High temperature resistant anticorrosion coating based on graphene and preparation method thereof

An anti-corrosion coating and graphene technology, applied in anti-corrosion coatings, epoxy resin coatings, coatings, etc., can solve the problems of unclear key functions of graphene, inability to uniformly disperse graphene, and fast electron transfer speed. The effect of easy industrial production, low production cost and simple operation

Inactive Publication Date: 2014-02-19
SHANGHAI UNIVERSITY OF ELECTRIC POWER
View PDF5 Cites 88 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although the patent uses graphene as the main filler, the preparation method only uses stirring and mixing, which cannot make the graphene evenly dispersed, so that it canno...

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • High temperature resistant anticorrosion coating based on graphene and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] Each component is equipped with the following mass percentages: epoxy resin (commercially available 665 silicone epoxy resin) 20%, polyphenylene sulfide resin 20%, amino resin (commercially available 520 urea-formaldehyde resin) 20%, pigment (titanium white powder) 5%, graphene 10%, n-butanol 14%, defoamer (tributyl phosphate) 0.2%, poly 2-hydroxyacrylic acid sodium salt 6%, dibutyl phthalate 4%, bentonite 0.5 %, leveling agent (silicone oil) 0.3%.

[0032] The graphene-based high temperature resistant anti-corrosion coating is prepared through the following steps:

[0033] (1) Graphene, epoxy resin and polyphenylene sulfide resin are added in n-butanol, ultrasonically stirred for 150 minutes;

[0034] (2) Add amino resin, pigment, defoamer, polyhydroxy acid sodium salt, dibutyl phthalate, and leveling agent into the grinder according to the specified amount, and grind to a fineness of less than 30 microns;

[0035] (3) Mix the material obtained in step (1) and step (...

Embodiment 2

[0037] The components are prepared according to the following mass percentages: epoxy resin (ES-06 silicone epoxy resin) 25%, polyphenylene sulfide resin 25%, amino resin (582 melamine formaldehyde resin) 15%, pigment (zinc oxide) 5% %, graphene 10%, n-butanol 10%, defoamer (GP type defoamer) 0.2%, polyhydroxy acid sodium salt 5.5%, dibutyl phthalate 3%, bentonite 0.8%, leveling Agent (polydimethylsiloxane) 0.5%.

[0038] The graphene-based high temperature resistant anti-corrosion coating is prepared through the following steps:

[0039] (1) Graphene, epoxy resin and polyphenylene sulfide resin are added in n-butanol, ultrasonically stirred for 150 minutes;

[0040] (2) Add amino resin, pigment, defoamer, polyhydroxy acid sodium salt, dibutyl phthalate, and leveling agent into the grinder according to the specified amount, and grind until the fineness is less than 30 microns;

[0041] (3) Mix the material obtained in step (1) and step (2) and stir for 90 minutes, add bentonit...

Embodiment 3

[0043] The components are prepared according to the following mass percentages: epoxy resin (ES-06 silicone epoxy resin) 40%, polyphenylene sulfide resin 10%, amino resin (576-1 melamine phenylguanamine resin) 10%, pigment (Red iron oxide) 8%, graphene 5%, n-butanol 20%, defoamer (GPE type defoamer) 0.3%, polyhydroxy acid sodium salt 3.5%, dibutyl phthalate 2%, Bentonite 0.8%, leveling agent (polyether polyester modified organosiloxane) 0.4%.

[0044] The graphene-based high temperature resistant anti-corrosion coating is prepared through the following steps:

[0045] (1) Graphene, epoxy resin and polyphenylene sulfide resin are added in n-butanol, ultrasonically stirred for 150 minutes;

[0046] (2) Add amino resin, pigment, defoamer, polyhydroxy acid sodium salt, dibutyl phthalate, and leveling agent into the grinder according to the specified amount, and grind until the fineness is less than 30 microns;

[0047] (3) Mix the material obtained in step (1) and step (2) and s...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention relates to a high temperature resistant anticorrosion coating based on graphene and a preparation method thereof. The high temperature anticorrosion coating comprises the following components by the mass percentage: 5-60% of epoxy resin, 3-30% of polyphenylene sulfide resin, 3-30% of amino resin, 1-10% of a pigment, 1-20% of graphene, 3-50% of n-butyl alcohol, 0.1-0.3% of a defoaming agent, 0.1-10% of polyhydroxy acid sodium salt, 0.1-5% of benzenedicarboxylic acid dibutyl ester, 0.5-1.0% of bentonite, and 0.2-0.5% of a leveling agent. Compared with the prior art, the prepared coating has the advantages of quite excellent waterproof and anticorrosion performance, high temperature resistance, weather resistance, alkali resistance, impact resistance, artificial aging resistance and the like, and the preparation method has the advantages of good controllability, simple operation, low production cost, and easy industrialized production.

Description

technical field [0001] The invention relates to a coating and a preparation method thereof, in particular to a graphene-based high temperature resistant anticorrosion coating and a preparation method thereof. Background technique [0002] High temperature resistant coating is an important coating, which is suitable for anticorrosion of chimney flue, high temperature steam pipe, heat exchanger, high temperature furnace, high temperature desulfurization equipment, petroleum and petrochemical cracking device, engine parts and exhaust pipe. In addition, some special high-temperature-resistant anti-corrosion coatings are widely used in aerospace, petroleum and petrochemical, metallurgy, electric power, and national defense fields. Since the industrial production of organic silicon in the 1940s, the high-temperature resistant coatings formulated with its products have been widely used in high-temperature motors and electrical insulation. For example, organosilicon-aluminum powder...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): C09D163/00C09D181/02C09D161/24C09D161/28C09D5/08C09D7/12
Inventor 时鹏辉姚伟峰周笑绿郑红艾胡晨燕蒋路漫
Owner SHANGHAI UNIVERSITY OF ELECTRIC POWER
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap