Patents
Literature
Patsnap Eureka AI that helps you search prior art, draft patents, and assess FTO risks, powered by patent and scientific literature data.

214 results about "Free acid" patented technology

Process for racemizing and isolating atropisomers of 7-chloro-6-fluoro-1-(2-isopropyl-4-methylpyridin-3-yl)pyrido[2,3-d]pyrimidine-2,4(1h,3h)-dione

Provided herein is a process comprising heating a composition comprising (P)-compound A or a salt thereof and a solvent to a temperature of 250° C. to 350° C. to form racemized compound A. Also provided is a process for isolating (P)-compound A from a composition comprising (P)-compound A and a tartrate, as described herein. Further provided herein, is a process for isolating a free acid of a tartrate or a hydrate thereof from a composition comprising a tartrate, (P)-compound A, and an organic solvent.
Owner:AMGEN INC

Compositions and methods for keto stacking with beta-hydroxybutyrate and acetoacetate

Compositions for delivering ketone bodies to a subject include one or more beta-hydroxybutyrate salts, one or more acetoacetate salts, beta-hydroxybutyric acid, and optionally acetoacetic acid. The compositions may optionally include one or more ketone body esters, such as one or more beta-hydroxybutyrate esters and / or one or more acetoacetate esters. An example composition contains about 2% to about 98% on a molar basis of the one or more beta-hydroxybutyrate salts and the one or more acetoacetate salts, about 2% to about 98% on a molar basis of the beta-hydroxybutyrate free acid and optionally the acetoacetate free acid, and optionally about 2% to about 98% on a molar basis of one or more ketone body esters.
Owner:AXCESS GLOBAL SCIENCES LLC

Tin-silver alloy electroplating solution, preparation method and application thereof, and electroplating method

ActiveCN119800461ACellsActive agentAlloy
The invention relates to the field of electroplating, and discloses a tin-silver alloy electroplating solution as well as a preparation method and application thereof and an electroplating method, and the electroplating solution comprises soluble stannous salt, soluble silver salt, a composite surfactant, free acid, an antioxidant, a complexing agent and a solvent. When the electroplating liquid is used for electroplating, the available current density can reach 25 ASD, the electroplating efficiency is high, tin-silver alloy salient points obtained through electroplating are uniform, the cavity proportion is small after the salient points flow back, and collapse is avoided.
Owner:SHENZHEN UNITED BLUEOCEAN APPLIED MATERIAL TECHNOLOGY CO LTD

Purification method of high-purity quartz sand

The invention discloses a method for purifying high-purity quartz sand, which belongs to the technical field of preparation of high-purity quartz sand, and comprises the following steps: (1) sequentially carrying out high-pressure water jet scrubbing, gradient screening classification and dielectric separation on sandstone type quartz ore raw ore with SiO2 content of 85-90% to remove feldspar to obtain quartz particles with feldspar content of less than or equal to 2%; (2) sequentially carrying out microwave field pretreatment, infrared light field crack propagation and pulse laser implosion stripping on the quartz particles obtained in the step (1), and regulating and controlling technological parameters of the three fields through linkage of a PLC (Programmable Logic Controller) system, so that the stripping rate of an impurity inclusion is greater than or equal to 92%; according to the invention, aiming at quartz particles with different particle sizes, a plurality of process parameters are automatically optimized and adjusted through the PLC system, accurate control and adaptive production are realized, and high-purity products can be stably produced from sandstone type quartz raw materials with different grades in different regions. And the inclusion is opened from inside to outside through a multi-field synergistic effect, and the completeness of the quartz particles is retained to the greatest extent by combining with an optimized fluoride-free acid leaching condition.
Owner:硅峪新材料科技(中山)有限公司

Extrusion process aids for polyolefins

PendingUS20250388737A1Polymer sciencePolyolefin
Processing aids and lubricants with free acid groups and relatively high molecular weights are used as process aids in the formation of extrudates and other molded materials. The compositions of this invention can be used as defined, or can be used with prior art processing aids, depending on the end use application. The novel materials and process provide a useful alternative to the sole use of fluorine-based polymer processing aids.
Owner:V-2 INNOVATIONS LLC

