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21491 results about "Hydroxy group" patented technology

A hydroxy or hydroxyl group is the entity with the formula OH. It contains oxygen bonded to hydrogen. In organic chemistry, alcohols and carboxylic acids contain hydroxy groups. The anion [OH⁻], called hydroxide, consists of a hydroxyl group.

Timber antiseptic agent

To provide a timber antiseptic agent which exhibits superior safety and superior antibacterial performance with low influence on the human body and environment.SOLUTION: The present invention relates to a timber antiseptic agent containing an alkyl 4-hydroxybenzoate represented by formula (1) [where R represents an alkyl group having 5 to 10 carbon atoms] or a salt thereof.SELECTED DRAWING: None
Owner:UENO PHARMA CO LTD

Alumina carrier as well as preparation method and application thereof

The invention belongs to the field of catalysts, and particularly relates to an alumina carrier as well as a preparation method and application thereof. The surface of the alumina carrier has oxygen-containing groups, and the density of the oxygen-containing groups on the surface of the alumina carrier is 0.15-5mmol / m < 2 >. Wherein the oxygen-containing group is at least one of hydroxyl, carboxyl and lactone group; the specific surface area of the alumina carrier is 10-150m < 2 > / g. The types, the number and the density of oxygen-containing groups on the surface of the obtained carrier are improved, and various index requirements of various supported catalysts on dispersion forms and dispersion degrees of different metal active components in the field of petrochemical engineering can be well met; and the carrier also has the characteristics of low bulk density, high water absorption rate, large pore volume and large average pore size, has a gain effect on uniform distribution of active metal components in the catalyst loading process, and has extremely high application value.
Owner:CHINA PETROLEUM & CHEMICAL CORP +1

Pure bio-based polyhydroxyalkanoate adhesive as well as preparation and application thereof

The invention discloses a pure bio-based polyhydroxyalkanoate adhesive as well as preparation and application thereof, and belongs to the technical field of degradable adhesives. According to the adhesive, polyhydroxybutyrate valerate or polyhydroxybutyrate hexanoate is used as a matrix, and the acid value reaches 2-15 mg KOH / g through molten end group activation; a reactive emulsifier with a hydrophilic-lipophilic balance value of 9-12 is introduced into a water phase, and the stable aqueous dispersion is prepared through phase inversion high-shear emulsification. The Z-average particle size of the dispersion is 0.12-0.30 [mu] m, and the content of the free surfactant is not higher than 30wt%. After the tackifying resin, the plasticizer and the vegetable wax are compounded, the bio-based carbon content of the obtained adhesive is not lower than 95%, and the volatile organic compound content is not higher than 100 mg / kg. The paper / paper heat sealing strength of the adhesive is not lower than 7.0 N / 15mm, the 180-degree peel strength is not lower than 7.5 N / 25mm, and the adhesive can pass repulping evaluation.
Owner:DU BAI CHENG NEW MATERIAL TECH (SHANGHAI) CO LTD +3

Photo-thermal aging resistant polyester composite material and preparation method thereof

InactiveCN119431756AIncrease the number of crosslinksImprove aging resistanceThermal ageingPolymer science
The invention discloses a photo-thermal aging resistant polyester composite material and a preparation method thereof, a modified monomer, a modified filler, benzophenone, terephthalic acid and neopentyl glycol are subjected to esterification condensation polymerization to prepare the composite material, and the modified monomer is added, so that the prepared polyester molecule is of a branched structure; the side chain of a polyester molecule and the surface of the modified filler both contain unsaturated double bonds which can react after being irradiated by ultraviolet light, so that the number of crosslinking points of the composite material is increased, the crosslinking density is further improved, and the anti-aging effect of the material is further improved; the modified filler can improve the high-temperature-resistant effect of the composite material, the modified filler is matched with the hindered phenol structure of the side chain to further improve the heat aging-resistant effect of the composite material, hydroxyl and ketone groups on the modified filler form intramolecular hydrogen bonds, light energy can be converted into heat energy to be released, and then the light aging-resistant effect of the composite material is improved.
Owner:JIANGXI PLASTIC HIGH-TECH MATERIALS CO LTD

High-temperature-resistant epoxy insulating material for transformer and preparation method thereof

