Patents
Literature
Patsnap Eureka AI that helps you search prior art, draft patents, and assess FTO risks, powered by patent and scientific literature data.

116 results about "Compound organic" patented technology

Organic compound, any of a large class of chemical compounds in which one or more atoms of carbon are covalently linked to atoms of other elements, most commonly hydrogen, oxygen, or nitrogen. The few carbon-containing compounds not classified as organic include carbides, carbonates, and cyanides.

Oil and gas well blocking remover and preparation method thereof

The invention belongs to the technical field of oil and gas development, and particularly relates to an oil and gas well blocking remover and a preparation method thereof. The blocking remover comprises the following components: 5-8% of low-carbon composite organic acid, 5-7% of fluoboric acid, 6-9% of ammonium bifluoride, 4-6% of an anti-acid sludge mutual solvent, 2-4% of a corrosion inhibitor, 2-4% of polyoxypropylene polyoxyethylene propylene glycol ether, 8-12% of a permeation dispersion surfactant, 2-5% of a sulfur dissolving agent, 2-5% of a stable chlorine dioxide solution and the balance of water. The preparation method comprises the following steps: adding the low-carbon composite organic acid, the fluoboric acid and the ammonium bifluoride into water and stirring; adding an acid sludge resisting mutual solvent and a sulfur dissolving agent, and stirring; adding the corrosion inhibitor, the polyoxypropylene polyoxyethylene propylene glycol ether and the permeation dispersion surfactant, and stirring; and finally, reducing the stirring speed, adding the stable chlorine dioxide solution, and stirring to uniformly mix. The blocking remover provided by the invention is comprehensive in blocking removal function, very good in dissolving and dispersing performance on complex blocking substances, very small in corrosion damage to a shaft pipe wall and wide in applicability.
Owner:CHENGDU XINMING CHEM CO LTD

Method for efficiently extracting lithium by roasting lepidolite at low temperature by using composite organic acid

The invention relates to a method for efficiently extracting lithium by roasting lepidolite at low temperature by using composite organic acid. The invention relates to a method for efficiently extracting lithium by roasting lepidolite at low temperature by using composite organic acid, which comprises the following steps of: adding an activating agent into lepidolite concentrate, and pre-activating to obtain activated lepidolite concentrate powder; the lepidolite concentrate powder and a composite organic acid roasting agent are mixed, acidified and roasted, and a roasted product is obtained; adding water into the roasted product for leaching, and carrying out suction filtration to obtain a lithium-containing leachate; the composite organic acid roasting agent at least comprises methanesulfonic acid. According to the method, the problem that the lithium ion extraction efficiency is low due to the fact that the TOT layered structure in the lepidolite is difficult to damage is solved, and the problem that the lithium ion extraction efficiency is low due to the fact that Si-O bonds with high bond energy in an existing lepidolite crystal framework are difficult to dissociate is also solved.
Owner:YICHUN JIANGLI LITHIUM BATTERY NEW ENERGY IND RES INST +1

Halogen-free soldering flux for solder paste and preparation method of halogen-free soldering flux

The invention relates to the technical field of solder paste, in particular to halogen-free soldering flux for solder paste and a preparation method of the halogen-free soldering flux. The halogen-free soldering flux for the solder paste comprises the following raw materials in parts by mass: 20-40 parts of hydrogenated rosin, 1-5 parts of maleic anhydride, 0.1-0.4 part of p-toluenesulfonic acid, 1-5 parts of activated mesoporous silica, 10-20 parts of a composite organic acid active agent, 5-10 parts of a thixotropic agent, 1-3 parts of a tackifier, 1-2 parts of a pH regulator, 1-2 parts of a surfactant, 1-2 parts of a chelating agent, 1-2 parts of an antioxidant and 50-80 parts of an organic solvent. Through the innovative component design and the preparation process, the technical contradiction existing in the field of halogen-free scaling powder for a long time is effectively solved, and an ideal material solution is provided for high-reliability electronic packaging.
Owner:SHENZHEN TONGFANG ELECTRONGIC NEW MATERIAL CO LTD

Synthesis and oxygen reduction application of metal cluster / polyphthalocyanine network compounded organic electrocatalytic material