A preparation method of lithium difluorooxalatoborate

The present invention provides a preparation method of lithium difluorooxalate borate, belonging to the technical field of lithium battery electrolyte additives. The present invention obtains a bis(methylsilyl) oxalate compound by a substitution reaction between a methylchlorosilane compound and oxalic acid, and mixes the bis(methylsilyl) oxalate compound with lithium oxalate, a boron trifluoride complex and an organic solvent to obtain lithium difluorooxalate borate; wherein the bis(methylsilyl) oxalate compound is used as a raw material, has strong reaction activity, generates a stable methylfluorosilane gas byproduct while introducing oxalate into the system, and does not cause chloride ions and free acid residues; in addition, when the raw material is bis(trimethylsilyl) oxalate, even if there is a small amount of raw material residue, it can be used as a new multifunctional electrolyte additive, play a certain synergistic role, and can improve the compatibility between electrolytes. The whole process is simple, the product yield obtained by the reaction is high, the product purity is high, and the separation is easy, which is suitable for industrial production.
Owner:GANFENG LITHIUM CO LTD

Tin-silver alloy electroplating solution as well as preparation method and application thereof

The invention relates to the field of electroplating, and discloses a tin-silver alloy electroplating solution and a preparation method and application thereof.The electroplating solution comprises soluble stannous salt, soluble silver salt, a composite defoaming agent, an anti-scorching agent, free acid, an antioxidant, a complexing agent and a solvent, and the composite defoaming agent comprises a first defoaming agent and a second defoaming agent; the first defoaming agent is selected from naphthol sulfonic acid, and the second defoaming agent is selected from naphthol ether; the molar ratio of the first defoaming agent to the second defoaming agent is 1: (1-4). The tin-silver alloy electroplating solution provided by the invention contains the composite defoaming agent compounded by the naphthol sulfonic acid and the naphthol ether, so that foam can be effectively prevented from being formed, and meanwhile, the formed foam is destroyed, so that a tin-silver alloy bump is prevented from generating a cavity after backflow. In addition, the composite defoaming agent has good water solubility and high cloud point, does not cause turbidity of the electroplating liquid at a relatively high temperature, and can avoid influence on normal use of the electroplating liquid.
Owner:SHENZHEN UNITED BLUEOCEAN APPLIED MATERIAL TECHNOLOGY CO LTD

Flash fire improver for electrolyte of boron-free aluminum electrolytic capacitor and preparation method of flash fire improver

The invention relates to the technical field of flash fire lifting agents, and discloses a flash fire lifting agent of an electrolyte of a boron-free aluminum electrolytic capacitor and a preparation method of the flash fire lifting agent, and the flash fire lifting agent comprises the following components in percentage by mass: 10-30% of organic ammonium carboxylate; 5%-15% of a nitro compound; 3%-10% of a phosphate ester compound; 2%-8% of a polyethylene glycol derivative; 0.5%-3% of organic siloxane; and the balance of deionized water. Through the synergistic effect of the organic ammonium carboxylate, the nitro compound, the phosphate ester substance and the organosiloxane in a specific proportion, the sparking voltage of the electrolyte is remarkably improved, and the negative effects of boron elements on the environment and the performance of a capacitor are avoided; a nitro compound is used as an electron acceptor to inhibit hydrogen precipitation, and cooperates with phosphate to fill oxide film micropores and block current concentration; the organic siloxane forms a hydrophobic barrier on an electrode interface, electrolyte decomposition is delayed, the organic carboxylic acid ammonium salt accurately controls the free acid concentration, and the conductivity rise caused by hydrogen ion migration is avoided.
Owner:NANTONG RUIDA ELECTRONICS MATERIAL

High-magnesium medium-trace particle water-soluble fertilizer and preparation method thereof

