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True triaxial loading and unloading test device for large-size bedded pressure-bearing rock and testing method

The invention discloses a true triaxial loading and unloading test device for large-size bedded pressure-bearing rock and a testing method. The device comprises a confining pressure loading module, a sample storage and water outlet module, a confined water loading module, a load loading module and a signal collecting and processing system, wherein the confining pressure loading module comprises two horizontal loading and unloading systems which are independent and perpendicular to each other and is used for performing horizontal load loading and unloading on the wrapped sample storage and water outlet module; the confined water loading module is located at the bottom of the sample storage and water outlet module and is used for performing confined water loading and unloading on the bottom of the bedded rock; the load loading module is located at the top of the sample storage and water outlet module and is used for performing vertical load loading and unloading on the top of the bedded rock; the signal collecting and processing system is used for collecting and analyzing signals in a test process. The test device realizes the true triaxial test of the bedded rock through four independent loading and unloading systems, truly simulates three-way anisobaric stress state of the coal-series bedded pressure-bearing rock and is more true and more reliable than a conventional triaxial test.
Owner:ANHUI UNIV OF SCI & TECH

Adjustable laser coaxial powder feeding nozzle

The invention discloses an adjustable coaxial laser nozzle for sending powder, comprising a laser head, a protection lens, a water-cooling sleeve for the protection lens and a column laser cavity arranged on the upper part, a coaxial conical laser cavity which is formed by the inner layer of a laser sleeve and arranged in the middle part, wherein a powder cavity, a secondary external protective cavity and an external water-cooling cavity are arranged on the lower part of the external part of the laser sleeve; the powder cavity is formed between the laser sleeve and a power cavity sleeve screwed together; the secondary external protective cavity is formed between the powder cavity and a protective air casing screwed together; the powder cavity and the protective sir casing are screwed together and adjustable between 1mm to 3mm; 4 to 6 power transmitting pipes and 4 to 6 air tubes are respectively positioned around the top parts of the cones of the powder cavity and the protective air cavity. The adjustable coaxial laser nozzle for sending powder has the advantages that the focus length of the focus lamp fit for the coaxial powder-sending nozzle is between 100mm to 300mm, which ensures convenient assembly and disassembly, even velocity, flexible adjustment of the powder converge diameter, convenient changeable lower coaxial conical parts (the powder cavity, the air casing and the water cavity).
Owner:XI AN JIAOTONG UNIV

Multi-hole foam glass carrier for fast mass transfer biological fluidized bed and preparation method and application thereof

The invention relates to a multi-hole foam glass carrier for a fast mass transfer biological fluidized bed and a preparation method and application thereof, which belong to sewage disposal technology. The multi-hole foam glass carrier is prepared by using waste glass as a raw material to be composited with volcanic rocks, coal ash, coal gangue, furnace clinker, iron powder, aluminum powder, binding agents, foaming agents, foam stabilizer and fluxing agents by weight, and multi-hole foam glass is obtained by stages of preheating, fast sintering, foaming, fast cooling and annealing. The preparation process of the multi-hole foam glass carrier is simple in route, easy to control and low in cost, and the prepared carrier is stable in performance, high in porosity, large in specific surface area, resisting in impact, good in mechanical performance, high in biocompatibility, favorable to efficient fixing of the microorganism, and suitable to the fast mass transfer biological fluidized bed. The multi-hole foam glass carrier solves the problem that biological immobilization carriers in the prior art are easy to abrade, small in bio-film formation amount, low in mass transfer effects and the like in the fast mass transfer biological fluidized bed. The preparation method opens up new approaches for preparing the biological carriers, and fills blank spaces in using of foam glass materials in sewage disposal.
Owner:NANJING UNIV OF TECH

Solid flaky polycarboxylate water-reducer and polymerization preparation method thereof

ActiveCN106543382AImprove conversion rateHigh branch densityWater solubleDicarboxylic acid
The invention discloses a solid flaky polycarboxylate water-reducer and a polymerization preparation method thereof. The polymerization preparation method comprises the following specific steps: placing 850 to 890 parts of polyether macro-monomer in a reaction kettle without adding water or any organic solvent, and heating to 65 to 75 DEG C; stirring until the polyether macro-monomer is dissolved completely, keeping the temperature at 65 to 75 DEG C, putting 5 to 10 parts of weak chain transferring agent, 2.5 to 5.0 parts of organic peroxide initiator, 7.5 to 12.5 parts of unsaturated dicarboxylic acid and 25 to 40 parts of acrylic acid at a time; after the materials are added at a time, starting to dropwise add a mixed solution of 50 to 80 parts of acrylic acid and 1.2 to 3.5 parts of strong chain transferring agent, and adding an azoic initiator at two times in the dropwise adding process; after finishing the dropwise adding, curing for 1 to 2 hours, adding 7.5 to 16.0 parts of neutralizing agent, stirring uniformly, and slicing after cooling to obtain a finished product. The solid flaky polycarboxylate water-reducer is convenient to store, is low in long-distance transportation cost, is completely water-soluble, and is suitable for cement-based binding materials in civil engineering.
Owner:HUBEI UNIV OF TECH

Electrochemical method of oil removal of wastewater produced in oil extraction by polymer flooding displacement

The invention discloses an electrochemical method of oil removal by polymer flooding oil recovery wastewater, which comprises the following steps of: 1, electrolysis; 2, sedimentation. In the process of the electrolysis, tiny oil droplets in the wastewater lose electrons due to discharge on the surface of an anode, charges on the surface of the oil droplets are reduced, and electric potential of interface xi is decreased; and residual polymer pieces in the wastewater after the electrolysis are oxidized and degraded, viscosity of the wastewater is decreased, and water film intensity on the interface of oil/water is reduced. Therefore, the tiny oil droplets after the electrolysis are liable to be converged into large oil droplets and are rapidly separated from the wastewater under the action of cathode hydrogen. As treated by the method, crude oil in wastewater produced in oil extraction by polymer flooding displacement is quite easy for removal with no need for large use of sedimentation tanks, thus saving construction fund for oilfield; the invention has simple process, requires no drug, saves resource and cost and conforms to green chemistry process, quality of the wastewater after the oil removal is obviously crystal-clear; in addition, the device is convenient and safe in operation, easy to control and realize automation, extensively adapted to the amount of water, and convenient for popularization and application.
Owner:SOUTH CHINA UNIV OF TECH
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