The invention provides synthesis and oxygen reduction application of a metal cluster / polyphthalocyanine network compounded organic electrocatalytic material. The preparation method comprises the following steps: by taking benzene ring-containing anhydride, chlorate and urea as raw materials, carrying out high-temperature reaction, cooling, and purifying for multiple times, so as to obtain an edge-functionalized polyphthalocyanine network precursor; dispersing the obtained polyphthalocyanine network precursor into a solution A by using a proper solvent; meanwhile, trifluoroacetate and a tert-butyl metal compound are mixed in a proper solvent to form a metal cluster, and the metal cluster compound is dissolved in the solvent to form a solution B; and mixing the two solutions, standing overnight, filtering, purifying, and carrying out ball milling treatment to finally obtain the target metal cluster / polyphthalocyanine network composite organic catalyst. The polyphthalocyanine oxygen reduction organic catalytic material designed by the invention is low in raw material cost and simple to prepare. The test shows that the half-wave potential of the material is 100 mV higher than that of Pt / C, the E1 / 2 reduction value is 30 mV lower than that of Pt / C after accelerated aging for 2500 circles, and the material has high activity and high stability and can be applied to devices such as lithium batteries and fuel batteries related to the oxygen reduction process.
Owner:LANZHOU JIAOTONG UNIV

Iron-based bimetallic catalyst as well as preparation method and use method thereof

The invention discloses an iron-based bimetallic catalyst as well as a preparation method and a use method thereof. The iron-based bimetallic catalyst comprises an active metal; the composite carrier comprises zirconium oxide, a zirconium-based organic framework and an iron-based organic framework, the zirconium-based organic framework is coated with the iron-based organic framework, and iron and the active metal are loaded on the zirconium oxide. The preparation method comprises the following steps: mixing zirconium nitrate pentahydrate and a first organic ligand for reaction to obtain a zirconium-based organic framework material; mixing the zirconium-based organic framework material, a second organic ligand and a metal salt for reaction to prepare a composite organic framework material; calcining the composite organic framework material, and soaking the calcined composite organic framework material in a metal salt solution; and carrying out drying treatment to obtain the iron-based bimetallic catalyst. The iron-based bimetallic catalyst is used for the catalytic reaction of carbon dioxide hydrogenation to generate low-carbon olefins.
Owner:EAST CHINA UNIV OF SCI & TECH

Indolocarbazole compound, perovskite solar cell and preparation method

The invention discloses an indolocarbazole compound, a perovskite solar cell and a preparation method, and belongs to the technical field of perovskite solar cells, the indolocarbazole compound provided by the invention is an organic small molecule material and has an asymmetric molecular structure, and an asymmetric conjugated structure system of the indolocarbazole compound enhances the molecular dipole moment and improves the photoelectric conversion efficiency. And the energy level matching is optimized. Meanwhile, benzene ring groups on side chains of molecules of the organic hole transport layer can further inhibit excessive aggregation of the molecules, uniform coverage is achieved, and efficient transport of carriers is achieved. Therefore, when the indolocarbazole compound organic small molecule material is used as a hole transport layer material for a perovskite solar cell, the energy levels of the highest occupied molecular orbital HOMO and the lowest unoccupied molecular orbital LUMO of the indolocarbazole compound organic small molecule material provided by the invention can be well matched with the energy level of an active layer material; therefore, the collection efficiency of current carriers is greatly improved, and the filling factor and the photoelectric conversion efficiency are improved.
Owner:ZHONGMAO LVNENG TECH (XIAN) CO LTD

Environment-friendly polyaluminum chloride flocculant

The invention relates to the technical field of flocculants, in particular to an environment-friendly polyaluminum chloride flocculant, which adopts modified aluminum oxide as a core component, improves the dispersibility and stability of the flocculant in water through a technology of coating an organosilicon compound on the surface, reduces the pollution to the environment, and meanwhile, improves the flocculating efficiency of the flocculant. The addition of the composite organic high-molecular polymer enhances the flocculation effect, increases the floc settling velocity and reduces the risk of secondary pollution, and in addition, the introduction of the natural mineral substance-nano composite material not only improves the adsorption performance of the flocculant, but also can decompose organic pollutants under the illumination condition to realize deep purification, and has good application prospects. Therefore, the environment-friendly polyaluminum chloride flocculating agent provided by the technical scheme effectively solves the problem of environmental pollution in the production and use processes of the traditional polyaluminum chloride flocculating agent.
Owner:CHONGQING YUJIE CHEM