The invention relates to the technical field of water-soluble fertilizers, in particular to a high-magnesium medium-trace particle water-soluble fertilizer and a preparation method thereof. The invention discloses a high-magnesium medium-trace particle water-soluble fertilizer, which is prepared by carrying out spray granulation on granulation slurry in a granulator through a nozzle, the specific gravity of the granulation slurry is greater than or equal to 1.68 g / cm < 3 >, and the mass content of magnesium in the granulation slurry is greater than or equal to 2.0%; in the high-magnesium medium-trace particle water-soluble fertilizer, the mass content of magnesium is greater than or equal to 1.0%. Through the steps of neutralization treatment and filtration impurity removal, free acid and impurities which influence the product quality are effectively removed; by accurately controlling concentration and cooling conditions, the content of free water in the product is reduced, and the physical property of the product is improved; through granulation, the final product has better appearance roundness and stability.
Owner:GUIZHOU BATIAN ECOTYPIC ENG CO LTD

Method for monitoring preparation process of bis (fluorosulfonyl) imide metal salt and preparation method of bis (fluorosulfonyl) imide metal salt

The invention relates to a monitoring method for a preparation process of bis (fluorosulfonyl) imide metal salt and a preparation method. The monitoring method is used for monitoring the preparation process of synthesizing the bis (fluorosulfonyl) imide metal salt through double decomposition reaction of bis (fluorosulfonyl) imide and metal salt, and comprises the following steps: taking a real-time reaction solution sample of the double decomposition reaction; testing the real-time total mass content W2 of the free acid in the reaction solution sample and the real-time mass content W3 of the free acid HR in the reaction solution sample; according to the initial mass content W1 of the free acid in the imidodisulfuryl fluoride raw material, the real-time total mass content W2 of the free acid in the reaction solution sample and the mass content W3 of the free acid HR in the reaction solution sample, the percentage content X of the mass of the residual imidodisulfuryl fluoride in the reaction solution to the mass of the imidodisulfuryl fluoride raw material is obtained; and judging the preparation process of the bis (fluorosulfonyl) imide metal salt according to the X value. According to the method, the preparation process of the bis (fluorosulfonyl) imide metal salt can be effectively monitored.
Owner:YUEYANG CHANGDE ENVIRONMENTAL TECH CO LTD

Resourceful treatment method for stainless steel pickling waste liquid and waste water

The invention discloses a resourceful treatment method for stainless steel pickling waste liquid and waste water. The waste liquid is divided into high-concentration waste liquid and low-concentration waste liquid according to the acid concentration and the salt concentration to be treated respectively. Sequentially recovering gypsum, chromic hydroxide, nickel sulfide, ferrous hydroxide and manganese-rich slag from the low-concentration waste liquid through gradient precipitation; and neutralizing free acid from the high-concentration waste liquid by using ferrous hydroxide generated in a low-concentration section, cooling and crystallizing to recover ferrous sulfate, deeply removing nickel by using nickel sulfide generated in the low-concentration section, and precipitating to recover chromium hydroxide. In the whole process, generation of ferric iron is strictly controlled, and high-value productization recovery of free acid and all metals is achieved. The method has the advantages of low medicament consumption, high metal recovery rate, high product value, no secondary pollution and the like.
Owner:SHENZHEN DAREN ENVIRONMENTAL PROTECTION CO LTD

Method for preparing polymeric ferric sulfate from solid waste yellow ferrous sulfate in titanium dioxide plant

