source and a carbon source, and is sintered in an inert atmosphere to obtain a pre-sodium-supplemented Na4Fe3(PO4)2P2O7 / C material. The application also provides a sodium iron phosphate pyrophosphate positive electrode material prepared by using the above method, and a sodium ion battery comprising the material. By impregnating and adsorbing the sodium salt of the organic weak acid sodium supplement on the industrial precursor of the sodium iron phosphate pyrophosphate, the nanoscale dispersion of the sodium supplement is achieved, the toxicity and high gas production of the traditional sodium supplement are avoided from the root, the process is adapted to the existing industrial production line, the first coulomb efficiency and the cycle stability of the sodium iron phosphate pyrophosphate positive electrode material are effectively improved, and the industrial application is promoted.

This invention relates to a sodium-supplementing material capable of simultaneously replenishing active sodium and sodium hexafluorophosphate, and its preparation and application. The sodium-supplementing material comprises the following raw material components by weight percentage: 10-50% elemental phosphorus, 50-90% sodium fluoride, and 1-5% Ketjen Black. Compared with existing technologies, the phosphorus-based bifunctional sodium-supplementing separator and sodium-supplementing cathode provided by this invention not only possess higher theoretical capacity, effectively compensating for irreversible capacity loss during the first cycle of the battery, but also generate NaPF6 in situ under electrochemical conditions through the synergistic reaction of red phosphorus and sodium fluoride, achieving simultaneous replenishment of active sodium and electrolyte sodium salts, thereby improving the initial coulombic efficiency and long-term cycle performance of the battery.

The invention provides a processing method of a salt-replacing freshness-enhancing food raw material, and the food raw material is subjected to enzymolysis treatment to enhance the salty and delicious taste of the food. Compared with the prior art that most salt substitute products in the market are prepared after proteolysis, but protein is used as an enzymolysis substrate, food raw materials need to be extracted for multiple times, and the cost is high. According to the processing method, cheap and easily available raw materials (such as potato whole flour and the like) are used as base materials, small molecule peptides with delicate flavor characteristics are generated after enzymolysis, and the small molecule peptides, starch, dietary fibers and the like have a synergistic effect to obtain the salty and delicious salt substitute product, so that various diseases caused by excessive intake of sodium salt can be effectively avoided.

A rinsing solution for photodynamic disinfection, in particular oral disinfection, including, at least one photosensitiser from the group comprising riboflavin 5′-phosphate sodium in a proportion of 0.2 to 0.6 wt. % and a photosensitiser other than riboflavin 5′-phosphate sodium in a proportion of 0.001 to 0.05 wt. %, at least one viscosity modulator from the group comprising glycerol in a proportion of 1.0 to 5.0 wt. % and hyaluronic acid sodium salt in a proportion of 0.01 to 0.3 wt. %, at least one biofilm inhibitor from the group comprising xylitol in a proportion of 7.0 to 25.0 wt. %, L-arginine in a proportion of 0.01 to 0.5 wt. % and urea in a proportion of 0.5 to 3.0 wt. %, with the remainder on a water base.

A method for producing an inclusion complex drug includes the following steps: adding cyclodextrin to an aqueous solution of ibuprofen sodium salt at a saturation concentration at a first temperature, then placing it in an electrodialysis apparatus to obtain a first crystallization solution; then removing it and adding acid to adjust the pH to 6.0-6.5, controlling the temperature at a second temperature to obtain a second crystallization solution; placing the second crystallization solution in an electrodialysis apparatus to obtain a third crystallization solution; then removing it and continuing to add acid to adjust the pH to below 3.0 to obtain a fourth crystallization solution; filtering and recovering the fourth crystallization solution, and rinsing to obtain the ibuprofen inclusion complex. This application uses pre-added cyclodextrin, with cyclodextrin and the ibuprofen sodium salt obtained from the reaction as feedstock, then obtaining the second crystallization solution through electrodialysis acidification and acid treatment, followed by electrodialysis to obtain raw materials that can be used as nucleation sites for crystallization, and finally adding acid for final crystallization. The entire crystallization process is controllable.