Saline-alkali soil conditioner based on two tailing-based composite organic matters and preparation method of saline-alkali soil conditioner

The invention discloses a saline-alkali soil conditioner based on two tailing-based composite organic matters and a preparation method of the saline-alkali soil conditioner. The saline-alkali soil conditioner is prepared from iron tailings, molybdenum tailings, optimized wormcast organic matters, wood vinegar and ammonium sulfate according to the part ratio of 20: 15: 5: 1: 1. According to the method, the low-molecular organic acid is adopted to fully consider the synergistic utilization of the two tailings, so that mineral solid wastes are effectively reduced, the content of organic matters and trace elements necessary for plants in the saline-alkali soil is remarkably increased, the soil structure is adjusted, the salinity and alkalinity are reduced, the soil environment is remarkably improved, and the growth condition of the plants is improved; the soil conditioner has a good improvement effect on medium-low saline alkali soil. The main raw materials of the modifier belong to mineral industry solid wastes, the used raw materials are easy to obtain, low in cost and free of pollution, the technical scheme is simple and easy to operate and convenient to implement, and rationalized and resource pollution-free comprehensive utilization of the solid wastes is achieved.
Owner:NORTH CHINA UNIVERSITY OF SCIENCE AND TECHNOLOGY

Production method for improving ethanol yield by treating corn straw with organic acid

The invention relates to a production method for improving the yield of ethanol by treating corn straws with organic acid, the corn straws treated with organic acid are subjected to segmented heat treatment by adopting a composite acid solution consisting of citric acid and acetic acid, and the segmented heat treatment comprises the following steps: firstly, carrying out heat treatment at 40-60 DEG C for 0.5-1 hour, and then, heating to 70-90 DEG C, and carrying out heat treatment for 1.5-2.5 hours. According to the method, the corn straw is pretreated by adopting the composite organic acid, so that the degradation efficiency of lignocellulose in the corn straw is effectively improved, more cellulose is reserved, meanwhile, the generation of toxic inhibitors is reduced, the inhibition effect on cellulase and yeast in the subsequent enzymolysis and fermentation process is reduced, and the yield of the corn straw is improved. And the yield of the prepared oxygen-containing organic compound ethanol is improved.
Owner:JILIN AGRICULTURAL UNIV

Ultrafiltration separation device and method for water body containing fluorinated alkyl substances

The invention discloses an ultrafiltration separation device and method for a water body containing fluorinated alkyl substances, and belongs to the field of water treatment. The method comprises the following steps: S1, mixing a water body containing a fluorinated alkyl substance with a cationic surfactant solution, stirring, and standing to form a composite solution containing a compound; s2, the composite solution is subjected to membrane separation through an ultrafiltration membrane, and percolation effluent is obtained. According to the embodiment of the invention, the cationic surface active agent is mainly used for inducing the pollutants to be self-assembled into the compound with larger particle size, so that the pollutants can be effectively intercepted by the ultrafiltration membrane with larger pore size, and the problem that the traditional ultrafiltration membrane is difficult to treat small-molecule pollutants is solved. The separation method has the advantages of simplicity and convenience in operation, low energy consumption, high applicability and the like, and is suitable for the processes of pretreatment, concentration recovery and the like of perfluorinated and polyfluoroalkyl compound organic pollutants in wastewater.
Owner:UNIV OF SCI & TECH OF CHINA

Organic acid excited solid waste-based cementing material

The invention provides an organic acid excited solid waste-based cementing material, and belongs to the technical field of solid waste utilization. The solid waste-based cementing material excited by the organic acid comprises 90-105 parts by mass of a silicon-aluminum solid waste base material, 7-12 parts by mass of sulfate and 15.3-19.8 parts by mass of a composite organic acid exciting agent, wherein the composite organic acid exciting agent comprises main acid and polyacrylic acid, and the mass of the polyacrylic acid is 10%-40% of the mass of the main acid; the main acid is one or a mixture of citric acid and tartaric acid. According to the organic acid excited solid waste-based cementing material, strong base is prevented from being adopted as an exciting agent, and the defects of a strong base excitation system are avoided.
Owner:XIAN YINDING TECH CO LTD +1