The present invention provides a method for preparing polyferric sulfate from solid waste yellow ferrous sulfate in a titanium dioxide factory, comprising the following steps: dissolving the yellow ferrous sulfate raw material in water, adding iron oxide red under heating conditions, stirring until the reaction is complete, and then filtering to remove insoluble impurities; adding an oxidant to the filtrate, heating and stirring to carry out oxidation, hydrolysis, and polymerization reactions to obtain a liquid product; concentrating and drying the liquid product to prepare solid polyferric sulfate. The method neutralizes the free acid in the raw material yellow ferrous sulfate by adding iron oxide red, increases the content of effective component iron in the system, and the prepared product has a relatively high basicity and good polymerization effect, and no external acid or alkali is required during the preparation process. The present invention eliminates the environmental protection hidden danger caused by the stacking of solid waste, enables the comprehensive utilization of industrial waste by-products, reduces the production cost of polyferric sulfate, and improves the economic benefit of titanium dioxide production.
Owner:EAST CHINA UNIV OF SCI & TECH +1

A method for rapidly and harmlessly treating phosphogypsum

ActiveCN121755541BPhosphatePhosphogypsum
The application discloses a method for rapidly and harmlessly treating phosphogypsum, and particularly relates to the harmless treatment technical field of industrial solid waste. The method comprises the following steps: mixing raw materials with an alkaline neutralizing agent, a trapping agent and an activating agent, adding a phosphorus solidifying agent and a fluorine solidifying agent, mixing, carbonizing and aging, and obtaining harmless phosphogypsum. The method adopts the alkaline neutralizing agent to rapidly neutralize free acid and improve the pH of the system; the trapping agent adsorbs heavy metals; the activating agent promotes As, Cd and the like to form a difficult-to-dissolve iron oxide gel or a precipitate; the phosphorus solidifying agent and the fluorine solidifying agent perform deep chemical precipitation to form a stable iron-calcium-phosphate / ferric fluoride composite solidified body. The functions of the agents are clear, and the agents have synergistic effects; the solidification effect of the agents on high water-solubility phosphorus, fluorine and various heavy metals is far better than that of a single or simply compounded agent system; and the leaching concentration can be reduced to a level far lower than the national standard.
Owner:贵州胜威凯洋化工有限公司

High-purity lithium bis (fluorosulfonyl) imide solution as well as preparation method and application thereof

The invention belongs to the technical field of electrolyte materials, and discloses a high-purity lithium bis (fluorosulfonyl) imide solution as well as a preparation method and application thereof. The preparation method of the high-purity lithium bis (fluorosulfonyl) imide solution comprises the following steps: 1) mixing inert chloralkane and lithium carbonate to form a suspension, dropwise adding bis (fluorosulfonyl) imide into the suspension at reaction temperature and pressure for reaction, after the reaction is finished, performing filter pressing, washing, and performing filter pressing again to obtain a filter cake; and 2) crushing the filter cake, feeding the crushed filter cake into a closed-loop circulating fluidized bed, sequentially drying in a low-temperature area and a medium-temperature area, instantaneously contacting and dissolving the obtained hot powder with an atomized and sprayed carbonate solvent to form a solution, and performing microfiltration to obtain the high-purity lithium bis (fluorosulfonyl) imide solution. The lithium bis (fluorosulfonyl) imide solution has ultra-high purity and ultra-low moisture, the content of other impurities such as chloride ions, free acids and metal ions is extremely low, additional steps of dehydration, purification or acidity adjustment and the like are not needed, and the lithium bis (fluorosulfonyl) imide solution can be directly used for preparing a high-performance lithium ion battery electrolyte.
Owner:WUHAN INFINITE CHEMICAL ENGINEERING CO LTD

A device for neutralizing free acid in by-product ammonium sulfate product of ammonia desulfurization

This utility model relates to the field of ammonium sulfate post-treatment technology in ammonia desulfurization, and discloses a free acid neutralization device for ammonium sulfate by-products of ammonia desulfurization. The device includes a hydrocyclone, centrifuge, neutralizing agent silo, metering feeder, feeding screw, dryer, dust removal equipment, and finished product storage silo. This free acid neutralization device for ammonium sulfate by-products of ammonia desulfurization, by setting up a neutralizing agent silo and a metering feeder, utilizes the post-treatment system equipment of the ammonia desulfurization unit to achieve compliant production of free acid from the by-product ammonium sulfate. It features a simple process, low equipment investment, negligible operating costs, low failure rate, and high safety and reliability.
Owner:SHAANXI CHANGQING ENERGY & CHEM IND CO LTD