The invention discloses a decontamination and dust fall reagent as well as a preparation method and application thereof. The preparation method comprises the following steps: (1) preparing a compound solution: adding ferrous gluconate, sodium alkyl sulfosuccinate, sodium alcohol ether sulfate, lauryl sodium sulfate and polyacrylamide into deionized water according to the mass fraction of 0.10%-0.15%, 0.05%-0.20%, 0.05%-0.15%, 0.10%-0.15% and 0.005%-0.02% respectively to obtain the compound solution; (2) preparing micro-nano bubble water; and (3) adding the compound solution into the micro-nano bubble water in a volume ratio of 1: (0.5-2), and fully mixing the compound solution and the micro-nano bubble water to obtain the decontamination and dust fall reagent. According to the decontaminating and dust-settling reagent prepared by the invention, an environment-friendly surfactant is selected, so that dust can be settled, toxic and harmful gases generated by explosion can be removed by utilizing the characteristic that micro-nano bubble water directly participates in catalytic oxidation, and a good decontaminating and dust-settling effect is achieved.

The invention belongs to the technical field of lithium salt purification, and discloses a lithium extraction method and a lithium extraction device. The method comprises the following steps: providing a lithium-containing mixed salt; contacting the lithium-containing mixed salt with an organic solvent to form an organic solution rich in lithium salt and a mixed system containing an undissolved sodium salt solid; and carrying out interface evaporation on the mixed system to remove part of the organic solvent and promote the precipitation of the sodium salt, and enriching the lithium salt in the residual liquid phase to realize the separation of the lithium salt and the sodium salt. The method provided by the invention can realize high-efficiency and high-selectivity separation of the lithium salt and the sodium salt.

The present invention is directed to a method for acidulation of tall oil soap in an alcohol selected from methanol, ethanol and / or iso-propanol. In the method according to the present invention, a mixture comprising sodium salts of fatty acids and rosin acids and an alcohol selected from methanol, ethanol and / or iso-propanol is acidulated using carbon dioxide.

The invention relates to the field of compound preparation, in particular to a high-efficiency dialkylation method of salicylic acid compounds, which is characterized in that salicylic acid and derivatives thereof are used as raw materials, and a dialkylation product of salicylic acid is efficiently prepared in one step through the steps of preparing multiple sodium salts, removing water, esterifying and the like. The method is simple to operate, high in atom economy, high in product purity and free of wastewater discharge.

This invention discloses a method for preparing high-quality low-sodium salt. The preparation method includes: providing a first raw material, a second raw material, and a base liquid, wherein the first raw material comprises a sodium-potassium saturated solution, the second raw material comprises magnesium chloride ore, and the base liquid comprises the following components: Na... + K + Mg 2+ C1 ‑ The process involves placing the base liquid in a DTB crystallization apparatus and simultaneously introducing the first and second raw materials at a first and a second feed rate, respectively, under a stirring speed of 500–700 rpm. After at least 80 minutes, intermittent discharge is performed, followed by solid-liquid separation to obtain high-quality low-sodium salt. The high-quality low-sodium salt prepared by this invention has a particle size greater than 150 μm in 96% of the product. Furthermore, the preparation method is simple and controllable, achieving precise particle size control in the low-sodium salt production process.

The application provides an in-situ liquid gel-forming water-retaining agent and a preparation method and application thereof. The water-retaining agent is composed of A component and B component which are applied in steps. The A component contains an aqueous solution of a natural modified polymer, and the natural modified polymer is selected from one or two of carboxymethyl chitosan, carboxymethyl cellulose or a sodium salt thereof. The B component contains an aqueous solution of a cationic crosslinking agent, and the cationic crosslinking agent is selected from one or more cations of copper nitrate, iron nitrate, zinc nitrate, manganese nitrate, chitosan quaternary ammonium salt, calcium nitrate and magnesium nitrate. The water-retaining agent can realize the integrated functions of slow release of trace elements, water retention, soil improvement and precise nutrition supply. Furthermore, the water-retaining agent is applied to crop growth in combination with the "step-by-step drip irrigation and in-situ gel formation" technology, so that the agronomic characters of crops can be significantly improved.

The application relates to the technical field of organic synthesis, and discloses a preparation method of a hydrocarbyl carboxylic acid, which comprises the following steps: mixing a hydrocarbyl aldehyde, an oxidizing agent and a first metal salt to perform pre-reaction, and then mixing the reaction system obtained through the pre-reaction with a second metal salt to perform reaction; wherein the first metal salt is selected from at least one of a sodium salt, a potassium salt, a calcium salt, a lithium salt, an iron salt and a copper salt; and the second metal salt is selected from at least one of a zinc salt, a manganese salt, a cobalt salt, a palladium salt and a silver salt. The preparation method of the hydrocarbyl carboxylic acid can greatly shorten the reaction time, and improve the raw material conversion rate, the target product selectivity and the target product purity of the aldehyde oxidation acid reaction.