Green and efficient purification method of high-purity quartz sand

The invention relates to the technical field of quartz sand purification, in particular to a green and efficient purification method of high-purity quartz sand, which comprises four steps of mechanical-chemical synergistic pretreatment, microwave-assisted deep impurity removal, directional adsorption purification and ultrapure water washing and drying. The traditional hydrofluoric acid process is replaced by the composite organic acid, so that the COD (Chemical Oxygen Demand) of the wastewater is reduced by more than 90%, the waste liquid treatment cost is greatly reduced, meanwhile, the problem of corrosion of strong acid to equipment is avoided, the energy consumption is reduced by 40% through the microwave process, and no chlorine is discharged, so that the production process is more environment-friendly and safer, the content of Al2O3 is reduced from 500ppm to 8ppm, and the production cost is reduced. Compared with the prior art, the method provided by the invention has the advantages that the content of Fe2O3 is reduced from 200ppm to 3ppm, meanwhile, the inclusion removal rate is greater than 99.5%, and the purity of SiO2 reaches 99.995%, so that the problem that micron-sized inclusion impurities are difficult to deeply remove is solved, and the purification efficiency is greatly improved.
Owner:HENAN XINXIN SILICON-BASED NEW MATERIALS CO LTD

Method for fully extracting and removing aluminum, calcium and magnesium and recovering nickel from waste hydrogenation catalyst pickle liquor

The invention discloses a method for removing aluminum, calcium and magnesium and recovering nickel from waste hydrogenation catalyst pickle liquor through complete extraction, and belongs to the technical field of hydrometallurgy. A method for removing aluminum, calcium and magnesium and recovering nickel from waste hydrogenation catalyst pickle liquor through complete extraction comprises the following steps that S1, the waste hydrogenation catalyst pickle liquor containing nickel, aluminum, calcium and magnesium is taken, the pH of the pickle liquor is adjusted, first-stage multi-stage counter-current extraction is conducted through a composite organic extraction phase, and an aluminum-loaded organic phase and aluminum-removed raffinate are obtained; s2, adjusting the pH value of the aluminum removal raffinate, and carrying out second-stage multi-stage counter-current extraction by adopting a composite organic extraction phase to obtain a calcium and magnesium loaded organic phase and a purified nickel sulfate solution; s3, the purified nickel sulfate solution is subjected to evaporative crystallization, and a nickel sulfate product is obtained; wherein the composite organic extraction phase comprises a main extraction agent, a synergistic extraction agent A and a synergistic extraction agent B; the method has the advantages of being high in nickel recovery rate, thorough in impurity removal, short in technological process, free of slag dust pollution and the like.
Owner:INSTITUTE OF PROCESS ENGINEERING CHINESE ACADEMY OF SCIENCES +1

A weather-resistant, high-hardness composite anti-corrosion coating and its preparation method

This invention discloses a weather-resistant, high-hardness composite anti-corrosion coating and its preparation method, belonging to the field of anti-corrosion coating technology. The preparation method includes: firstly, synthesizing an epoxy resin containing dynamic disulfide bonds by reacting dithiodibenzoic acid and epichlorohydrin in an alkaline aqueous phase; secondly, constructing a low surface energy siloxane network using hydroxyl-terminated polydimethylsiloxane and methyltriethoxysilane; subsequently, introducing chlorzoxazone and N-acetyl-p-aminophenol as composite organic corrosion inhibitors, blending them with the resin to obtain a composite base material; finally, adding graphene, carbon nanotubes, and inorganic anti-corrosion fillers, and cross-linking and curing to form a film using a polyamine curing agent. This invention suppresses microcracks through the dynamic stress relief of disulfide bonds, combined with the weather-resistant barrier of the siloxane network, the active interface passivation of the heteroatom corrosion inhibitor, and the three-dimensional synergistic mechanical bonding of carbon-based nanomaterials, achieving a perfect unity of ultra-strong corrosion resistance, excellent weather resistance, and high mechanical hardness in the coating.
Owner:ZENGCHENG BOYA CHEM CO LTD

Preparation method of nitrogen-doped coal-based carbon material for methane enrichment