Method for preparing high-purity lactide through double-solvent phase change extraction

The invention relates to the field of chemistry and chemical engineering, in particular to a method for preparing high-purity lactide through double-solvent phase change extraction. A compound containing oxygen-containing functional groups such as alcohol, ether, ketone, carboxylic acid and amide is selected as a hydrogen bond acceptor solvent, and water is selected as a hydrolysis solvent. Wherein the hydrogen bond acceptor solvent is combined with free acid impurities (hydrogen bond donors) in the crude lactide to form a deep eutectic solvent, and the water hydrolyzes meso-lactide into lactic acid retaining D, L-lactide. In the process, the whole system is subjected to heating, melting, blending, cooling, crystallizing and separating out, finally, solid-phase high-purity D, L lactide is subjected to separation and drying treatment, the chemical purity is improved to 99% or above from 40%-95%, and the optical purity is improved to 98% or above. According to the scheme, the operation is simple and convenient, the separation efficiency is high, the method is environment-friendly, the energy consumption is remarkably reduced, the defects of traditional high-temperature distillation and repeated recrystallization are avoided, and an efficient and environment-friendly new scheme is provided for industrial purification of lactide.
Owner:HENAN XINGHAN BIOTECHNOLOGY CO LTD

Tin-silver alloy electroplating solution, its preparation method and application, electroplating method

ActiveCN119800461BCellsActive agentAlloy
The present invention relates to the field of electroplating, and discloses a tin-silver alloy electroplating solution, a preparation method and application thereof, and an electroplating method. The electroplating solution contains a soluble stannous salt, a soluble silver salt, a composite surfactant, a free acid, an antioxidant, a complexing agent and a solvent. When electroplating with the electroplating solution, the available current density can reach 25 ASD, the electroplating efficiency is high, and the tin-silver alloy bumps obtained by electroplating are uniform, the proportion of voids after bump reflow is small, and no collapse occurs.
Owner:SHENZHEN UNITED BLUEOCEAN APPLIED MATERIAL TECHNOLOGY CO LTD

Solution composition for testing grafting rate of maleic anhydride as well as preparation method and application of solution composition

The invention provides a solution composition for testing the grafting rate of maleic anhydride, and belongs to the field of high polymer material detection. The solution composition for testing the maleic anhydride grafting rate is prepared from the following components in parts by weight: 80 to 90 parts of a main solvent, 5 to 10 parts of an auxiliary solvent, 3 to 5 parts of a surfactant, 2 to 5 parts of a solubilizer, 0.05 to 0.15 part of a disentangling agent and 0 to 0.15 part of water. The method comprehensively solves the four key problems of high-temperature volatilization / low-temperature precipitation, entanglement embedding, low titration efficiency and free anhydride interference in the traditional method which influence the test accuracy of the maleic anhydride grafting rate.
Owner:JIANGSU KINGFA SCI & TECH ADVANCED MATERIALS CO LTD +1

Preparation method and recrystallization method of lithium bis (oxalato) borate

The invention discloses a preparation method and a recrystallization method of lithium bis (oxalato) borate. The invention provides a preparation method of lithium bis (oxalato) borate, which comprises the following steps: in a solvent, carrying out reaction on chain-like silicon oxalate as shown in a formula II and lithium bis (oxalato) borate to obtain lithium bis (oxalato) borate as shown in a formula III, the solvent is an aprotic organic solvent. The preparation method has one or more advantages as follows: the yield is high, the purity is high, insoluble substances are few, the chromaticity is low, free acid or chloride ions are lower, lithium bis (fluoro) oxalato borate can be recycled, and the cost is reduced.
Owner:LIANHE CHEM TECH +2