The invention provides (Z)-(4-(4-aminophenyl) amino)-sodium maleate and a preparation method and application thereof, and belongs to the technical field of rubber assistants.The preparation method comprises the following steps that S1, maleic anhydride is added into a mixed solution of 4-aminoaniline and an organic solvent for a reaction, an intermediate is generated, and a reaction mixture is obtained; s2, heating the reaction mixture, carrying out an isomerization reaction to promote the intermediate to be converted into a (Z) type configuration, then adding an alkaline compound, carrying out a salt forming reaction, and adjusting the pH value; and S3, carrying out post-treatment on the solution obtained in S2 to obtain the (Z)-(4-(4-aminophenyl) amino)-sodium maleate. According to the technical scheme provided by the invention, the purpose of obtaining the novel multifunctional rubber additive which has anti-reversion and thermal aging-resistant functions and is environment-friendly is achieved.

The application belongs to the technical field of wastewater treatment, and particularly relates to a method for separating inorganic salts in a sodium-magnesium sulfate mixed solution. A magnesium salt with relatively large solubility is added to a feed liquid containing sodium-magnesium sulfate, and magnesium sulfate heptahydrate is precipitated at normal temperature and low temperature, respectively, and sodium salt is precipitated at high temperature in the heating and evaporation process, thereby forming a continuous zero-emission disposal sodium-magnesium sulfate separation process. The process has strong universality, is suitable for an aqueous solution system with a mass ratio of magnesium sulfate to sodium sulfate of 1-4, has zero emission in the process, does not pollute the environment, and is an environmentally friendly new technology for separating sodium-magnesium sulfate.

The application belongs to the technical field of oil exploitation, and particularly relates to an acid liquid for acid treatment of an oil layer and a preparation method thereof. The preparation method is as follows: the specific steps of the preparation method are as follows: in a reactor, piperazine-1,4-diethyl sulfonate monosodium salt, ethanol and bromoalkane are added, heated to reflux, and during the reaction, sodium hydroxide solution is used to maintain pH 7-8; 1-bromo-6-(trimethylammonium) hexyl bromide is added, heated to reflux, and during the reaction, sodium hydroxide solution is used to maintain pH 8-9; vacuum distillation is performed to obtain a viscous solid, cyclohexane recrystallization is performed to obtain a solid, and the solid is dried at 90 DEG C overnight to obtain corrosion-inhibiting acid; hydrochloric acid, hydrofluoric acid, hydroxyethylidene diphosphonic acid, corrosion-inhibiting acid and water are added to the reactor, stirred uniformly, and the acid liquid is obtained. The acid liquid has the advantages of low corrosion rate and long acidification time.

The invention belongs to the technical field of molecular biology, and particularly relates to a pathogenic microorganism nucleic acid co-extraction kit, an extraction method and application. The invention provides a lysis solution for nucleic acid co-extraction of pathogenic microorganisms. The lysis solution comprises a first guanidine salt, an ionic surfactant, a first sodium salt and a first nonionic surfactant. According to the splitting system, guanidine salt is adopted and matched with a certain content of sodium salt and a surfactant, a sample is split and precipitated under the grinding condition, nucleic acid cannot be damaged in the crushing process, and pathogenic microorganism DNA and RNA with high concentration and complete fragments can be extracted.

The present application relates to a combination of 5-amino-2,3-dihydro-1,4-phthalazinedione or one of its pharmaceutically acceptable salts and at least one fumaric acid ester or a pharmaceutically acceptable salt thereof. In particular, the invention relates to the use of 5-amino-2,3-dihydro-1,4-phthalazinedione sodium salt in said pharmaceutical combination. Pharmaceutical compositions and advantageous formulation techniques are disclosed.

Pharmaceutical compositions containing specific tetrapeptides for use in treating, preventing, minimizing, diminishing or reversing degenerative, age-related, or trauma-induced diseases or disorders in a subject in need thereof. The disease may be a disease associated with ROS-related oxidative stress. The tetrapeptides may have an amino acid sequence of pGlu-Asn-Trp-Lys(Octanoyl)-OH as set forth in SEQ ID NO: 1 or pGlu-Asn-Trp-Thr-OH as set forth in SEQ ID NO: 2, preferably as a sodium salt thereof.