The invention discloses a preparation method of a nitrogen-doped coal-based carbon material for methane enrichment, and belongs to the technical field of carbon materials for gas separation. The method comprises the following steps: carrying out controlled change on a coal structure through pretreatment of composite organic acid, mixing biomass waste as a nitrogen source with pretreated coal, and carrying out pyrolysis to obtain a nitrogen-doped coal-based crude product; and mixing the nitrogen-doped coal-based crude product with an activating agent, and activating in a nitrogen atmosphere to obtain the nitrogen-doped coal-based carbon material. Through pretreatment, chemical bonds in organic macromolecules in the coal are broken, the pore structure of the coal is improved, and the carbon element is enriched; the composite organic acid is used as a pickling agent, the biomass waste is used as a nitrogen source for nitrogen doping, use of a traditional high-energy-consumption chemical nitrogen source is reduced, pretreated coal and the nitrogen source are co-pyrolyzed to provide more micropores and channels for the carbon material, and the adsorption performance of the carbon material is obviously improved; the preparation process is simple and effective, and green preparation of the nitrogen-doped coal-based carbon material is realized.
Owner:TAIYUAN UNIVERSITY OF TECHNOLOGY

Process for the preparation of a foamed copper-based composite organic compound layer catalytic material

This invention provides a method for preparing a foamed copper-based composite organic compound layer catalytic material, comprising the following steps: forming 8-hydroxyquinoline molybdenum (Mo(C)) on the surface of a foamed copper matrix. 9 H 6 NO) 4 Organic compound layer; 8-hydroxyquinoline molybdenum (Mo(C)) 9 H 6 NO) 4 The organic compound layer is converted into phthalimide 8-hydroxyquinoline molybdenum (C). 8 H 4 NO 2 ) 2 (C 9 H 6 NO) 2 ; Phthalimide 8-hydroxyquinoline molybdenum Mo(C) 8 H 4 NO 2 ) 2 (C 9 H 6 NO) 2 Conversion to copper phthalimide / 8-hydroxyquinoline molybdenum Cu(C) 8 H 4 NO 2 ) 2 / Mo(C 9 H 6 NO) 2 The foamed copper-based composite organic compound layer catalytic material is finally obtained. The catalytic material prepared by the method of this invention can effectively improve the Faradaic efficiency, ammonia selectivity, production rate, and nitrate removal rate of the electrochemical reduction of nitrate to ammonia technology.
Owner:NORTH CHINA UNIVERSITY OF TECHNOLOGY

A method for extracting complex organic acids from a waste liquid produced from a raspberry extract

The present application provides a method for extracting complex organic acid from the waste liquid of the extract of Rubus corchorifolius L.f. The waste liquid of the column chromatography effluent of the Rubus corchorifolius L.f. extract is taken, the specific gravity of the secondary waste liquid is adjusted to obtain the column loading liquid, the column loading liquid is passed through a resin column A, water washing is performed, the column effluent and the water washing liquid are collected to obtain a combined liquid 1, the combined liquid 1 is passed through a resin column B, water washing is performed, reagent C is used for elution, and the eluate is collected. The combined liquid 2 is obtained by passing through a resin column D and collecting the effluent and the water washing liquid, vacuum concentration is performed, crystallization is performed, and filtration is performed to obtain quinic acid.
Owner:TIANJIN JIANFENG NATURAL PROD RES & DEV CO

Preparation method of water-retention expanded compound organic fertilizer

The invention discloses a preparation method of a water-retention expanded compound organic fertilizer, and relates to a preparation method of a compound organic fertilizer. The invention aims to solve the problem that the existing organic fertilizer has poor water retention or water storage capacity after improving soil. The preparation method comprises the following steps: carrying out hydrophobic treatment on attapulgite and humic acid, carrying out functional modification on the attapulgite by utilizing active functional groups such as carboxyl and phenolic hydroxyl of the humic acid, and compounding with an acrylic acid-acrylamide copolymer, a modified expanding agent, the humic acid, mushroom bran and the attapulgite to form the water-retaining expanded composite organic fertilizer. The surface of calcium carbide in the modified expanding agent is provided with a coating layer formed by xanthan gum, and after the modified expanding agent is applied to soil, the gel generates volume expansion, so that the water storage space is increased, and the water storage capacity is further improved. Due to the use of the expanding agent, the use amount of the acrylic acid acrylamide copolymer is remarkably reduced, the cost is remarkably reduced, and the expanding agent has relatively good practicability and can be popularized.
Owner:JILIN SONGLING ORGANIC FERTILIZER TECH CO LTD +1

