The invention relates to a method for preparing a flower-shaped
copper sulfide (CuS)
nanocrystal, which comprises the following steps of: dissolving a dissoluble
copper salt into deionized water to obtain a solution A; adding sulfourea into the solution A to obtain a solution B; adding hexadecyl trimethyl
ammonium bromide into the solution B to form a precursor solution C; pouring the precursor solution C into a
microwave hydrothermal reaction kettle, sealing the reaction kettle, putting the reaction kettle into a
temperature and pressure dual-control
microwave hydrothermal reactor, and carrying out natural cooling to
room temperature after the reaction is finished; and opening the
hydrothermal reaction kettle, carrying out centrifugal collection on a product, then, washing the production by respectively using deionized water and absolute
alcohol, and
drying to obtain the flower-shaped
copper sulfide nanocrystal. According to the method for preparing the flower-shaped
copper sulfide nanocrystal, flower-shaped
copper sulfide nanocrystals with different grain sizes are prepared through changing the concentration of an added surfactant, i.e. the hexadecyl trimethyl
ammonium bromide, the grain size controllable preparation of the flower-shaped
copper sulfide nanocrystals is achieved, and then, copper
sulfide semiconductor materials with different optical and electrical properties are prepared; and CuS grains prepared by the method are of a flower-shaped structure formed by assembling flake-shaped crystals with the thickness of 20-50 nm, so that the CuS grains have larger surface areas and can be applied to the catalytic field.