The invention discloses a high-temperature-resistant epoxy insulating material for a transformer and a preparation method thereof, and belongs to the technical field of insulating materials. The high-temperature-resistant epoxy insulating material for the transformer is prepared from the following components in parts by weight: 50 to 60 parts of bisphenol A epoxy resin, 20 to 50 parts of anhydride curing agent, 10 to 20 parts of modified composite filler and 5 to 10 parts of epoxidized hydroxyl-terminated liquid polybutadiene, wherein the modified composite filler is a mixture of first boron nitride, second boron nitride and silicon nitride grafted with a silane coupling agent and dopamine, and the mass ratio of the first boron nitride to the second boron nitride to the silicon nitride is (1-2): (2-4): 1. The high-temperature-resistant epoxy insulating material for the transformer has excellent mechanical property, insulating property, heat-conducting property and high-temperature aging resistance.
Owner:STATE GRID ANHUI ULTRA HIGH VOLTAGE CO +1

Construction method for and use of rhizoma pinellinae praeparata decoction piece, standard decoction and formula granule characteristic spectra

A construction method for and a use of rhizoma pinellinae praeparata decoction piece, standard decoction and formula granule characteristic spectra. The construction method comprises the following steps: dissolving a test sample by using a solvent, and extracting to obtain a solution to tested; and measuring said solution by using high-performance liquid chromatography (HPLC) to obtain rhizoma pinellinae praeparata decoction piece, standard decoction and formula granule characteristic spectra, wherein chromatographic conditions of the HPLC are as follows: the chromatographic column is a C18 column; and gradient elution is performed by using acetonitrile as mobile phase A and a 0.1% phosphoric acid aqueous solution as mobile phase B. HPLC is used, gradient elution is performed by using acetonitrile and a 0.1% phosphoric acid aqueous solution as mobile phases, and 4-hydroxybenzoic acid is used as a reference object, so that rhizoma pinellinae praeparata decoction piece, standard decoction and formula granule HPLC characteristic spectra are established; the method has good repeatability and precision, is stable and reliable, and can control the quality of rhizoma pinellinae praeparata decoction pieces, a standard decoction and formula granules.
Owner:SICHUAN NEO GREEN PHARMA TECH DEV

Fiberglass insulation product

A fibrous insulation product comprising a plurality of randomly oriented glass fibers and a cross-linked formaldehyde-free binder composition at least partially coating the fibers is disclosed. The cross-linked formaldehyde-free binder composition is formed from an aqueous binder composition comprising 5.0% by weight to 37.0% by weight of at least one monomeric polyol having at least four hydroxyl groups and at least 50.0% by weight of a cross-linking agent comprising a polymeric polycarboxylic acid having at least two carboxylic acid groups, based on the total solids content of the aqueous binder composition. The glass fibers have an average fiber diameter in the range of 8 HT to 12 HT. The fibrous insulation product, after curing, has a density, when uncompressed, in the range of 0.30 pcf to 2.7 pcf.
Owner:OWENS CORNING INTELLECTUAL CAPITAL LLC

Carbonyl reductase mutant and application thereof in synthesis of statin drug intermediates

The invention provides a carbonyl reductase mutant. The carbonyl reductase mutant is obtained by performing single-point mutation or multi-point combined mutation on the 17th site, the 40th site and the 64th site of an amino acid sequence as shown in SEQ ID NO.1. The invention also provides a coding gene, a recombinant vector containing the coding gene, a co-expression engineering bacterium and an application of the co-expression engineering bacterium. Compared with a wild type enzyme, the carbonyl reductase mutant has high activity and high stereoselectivity, the enzyme activity can reach more than two times that of the wild type enzyme, the catalytic efficiency on a substrate precursor ketone is remarkably improved, the yield of a statin drug intermediate and chiral alcohol synthesized by an enzyme method of the carbonyl reductase mutant is remarkably improved, and the yield of a rosuvastatin intermediate (3R, 3R, 3R, 3R, 3R, 3R, 3R, 3R, 3R, 3R, 3R, 3R, 3R, 3R, 3R, 3R, 3R, 3R, 3R, 3R, 3R) is remarkably improved. The highest yields of the (3R, 5R)-6-chloro-3, 5-dihydroxyhexanoic acid tert-butyl ester and the atorvastatin intermediate (3R, 5R)-6-cyano-3, 5-dihydroxyhexanoic acid tert-butyl ester reach 99% and 97.6% respectively, e.e. Is larger than 99%, and the method has high industrial application value.
Owner:ZHEJIANG UNIV OF TECH