Composite phosphorus locking agent for water body and preparation method of composite phosphorus locking agent

The invention discloses a water body composite phosphorus locking agent and a preparation method thereof, and belongs to the technical field of water quality treatment. The composite phosphorus locking agent for the water body comprises the following raw material components in parts by weight: 0.5-1.5 parts by mass of modified zirconium hydroxide, 4 parts by mass of sodium alginate, 2.3-2.5 parts by mass of a composite organic material, 6 parts by mass of calcium chloride and 1-3 parts by mass of ferric trichloride, the modified zirconium hydroxide is obtained by modifying zirconium hydroxide with epoxy chloropropane; the composite organic material is prepared from diethanol amine and chitosan; the water body composite phosphorus locking agent prepared by the method is relatively high in phosphorus removal rate.
Owner:CHINESE ACAD OF ENVIRONMENTAL PLANNING

Water-based drilling fluid high-temperature-resistant plugging agent as well as preparation method and device thereof

The invention belongs to the technical field of drilling fluid plugging agents, and particularly relates to a water-based drilling fluid high-temperature-resistant plugging agent and a preparation method and device thereof.The water-based drilling fluid high-temperature-resistant plugging agent is prepared from, by weight, 20-30 parts of walnut shell powder, 10-20 parts of calcium silicate, 5-10 parts of mica sheets, 10-17 parts of a structure reinforcing agent, 1-3 parts of a dispersing agent and 1-2 parts of a lubricating agent. The structure reinforcing agent is composed of 5-10 parts of a fiber material and 5-7 parts of sodium silicate, the dispersing agent is a phosphate dispersing agent, and the lubricating agent is a silane compound lubricating agent; sodium silicate has high thermal stability and can maintain good structure and function at high temperature, the plugging agent can adapt to the environment with high stability, the dispersing agent and the lubricating agent are used for improving the dispersity and fluidity of the plugging agent, the plugging agent is helped to play a role under different operation conditions, and the plugging agent has good application prospects. The plugging agent is prepared by compounding the organic raw materials and the inorganic raw materials, so that the high-temperature-resistant and plugging effects of the plugging agent are enhanced.
Owner:RYAN INT OIL&GAS ENG TECH SERVICE LTD

Device for observing dissolution phenomenon of compound organic fertilizer

The utility model relates to the technical field of dissolution phenomenon observation, in particular to a compound organic fertilizer dissolution phenomenon observation device which comprises a dissolution barrel, a rotating shaft is vertically and rotatably mounted in the dissolution barrel, a plurality of rectangular plates are symmetrically and fixedly mounted on the rotating shaft, a rectangular groove is formed in one end of each rectangular plate, and a plurality of rectangular grooves are formed in the other end of each rectangular plate. A rectangular groove is formed in the upper end of the rotating shaft, a stirring plate is inserted into the rectangular groove, cross rods are symmetrically, horizontally and fixedly mounted on the rotating shaft, moving grooves are formed in one ends of the cross rods, moving rods are mounted in the moving grooves, connecting rods are fixedly mounted at one ends of the two moving rods, a cylindrical groove is formed in the upper end of the rotating shaft, and a gas injection assembly is arranged at the upper end of the rotating shaft. Through mutual cooperation of the gas injection assembly, the rotating shaft, the transverse rod, the moving rod and the connecting rod, the contact area between the stirring plate and the rectangular plate and a solution is changed, experimental data between the organic fertilizer dissolution rate and the contact area between the stirring plate and the rectangular plate and the solution are obtained, and experiments are diversified.
Owner:HEILONGJIANG FUDISHENG AGRICULTURAL SCIENCE & TECHNOLOGY DEVELOPMENT CO LTD

Method for efficiently extracting lithium from lepidolite by low-temperature calcination with composite organic acid

The present application relates to a kind of composite organic acid low-temperature calcination lepidolite high-efficiency lithium extraction method.Composite organic acid low-temperature calcination lepidolite high-efficiency lithium extraction method includes the following steps: adding activating agent to lepidolite concentrate, pre-activation treatment, obtain the activated lepidolite concentrate powder;Lepidolite concentrate powder is mixed with composite organic acid calcining agent acidification calcination, obtain the calcination product;Water is added to the calcination product and leaching, suction filtration, obtain the lithium-containing leaching solution;Composite organic acid calcining agent at least includes methyl sulfonic acid.The present application solves the problem that TOT layered structure in lepidolite is difficult to destroy, resulting in low lithium ion extraction efficiency, also solves the problem that Si-O bond in the existing lepidolite crystal framework is difficult to dissociate, resulting in low lithium ion extraction efficiency.
Owner:YICHUN JIANGLI LITHIUM BATTERY NEW ENERGY IND RES INST +1