Poly-L-lactic acid polymer and preparation method thereof

PendingCN120647896APolymer sciencePtru catalyst
The invention provides a poly-L-lactic acid polymer and a preparation method thereof, and the method comprises the following steps: replacing halogen atoms in a catalyst with an initiator containing a hydroxyl compound to generate an alkoxy compound Bi-OR, and then carrying out a polymerization reaction with L-lactide to obtain the high-molecular-weight poly-L-lactic acid polymer. The catalyst has high tolerance to water and free acid, the requirements for the free acid and the water content of the L-lactide are reduced, the L-lactide with high free acid and water content can be directly used, and the refining cost of the L-lactide is greatly reduced. The specific rotation of the poly-L-lactic acid polymer prepared by the method meets the standard, the poly-L-lactic acid polymer has high tolerance to moisture and free acid, the catalytic efficiency is high, the process stability is good, and the molecular weight can be regulated and controlled through the dosage of the initiator.
Owner:WEIHAI GUYUCHUN BIOTECHNOLOGY CO LTD

Treatment method and equipment for neutralizing phosphogypsum free acid and storage medium

The invention provides a treatment method and device for neutralizing phosphogypsum free acid and a storage medium. The method comprises the steps that the initial free acid concentration of to-be-neutralized phosphogypsum and the release rate constant of the free acid are obtained; calculating first dynamic data according to the initial free acid concentration and the release rate constant of the free acid; obtaining an initial neutralizer release rate and a dissolution rate constant of the neutralizer; calculating to obtain second dynamic data according to the initial neutralizer release rate and dissolution rate constant; acquiring a temperature parameter and a humidity parameter; performing correction processing on the first dynamic data according to the temperature parameter to obtain third dynamic data; correcting the second dynamic data according to the humidity parameter to obtain fourth dynamic data; according to the third dynamic data and the fourth dynamic data, the free acid remaining amount of the phosphogypsum to be neutralized is determined, and the technical effect of improving the neutralization treatment efficiency and the neutralization stability of the phosphogypsum free acid is achieved.
Owner:CHINA THREE GORGES CORPORATION

Extrusion process aids for polyolefins

PCT designated stageWO2026101852A1Polymer sciencePolyolefin
Organic molecules with free acid groups and a molecular weight of greater than 140 g / mol used in combination with surfactants, are used as processing aids in the formation of extrudates and other molded materials. The compositions of this invention can be used as defined herein, or can be used with prior art processing aids, depending on the end use application. The novel materials and processes provide a useful alternative to the sole use of fluorine-based polymer processing aids.
Owner:MEHTA VEERAG +1

Antibacterial and mildew-proof TPE material and preparation method thereof

PendingCN122356713AElastomerStearic acid
This invention provides an antibacterial and antifungal TPE material, belonging to the field of thermoplastic elastomer technology. The antibacterial and antifungal TPE material of this invention comprises the following components: SEBS, PP, a plasticizer, modified nano-zinc oxide, N-n-butyl-1,2-benzisothiazolin-3-one, 4,5-dichloro-2-n-octyl-4-isothiazolin-3-one, an antioxidant, and zinc stearate; wherein the modified nano-zinc oxide is obtained by melt blending nano-zinc oxide with maleic anhydride-grafted SEBS, the mass ratio of the modified nano-zinc oxide to the maleic anhydride-grafted SEBS is (0.6-1.7):1, and the particle size of the nano-zinc oxide is 20-50 nm; the free acid content of the zinc stearate is 0.3%-0.5%. The antibacterial and antifungal TPE material of this invention possesses good antibacterial properties, antifungal properties, and tensile strength.
Owner:SHANTOU HONGLONG IND CO LTD

A segmented curing preparation process of low free acid high water-soluble phosphoric superphosphate