Copper-carbon quantum dot nano-enzyme as well as preparation method and application thereof

PendingCN119186562AEnhanced electron transport capabilitiesIncreased peroxidase activityMaterial nanotechnologyMaterial analysis by observing effect on chemical indicatorPeroxidaseGliphosate
The invention relates to the technical field of optical sensing, in particular to a copper-carbon quantum dot nano-enzyme and a preparation method and application thereof. Poria cocos and Cu < 2 + > are taken as raw materials, and the copper-carbon quantum dots with excellent peroxidase activity are prepared by adopting a one-pot hydrothermal method and can be used for sensitively, accurately and selectively detecting glyphosate. Cu < 2 + > is combined with oxygen-rich and nitrogen-rich components in poria cocos to generate an oxidation-reduction reaction, CuCDs with Cu < 2 + > / Cu < + > are obtained, Cu < 2 + > doping changes electron cloud distribution of the CDs, the electron transmission capability of the CuCDs is enhanced, and Cu < 2 + > and the CDs have a synergistic effect to generate three ROS (. OH,. O2 <-> and < 1 > O2), so that excellent peroxidase activity is exerted. The glyphosate is chelated with hydroxyl, amino, carbonyl, carboxyl and Cu on the surface of the CuCDs to occupy active sites, so that the active sites are poisoned, the peroxidase activity of the CuCDs is selectively inhibited, and a powerful choice is provided for simply, quickly, sensitively and selectively detecting the glyphosate.
Owner:BAISE CITY MODERN AGRI TECH RES & PROMOTION CENT +2

Use of S-beta-hydroxybutyrate compounds for induction and maintenance of flow

Compositions for inducing and maintaining a state of flow in a subject include optically pure S-beta-hydroxybutyrate or non-racemic mixtures enriched with the S-enantiomer. The S-beta-hydroxybutyrate enantiomer modulates the effect of ketone bodies in the subject and controls the rate at which ketosis is achieved. Beta-hydroxybutyric acid is more rapidly absorbed and utilized by the body than salts or esters, enhances taste, and reduces the need to include citric acid or other edible acids. Beta-hydroxybutyrate salts are more slowly absorbed and utilized by the body and can provide one or more electrolytes. Compositions for controlling ketone body level in a subject may contain a dietetically or pharmaceutically acceptable carrier and optically pure S-beta-hydroxybutyrate or non-racemic mixture enriched with S-beta-hydroxybutyrate, wherein the compositions contain from about 50.5% to 100% by enantiomeric equivalents of S-beta-hydroxybutyrate and from about 49.5% to 0% by enantiomeric equivalents of R-beta-hydroxybutyrate.
Owner:AXCESS GLOBAL SCIENCES LLC

Antibacterial PP material and preparation method thereof

InactiveCN119264554Aaccelerated deathExtended service lifeCarbon layerActive agent
The invention relates to an antibacterial PP material and a preparation method thereof, and belongs to the technical field of high polymer materials. The antibacterial PP material is prepared from the following components in parts by weight: 60 to 80 parts of PP resin, 2 to 4 parts of a surfactant, 0.5 to 1.5 parts of a modified antibacterial agent, 0.5 to 1.5 parts of a flame retardant and 0.2 to 0.8 part of an antioxidant, titanium ions in the modified antibacterial agent destroy bacterial cell walls, quaternized intermediate products react with proteins of cell membranes to accelerate bacterial death, and in addition, phenolic hydroxyl groups absorb ultraviolet rays with different wavelengths to inhibit the light aging process; a compact and continuous carbon layer is formed during combustion of the flame retardant and cooperates with phosphorus-oxygen double bonds and melamine, the flame retardant efficiency is improved, aluminum hydroxide coats the surface, hydroxyl is subjected to heat absorption decomposition during combustion, the surface temperature of combustible materials is stabilized, meanwhile, an inert aluminum oxide layer is formed, and the flammability is reduced. The antibacterial PP material prepared by the invention not only has good antibacterial and anti-aging effects, but also has excellent flame retardant property.
Owner:DONGGUAN AURORA BIOTECHNOLOGY CO LTD

