The invention relates to the field of materials, and particularly discloses
metal-phase
molybdenum disulfide, a self-supporting
electrode, preparation methods and application. The
metal-phase
molybdenum disulfide comprises the following raw materials:
molybdenum trioxide (serving as a molybdenum source), a
sulfur source, a proper amount of a
reducing agent and a proper amount of water, wherein a ratio of the number of molybdenum atoms in the
molybdenum trioxide to the number of
sulfur atoms in the
sulfur source is 1: (5-40). According to the
metal-phase
molybdenum disulfide provided by an embodiment of the invention,
molybdenum trioxide is adopted as the molybdenum source,
hydrothermal synthesis from a proper amount of the sulfur source, the
reducing agent and the water is carried out to prepare the metal-phase
molybdenum disulfide, and the content of the metal-phase
molybdenum disulfide in the product is high; and the preparation method of the metal-phase molybdenum disulfide providedby the invention has the advantages of simplicity and safety in operation, short preparation period and suitability for large-scale production, solves the problems of long preparation period and lowsafety due to the fact that most of conventional metal-phase molybdenum disulfide is synthesized through
lithium ion delamination, and has wide market prospects.