PendingCN122145199ASuperphosphatesPhosphatic fertiliser granulation/pelletisationPhysical chemistryPhosphorite
This invention relates to the field of fertilizer production technology, specifically to a segmented ripening preparation process for low-free-acid, high-water-soluble superphosphate; the process includes the following steps: feeding phosphate rock powder into a ball mill for grinding to a particle size ≤120 mesh, preparing 93%±0.5% industrial sulfuric acid; adding phosphate rock powder at a molar ratio of available P2O5 to sulfuric acid of 1:1.05~1:1.07, adding 0.3%~0.5% (by weight of phosphate rock powder) of a modifying agent, and reacting at 65~70℃ for 40~50 minutes. In the later stage of the reaction, low-pressure steam of 0.2 MPa is introduced; staged maturation is carried out, first in a closed chamber at 55~60℃ for 24 hours, and then in a ventilated chamber at 45~50℃ and a wind speed of 0.8~1.0 m / s for 48 hours; granulation and screening are carried out, with the granulation drum rotating at 14~16 r / min and tilted at an angle of 3°~5°; through the above methods, the problems of high free acid, low proportion of water-soluble phosphorus and insufficient production efficiency in traditional processes are solved, and the product quality and production capacity are synergistically improved.
Owner:HUBEI LONGXIANG PHOSPHATE

Efficient and energy-saving arsenic sulfide residue cleaning treatment process

ActiveCN117088411BArsenic oxides/hydroxides/oxyacidsUsing liquid separation agentBrickSlurry
The application discloses a kind of high-efficiency energy-saving sulphidized arsenic residue cleaning treatment process, comprising the following steps: (1) the sulphidized arsenic residue containing free acid is slurried with calculated amount 3~6 times of reducing agent, the pH value of slurry is adjusted to 6.5 with adjusting agent, and dry material is obtained by filtering and drying;(2) adding skeleton material to dry material, and making hollow brick by brick making machine after mixing evenly;(3) the hollow brick is transferred into furnace to carry out drying, reduction, sublimation and cooling in turn to complete the process of arsenic removal, and obtain arsenic removal residue and arsenic-containing high-temperature flue gas;(4) after heat exchange and cooling by heat exchanger, the arsenic-containing high-temperature flue gas enters condensing chamber to condense and recover arsenic to obtain arsenic trioxide;(5) after flue gas purification and water-gas separation, the arsenic removal tail gas returns to use.The application uses the above treatment process, basically no external heating is needed during continuous production, the purity of arsenic trioxide recovered by condensation is relatively high, the arsenic removal tail gas is recycled after nitrogen purification, basically no external discharge or very small discharge amount, and it is environment-friendly.
Owner:GUANGXI KAIXI NONFERROUS METALS CO LTD

Inverse latex for cosmetic composition comprising specific chelating agent and polyelectrolyte combining strong acid function and neutral function

To provide a novel inverse latex using a novel metal ion sequestering agent.SOLUTION: There is provided a self-invertible inverse latex having an aqueous phase, comprising: a) a cross-linked anionic polyelectrolyte consisting of: at least one first monomer unit derived from 2-methyl-2-[(1-oxo-2-propenyl)amino]1-propane sulfonic acid in the form of a free or partially or totally salified acid; and at least one second monomer unit derived from at least one monomer selected from the group consisting of (2-hydroxyethyl)acrylate, (2,3-dihydroxypropyl)acrylate, (2-hydroxyethyl)methacrylate and the like; and at least one monomer unit derived from a cross-linking polyethylenic monomer; b) at least one chelating compound selected from the group consisting of ethylenediamine disuccinic acid in the form of trisodium salt, tetrasodium salt of glutamic acid, N,N diacetic, or the sodium salt of imminosuccinic acid.SELECTED DRAWING: None
Owner:SOC DEXPLOITATION DE PROD POUR LES IND CHEM SEPPIC

