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473 results about "Acrydite" patented technology

Acrydite is a phosphoramidite that allows the synthesis of oligonucleotides with a methacryl group at the 5' end (less commonly 3' or internal). Acryl oligonucleotides have been tested, but the acryl group is not stable to storage. Acrydite-modified oligonucleotides can react with nucleophiles such as thiols (Michael addition chemistry), this forms the basis of the ez-rays chemistry which was used for microarrays. More importantly, Acrydite-modified oligonucleotides can be incorporated, stoichiometrically, into hydrogels such as polyacrylamide, using standard free radical polymerization chemistry, where the double bond in the Acrydite group reacts with other activated double bond containing compounds such as acrylamide.

Thickener used for self-compact concrete, preparation method thereof, and self-compact concrete using thickener

The invention discloses a preparation method of a thickener used for self-compact concrete. The method comprises the following steps: 1, weighing 2-acrylamide-2-methylpropanesulfonic acid and acrylic acid in proportion, processing to prepare an aqueous solution, and adjusting the pH value to 6.5-7.0; 2, adding a prepared monomer acrylamide solution with the concentration of 25-35% while stirring, uniformly stirring, dumping the obtained mixed solution into a flask, carrying out constant temperature water bath, and introducing nitrogen for protection; and 3, adding an initiator in a dropwise manner when the reaction temperature rises to 30-40DEG C, carrying out heat insulation at 40DEG C, carrying out a stirring reaction for about 1.5-2h, stopping the introduction of nitrogen when reactants are a viscous liquid, and carrying out constant temperature slaking for a period of time to obtain a white transparent colloid which is the thickener. The thickener obtained in the invention is used for preparing the self-compact concrete, has a good water solubility and a good thickening effect, can effectively improve the plastic viscosity of the self-compact concrete, and solves the water segregation and separation problems of the self-compact concrete.
Owner:CCCC FOURTH HARBOR ENG INST +4

Heatproof oil well cement fluid loss additive and preparation method thereof

The invention belongs to a heat-resistant oil well cement fluid loss additive and a preparation method thereof. The invention is characterized in that the method adopts industrial raw materials of acrylamide and 2-acrylamide-2-methyl-1-AMPSA to carry out copolymerization with N-vinyl pyrrolidone; firstly 10-120 portions of 2-acrylamide-2-methyl-1-AMPSA and 15-50 portions of deionized water are added into a reactor with an agitator and a thermometer, agitated and then added with sodium hydroxide aqueous solution with the mass fraction of 5-10 percent for neutralizing to pH equal to 3-11; then 10 portions of acrylamide, 0.1-1 portion of complexing agent EDTA and 0.01-1 portion of chain transfer agent are added, the chain transfer agent is isopropyl alcohol or sodium benzoate, the temperature is controlled between 30 DEG C and 60 DEG C and N2 is introduced for 30 minutes; 2-10 portions of N-vinyl pyrrolidone and 0.01-0.5 portion of initiator are added, the initiator is potassium persulfate or ammonium persulfate, and the reaction is carried out for 4-12 hours to obtain the oil well cement fluid loss additive. The method has simple preparation. The prepared high-temperature resistant spacer fluid keeps still for 5 hours at the temperature of 180 DEG C, and is cooled through flowing water after being taken out, without sedimentation or water separating; and the spacer fluid keeps still for 15 hours at the temperature of 200 DEG C, and is cooled through flowing water after being taken out, without sedimentation.
Owner:CHANGZHOU INST OF ENERGY STORAGE MATERIALS &DEVICES
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