High-damping organic silicon-based composite hydrogel as well as preparation method and application thereof

The invention belongs to the technical field of functional composite materials, and particularly relates to high-damping organic silicon-based composite hydrogel as well as a preparation method and application thereof. The method comprises the following steps: mixing polydimethylsiloxane, silicate ester and a polyvinyl alcohol aqueous solution in proportion, and emulsifying in an ultrasonic microreactor to form an oil-in-water emulsion with specific particle size distribution. Wherein after the oil phase in the emulsion is subjected to ultrasonic action, rapid chemical crosslinking is performed to form organic silicon microspheres, and finally the organic silicon-based composite water-based damping material with the damping factor larger than 0.5 is prepared. By regulating and controlling the particle size distribution of the organic silicon microspheres, the stacking density of the microspheres in the damping material is maximized, so that the friction between the microspheres and a gel network is enhanced, and high damping is realized. The elastic composite organic silicon material has good damping performance, molding processability, recoverability and biocompatibility, raw materials are environment-friendly and low in cost, and the elastic composite organic silicon material is suitable for large-scale production and can be widely applied to the fields of flexible wearing, elastic vibration isolation, flexible protection and the like.
Owner:SHANTOU UNIV

A composite organic acid catalyst for acetate production and a preparation method and application thereof

The application relates to the technical field of catalysts, and discloses a composite organic acid catalyst for acetate production, a preparation method and application thereof.The composite organic acid catalyst for acetate production comprises silica-supported organic acid; the silica-supported organic acid is silica-supported methyl sulfonic acid and silica-supported alkane disulfonic acid; and the mass ratio of the silica-supported methyl sulfonic acid and the silica-supported alkane disulfonic acid is 1.5:0.4-1.4.Through the technical scheme, the problem that the yield of acetate is not high due to the insufficient catalytic effect of the solid acid catalyst in the prior art is solved.
Owner:ZHONGRONG TECH CORP LTD

Fermentation medium for producing mycophenolic acid and fermentation method

The fermentation medium for producing mycophenolic acid comprises methionine, a carbon source and a nitrogen source, and the nitrogen source does not comprise a composite organic nitrogen source. According to the fermentation medium and the fermentation method disclosed by the invention, the titer of producing mycophenolic acid by utilizing penicillium brevicompactum is obviously improved, especially when the concentration of methionine is 1.5 g / L, the fermentation titer can be improved to 9214 mu g / mL, and the fermentation titer can reach 13506 mu g / ml due to the development of a feeding process.
Owner:HANGZHOU ZHONGMEI HUADONG PHARMACEUTICAL CO LTD

Compound substrate for ecological restoration of side slope as well as preparation method and application of compound substrate

The invention discloses a compound matrix for ecological restoration of a side slope as well as a preparation method and application of the compound matrix, and belongs to the technical field of geotechnical engineering and ecological restoration. The composite substrate for ecological restoration of the side slope is prepared from the following raw materials in parts by mass: 20 to 40 parts of mining area coal gangue crushed materials, 15 to 30 parts of fly ash, 20 to 35 parts of soil, 8 to 15 parts of organic fertilizer, 0.3 to 1.0 part of water-retaining agent and 1.5 to 4 parts of binder. The high-performance slope ecological restoration material is constructed by taking coal gangue, fly ash and soil in a mining area as main frameworks and compounding an organic fertilizer, a water-retaining agent and an organic-inorganic hybrid gel binder. The method has the core advantages that high-valued resource utilization of industrial solid waste is achieved, the cost of matrix raw materials and dependence on high-quality cultivation soil are remarkably reduced, and the method has both environmental and economic benefits.
Owner:HUAINAN MINING IND GRP +2

Water-soluble organic suspended silicon liquid fertilizer and preparation method thereof