This invention discloses a method for preparing tert-butyl benzoate peroxide using a microchannel reactor, comprising the following steps: adding liquid alkali to tert-butyl hydroperoxide, allowing it to stand and separate into layers, and obtaining the lower sodium salt; passing the obtained sodium salt into the microchannel reactor, simultaneously passing benzoyl chloride into the microchannel reactor for mixing and reaction; passing the material emanating from the microchannel reactor into an RTB reactor for incubation and reaction to obtain crude tert-butyl benzoate peroxide; purifying the crude tert-butyl benzoate peroxide to obtain tert-butyl benzoate peroxide. This invention employs continuous feeding and achieves the synthesis reaction through a microchannel reactor, reducing the reaction time from several hours to tens of seconds to several minutes, significantly improving reaction efficiency. The entire reaction process in the microchannel reactor used in this invention is a continuous reaction, which is safe and environmentally friendly, has high production efficiency, requires a small equipment footprint, is simple to operate, reduces manual operation, and lowers production costs.

The application relates to the technical field of synthetic rubber, in particular to a nitrile rubber, a preparation method and application thereof, wherein the preparation method adopts at least potassium saponification soap and / or sodium saponification soap of disulfated rosin acid, C 10 -C 13 A composite emulsifier system composed of linear alkyl benzene sulfonic acid and naphthalene sulfonic acid formaldehyde condensate sodium salt and a low-temperature emulsion polymerization process, and the obtained nitrile rubber can be used in the field of oil-resistant sealing in a hydraulic oil operation environment.

The invention discloses a 2-hydroxy-benzonitril solution and a production method thereof, the production method comprises the step of preparing a wet 2-hydroxy-benzonitril product through reaction of salicylamide and phosgene, and is characterized in that the wet 2-hydroxy-benzonitril product is directly added into a sodium hydroxide aqueous solution to obtain the 2-hydroxy-benzonitril solution. The sodium salt solution can be directly produced without taking out the 2-hydroxy-benzonitril, so that exposure of the 2-hydroxy-benzonitril is avoided, personal injury is reduced, investment of drying equipment is reduced, and direct feeding of downstream products is facilitated.

The application discloses a preparation method and system of sodium difluorophosphate. The preparation method of sodium difluorophosphate comprises the following steps: S100, in a water-free or low-water environment, a solid-phase reaction is generated between diphosphorus pentoxide and ammonium fluoride to obtain an ammonium difluorophosphate intermediate, and volatile substances generated in the reaction process are removed and recovered; S200, in a water-free organic solvent, the ammonium difluorophosphate intermediate obtained in the step S100 is reacted with a sodium salt to obtain sodium difluorophosphate. The preparation method of sodium difluorophosphate provided by the application uses diphosphorus pentoxide and ammonium fluoride as reaction raw materials to obtain an ammonium difluorophosphate intermediate, and then reacts to obtain sodium difluorophosphate. The obtained sodium difluorophosphate has high purity and few impurities. The preparation method of sodium difluorophosphate has the advantages of cheap and easily obtained raw materials, stable chemical properties, few by-products generated in the reaction, and easy recovery, and is a green and safe preparation method of sodium difluorophosphate.

The application provides a nanoemulsion and a preparation method and application thereof. The total amount of raw materials for preparing the nanoemulsion is 100%, and the raw materials include the following components: 1-40% of a composite surfactant, 1-25% of an oil phase, 1-30% of a co-surfactant, and the balance of a water phase; wherein the mass of the composite surfactant is 100%, and the composite surfactant includes the following components: 5-25% of a biological surfactant, 35-65% of a fatty alcohol polyoxyethylene ether surfactant, 1-20% of dodecyl benzene sulfonic acid and / or sodium salt thereof, 1-20% of oleic acid, and 1-5% of citric acid; the biological surfactant includes one or more than two combinations of sophorolipid, rhamnolipid, trehalose lipid, surfactin, alkyl polyglycoside, phosphatidylcholine, amino acid lipid, saponin, phospholipid, or derivatives thereof; and the average particle size of the emulsion droplets in the nanoemulsion is 1.5-5 nm. The nanoemulsion has excellent recovery performance.

The invention relates to a preserving fluid for stabilizing viruses at normal temperature and high temperature as well as a preparation method and application of the preserving fluid. The preserving fluid is an aqueous solution containing the following components in concentration: 2mM-15mM of ethylenediamine tetraacetic acid tetrasodium salt, 5mM-20mM of sodium citrate, 0.1 wt%-10wt% of tween-20, 10wt%-30wt% of a structure stabilizer, 0.5 wt%-10wt% of an amide solution, 0.5 wt%-10wt% of a hemolysis inhibitor, 0.05 wt%-10wt% of a reducing agent and 0.1 mM-2mM of 3-morpholine propanesulfonic acid. According to the preservation solution, the formula is optimized, and particularly, the amide solution and the reducing agent component are matched with MOPS for use, so that the activity of viruses in a sample under normal-temperature and high-temperature conditions can be greatly maintained, and the stability of nucleic acid is effectively improved.