The invention discloses a
wastewater treatment and
recovery process in the production process of a layered
oxide positive
electrode material of a
sodium-
ion battery, and belongs to the field of
environmental protection, the
wastewater treatment and
recovery process comprises the following steps: S1, respectively carrying out
pH regulation on
mother liquor and washing water, and respectively carrying out MF microporous
filtration on the
mother liquor and the washing water after
pH regulation; s2, the filtered
mother liquor and washing water are subjected to pH adjustment respectively, and the mother liquor and washing water subjected to pH adjustment are subjected to
UF ultrafiltration respectively; s3, carrying out first-stage RO membrane treatment on the washing water UF
produced water subjected to
UF ultrafiltration; carrying out second-stage RO membrane treatment on mother liquor UF
produced water and first-stage RO concentrated water after
UF ultrafiltration; s4, carrying out resin defluorination on the concentrated water treated by the second-stage RO membrane; the
produced water after the second-stage RO membrane treatment is returned to the first-stage RO membrane treatment in the step S3; and S5, treating the
wastewater subjected to resin defluorination through a bipolar membrane, and recovering to obtain
sodium hydroxide and
sulfuric acid, so that the problem that
sodium ions and
sulfate ions cannot be recovered in the prior art is solved.