Wear-resistant and high-temperature-resistant synchronous belt and preparation method thereof

The invention discloses a wear-resistant and high-temperature-resistant synchronous belt and a preparation method thereof. The wear-resistant and high-temperature-resistant synchronous belt comprises a synchronous belt framework and a synchronous belt rubber sheet, the synchronous belt rubber sheet is prepared from the following raw materials: a fluorosilicone thermoplastic polyurethane elastomer containing a benzene ring structure, an amino-containing hyperbranched liquid crystal polymer, methyl vinyl phenyl silicone rubber, epoxidized natural rubber, molybdenum sulfide nanosheets, reinforced fibers, bis (1-vinyl imidazole-2-) ketone, 2-acrylamido-2-methylpropanesulfonic acid, 4, 4 '-difluoro-1, 3, 4-trimethyl-1, 3, 4-trimethyl-1, 3, 4-trimethyl-1, 3, 4-trimethyl-1, 3, 4-trimethyl-1, 3, 4-trimethyl-1, 3, 4-trimethyl-1, 3, 4-trimethyl-1 The high-temperature-resistant rubber is prepared from 2, 6-hydroxy-2-cyanobenzothiazole, bis (3-aminophenyl) 3, 5-bis (trifluoromethyl) phenylphosphine oxide, a catalyst, a coupling agent, a vulcanizing agent, an anti-aging agent, a scorch retarder and a lubricating agent. The synchronous belt is good in mechanical property, sufficient in high-temperature resistance and cold resistance, good in wear resistance and excellent in aging resistance and flame retardance.
Owner:NINGBO FULONG SYNCHRONOUS BELT

Sulfonated cellulose, preparation method thereof and application of sulfonated cellulose as filtrate reducer for drilling fluid

The invention provides sulfonated cellulose. The sulfonated cellulose is obtained by etherifying alkalized cellulose with water-soluble halogenated sulfonate. Compared with the prior art, the sulfonated cellulose provided by the invention contains sulfonic acid groups, hydroxyl groups and other groups, so that when the sulfonated cellulose is used in the drilling fluid, the filter loss of the drilling fluid can be effectively controlled, and meanwhile, the salt pollution resistance, especially the calcium ion pollution resistance, of the drilling fluid can be improved; in addition, sulfonic groups in the product are also beneficial to improving the thermal stability of the drilling fluid, and the application range is expanded. In a word, compared with carboxymethyl cellulose for drilling fluid, sulfonated cellulose provided by the invention has obvious temperature resistance and high-valence metal ion resistance.
Owner:SINOPEC OILFIELD SERVICE CORPORATION +2

High-performance solid waste-based grouting material and preparation method thereof

The invention relates to the technical field of building materials, and particularly discloses a high-performance solid-waste-based grouting material and a preparation method thereof. Comprising the following raw materials in parts by weight: 32 to 54 parts of Portland cement, 12 to 16 parts of a modified admixture, 2.4 to 3.6 parts of a functional filler, 42 to 56 parts of aggregate, 45 to 55 parts of a photoinitiator solution, 0.6 to 0.8 part of a water reducing agent, 0.9 to 1.1 parts of a composite expanding agent, 0.04 to 0.06 part of a defoaming agent and 9.2 to 12.4 parts of deionized water. Siloxane groups, acylamino groups, ester groups and benzene rings are chemically bonded on the surface of the modified admixture, so that the hydrophilicity of the modified admixture is reduced, the modified admixture can form hydrogen-bond interaction with hydroxyl groups and cement hydrates on the functional filler, and meanwhile, a flexible long-chain alkane structure on the functional filler can be entangled with the modified admixture, so that the flexibility of the modified admixture is improved. The mechanical property, the durability and the fluidity of the grouting material are improved.
Owner:太行城乡建设集团有限公司