The present application relates to the technical field of agricultural liquid fertilizer, and specifically relates to a water-soluble organic suspended silicon liquid fertilizer, which is composed of a silicon source, a compounded organic carrier, a composite dispersion stabilizer, a defoaming agent and water; the compounded organic carrier comprises humic acid and amino acid; the composite dispersion stabilizer comprises sodium lignosulfonate and xanthan gum; the silicon source comprises potassium silicate; the weight of each component is as follows: potassium silicate 6-12 parts, humic acid 3-5 parts, amino acid 2-3 parts, sodium lignosulfonate 0.8-1.5 parts, xanthan gum 0.3-0.5 parts, defoaming agent 0.08-0.12 parts, and water is supplemented to 100 parts. The present application is designed in cooperation with the compounded organic carrier and the composite dispersion stabilizer, the organic carrier and the silicon source form a stable complex structure, the composite dispersion stabilizer inhibits the agglomeration of silicon particles through component cooperation, and a low-temperature aging process is matched, so that the suspension stability of the product is greatly improved.
Owner:YUNNAN JINSUI AGRI MEANS OF PROD CO LTD

Composite nanofiltration membrane regulated and controlled by amino acid modified gamma-cyclodextrin as well as preparation method and application of composite nanofiltration membrane

The invention belongs to the technical field of nanofiltration membrane preparation, and particularly relates to an amino acid modified gamma-cyclodextrin regulated composite nanofiltration membrane as well as a preparation method and application thereof. Comprising the following steps: dissolving an amine compound, amino acid and gamma-cyclodextrin in a solvent, and mixing to obtain a water-phase composite solution; placing the water-phase composite solution on the surface of the base membrane, and performing in-situ deposition to obtain a primary membrane; placing an acyl chloride compound organic phase solution on the surface of the primary membrane, performing interfacial polymerization to obtain a composite nanofiltration membrane precursor, and performing heat treatment to obtain the amino acid modified gamma-cyclodextrin regulated composite nanofiltration membrane. A polyacrylonitrile membrane is used as a substrate, amino acid, gamma-cyclodextrin and polyethyleneimine are coupled to obtain a water-phase composite solution, the water-phase composite solution reacts with 1, 3, 5-benzoyl chloride by adopting an interfacial polymerization method, and the obtained polyacrylonitrile nanofiltration membrane has excellent rejection rate of metal cations with different valence states and specific separation performance and can be used for preparing a high-performance membrane. And the method has a wide prospect in the aspects of resource recycling and reutilization of the lithium slag.
Owner:JINGGANGSHAN UNIVERSITY +1

Multi-granularity iron tailings composite organic matrix, and preparation method and application thereof

The application discloses a kind of multi-particle grade iron tailings composite organic matrix and its preparation method and application, belong to the technical field of composite organic matrix, the application uses multi-particle grade tailings (fine tailings, total tailings and fine tailings) Collaborative compound agricultural organic matter, by the gradation optimization of coarse and fine particles, build stable, continuous pore structure, realize the collaborative improvement of aeration and water retention capacity;At the same time, using the adsorption and buffering effect of organic matter, effectively dilute the soluble salt concentration in the matrix, reduce the risk of salt stress, create a suitable environment for plant growth. With the increase of total tailings / fine tailings ratio, the matrix conductivity decreases, the bulk density increases, the aeration porosity improves, and the water holding porosity remains relatively stable, indicating that the ratio of multi-particle grade tailings can improve the physical and chemical properties of the matrix.
Owner:ANHUI MASTEEL MINING RESOURCES GRP NANSHAN MINING CO LTD

Preparation method of foamy copper-based composite material with photothermal effect

The invention provides a preparation method of a foamy copper-based composite material with a photothermal effect. The preparation method comprises the following steps: (1) loading a nickel atom modified polydopamine / aniline composite organic matter on the surface of a foamy copper matrix; (2) converting the nickel atom modified polydopamine / aniline composite organic matter on the surface of the foamy copper matrix into a Ni (PDA) 2 (PANI) 2 coordination polymer; and (3) loading a CeCo2Fe16O27 crystal on the surface of the Ni (PDA) 2 (PANI) 2 coordination polymer. The foamy copper-based composite material prepared by the method disclosed by the invention has an excellent photothermal effect and can efficiently activate peracetic acid to degrade metronidazole sewage.
Owner:NORTH CHINA UNIVERSITY OF TECHNOLOGY