A method of preparing a south fragment of MK-0616

The application provides a preparation method of MK-0616 south fragment, and relates to the technical field of polypeptide synthesis. The preparation method comprises the following steps: condensation reaction of alkyl primary alcohol 17 and protected amino acid 2 to obtain intermediate 18; deprotection reaction of the intermediate 18 to obtain intermediate 19; condensation reaction of the intermediate 19 and compound 4 to obtain intermediate 20; deprotection reaction of the intermediate 20 to obtain intermediate 21; condensation reaction of the intermediate 21 and compound 10 to obtain intermediate 22; deprotection reaction of the intermediate 22 to obtain intermediate 23; condensation reaction of the intermediate 23 and compound 14 to obtain intermediate 24; hydrolysis reaction of the intermediate 24 to obtain a crude product of MK-0616 south fragment; salt crystallization of the crude product of MK-0616 south fragment to obtain intermediate 15; and free acidization of the intermediate 15 to obtain a pure product of MK-0616 south fragment.
Owner:HANGZHOU NUOAO BIOMEDICAL TECH CO LTD +1

Alkalinity slow-release material for promoting carbon sequestration and sink in marine artificial reefs and preparation method thereof

The application discloses a kind of alkalinity slow-release materials and preparation method for promoting carbon sequestration and sink in marine artificial reef.The alkalinity slow-release material includes magnesium hydroxide, sodium carbonate, glutaraldehyde, cement, three light methyl aminomethylane buffer and water.Sodium carbonate, magnesium hydroxide and glutaraldehyde are mixed with cement, then water and three light methyl aminomethylane buffer are added for stirring.After sufficient stirring, the alkalinity slow-release material is obtained by setting and solidifying in a mold.The magnesium hydroxide and sodium carbonate of slow-release material react with free acid ions in water body to generate soluble salt that can be absorbed and salt that inhibits the growth of algae.The slow-release material increases the CO2 absorption capacity of water body and has no adverse effects on the environment.It can also be used to make artificial reefs, which can adjust the alkalinity of seawater and promote the growth of corals in addition to the function of transplantation and fixation.By using the slow-release material, the alkalinity of seawater can be maintained within a certain range, CO2 absorption and seawater acidification can be reduced, which is helpful for the recovery of coral reef community and promotes carbon sequestration and sink in seawater.
Owner:SOUTH CHINA SEA INST OF OCEANOLOGY CHINESE ACAD OF SCI +1

Tin alloy plating solution

PCT designated stageWO2026177032A1Active agentPhenyl group
This tin alloy plating solution comprises: (A) a soluble salt that contains at least a stannous salt; (B) a soluble salt of a metal that is nobler than tin; (C) a leveling agent that is composed of an alkanesulfonic acid which contains 9-18 carbon atoms in each molecule or a salt thereof; (D) a free acid; (E) a nonionic surfactant that contains one or more phenyl groups in each molecule; and (F) an EO / PO block polymer that has an EO group at an end. The EO ratio in the EO / PO block polymer is within the range of 20 mol% to 50 mol% inclusive, and the molecular weight of the EO / PO block polymer is within the range of 1,500 to 3,500 inclusive.
Owner:MITSUBISHI MATERIALS CORP

Driver special anti-stuck spicy water and preparation method and application thereof

PendingCN122320213ACapsicum extractIodised salt
The application discloses a driver special anti-drowsy spicy water and a preparation method and application thereof, and relates to the technical field of functional drinks.The raw material components of the spicy water include aged old-lake sour water, self-made iodine-free acid salt water, pepper extract and trace chicken essence;the self-made iodine-free acid salt water is prepared by mixing 92 parts of drinking water and 8 parts of iodine-free salt by weight;the salt content of the finished product is 0.5%-0.8%, the pH value is 3.0-3.6, and the spiciness of the pepper extract is 10000-40000 SHU.The application further discloses a preparation method of the spicy water and an anti-slip light-proof glass bottle packaging structure specially designed for drivers.The natural sour and spicy synergistic stimulation of the aged old-lake sour water and the pepper extract can effectively inhibit the drowsiness of drivers, relieve fatigue driving, and keep the drivers awake for more than 30 minutes after single drinking;the application is suitable for long-distance drivers, and has a remarkable anti-drowsy effect and good driving scene adaptability.
Owner:唐泽成