Scratch repair coating and preparation method thereof

The invention discloses a scratch repair coating and a preparation method thereof, and relates to the technical field of high polymer materials. When the scratch repair coating is prepared, hydroxylated boron nitride reacts with 1-(3-triethoxysilylpropyl)-2-imidazoline to prepare pre-modified boron nitride, and then the pre-modified boron nitride and 4-chloro-1-butene are subjected to quaternization to prepare modified boron nitride; the preparation method comprises the following steps: reacting styryl phosphonic dichloride with 4, 4, 5, 5, 6, 6, 7, 7, 7-nonafluoro-1, 2-heptanediol to prepare a hydroxyl-terminated phosphorus-fluorine-containing polymer; the preparation method comprises the following steps: reacting isophorone diisocyanate with a hydroxyl-terminated phosphorus and fluorine-containing polymer to prepare a polyurethane prepolymer; reacting the polyurethane prepolymer with hydroxyl-terminated coumarin to generate modified polyurethane; and uniformly mixing the modified polyurethane, the modified boron nitride and a photoinitiator to prepare the scratch repair coating. The scratch repairing coating prepared by the invention has good self-repairing performance, flame retardant property, corrosion resistance and mechanical property.
Owner:ZHEJIANG HEKE LI ENERGY CO LTD

Low-cost flow battery and application thereof

The invention provides a low-cost flow battery and an application thereof, a redox active substance of a positive electrode electrolyte of the low-cost flow battery contains a hydroxylamine cyclic structure group with hindered amine, and the hydroxylamine cyclic structure group with hindered amine is preferably selected from 1-hydroxy-2, 2, 6, 7, 8-tetramethyl-1, 3, 5-tetramethyl-1, 3, 5-tetramethyl-1, 3, 5-tetramethyl-1, 3, 5-tetramethyl-1, 3, 5-tetramethyl-1, 3, 5-tetramethyl-1, 3, 5-tetramethyl-1, one or more of a 1-oxo-2, 2, 6, 6-tetrasubstituted piperidine group, a 1-oxo-2, 2, 6, 6-tetrasubstituted piperidine group, a 1-oxo-2, 2, 6, 6-tetrasubstituted piperidine group, and a 1-oxo-2, 2, 6, 6-tetrasubstituted piperidinium group; a redox active substance of the negative electrode electrolyte contains one or more of a titanium element, a vanadium element, a chromium element, an iron element and a zinc element. The low-cost flow battery has the advantages of high output voltage, high energy density, environment friendliness and low cost, and has good application prospects and large-scale popularization potential in the field of energy storage.
Owner:SUQIAN TIMES ENERGY STORAGE TECH CO LTD

Mildew-proof silicone sealant with high curing rate and high adhesive strength

The invention relates to a mildew-proof silicone sealant with high curing rate and high adhesive strength, and belongs to the technical field of adhesives. The anti-mildew coating is prepared from alpha, omega-dihydroxy polydimethylsiloxane, dimethyl silicone oil, fumed silica, phenoxy resin coated nano calcium carbonate, a modified hydroxypropyl-gamma-cyclodextrin loaded mildew preventive, dibutyltin dilaurate, methyltrimethoxysilane and a curing accelerator. According to the mildew-proof silicone sealant with the high curing rate and the high adhesive strength, the surface drying time is 9-13 minutes, the 24-hour curing depth is 6.3-7.2 mm, the adhesive strength is 3.0-3.6 MPa, the tensile strength is 5.8-6.4 MPa, the shear strength is 3.0-3.9 MPa, the elongation at break is 410-457%, and the mildew-proof grade is 0 grade in 30 days, 60 days, 180 days and 360 days.
Owner:SHANDONG JINGMAO NEW MATERIAL CO LTD

High-temperature-resistant welding slag-resistant cable sheath material

The invention relates to a high-temperature-resistant welding slag-resistant cable sheath material, and belongs to the technical field of sheath material preparation. The sheath material is prepared from the following raw materials in parts by weight: 80 to 100 parts of TPU, 20 to 40 parts of modified montmorillonite, 18 to 35 parts of cross-linked resin, 0.1 to 1.5 parts of a processing auxiliary agent, 2 to 6 parts of an assistant cross-linking agent and 0.1 to 0.5 part of a reaction type catalyst, the cross-linked resin is prepared by mixing hexamethylene diisocyanate tripolymer and alcoholic hydroxyl group double-terminated silicone oil according to a molar ratio of (1-1.5): 1 in a first organic solvent and under an organic tin catalyst and reacting. Through introduction of the modified montmorillonite, the cross-linked resin and the assistant cross-linking agent, an interpenetrating network is formed in the composite material, and through triple high-temperature-resistant modification of the high-temperature-resistant characteristic of the montmorillonite, the high-temperature-resistant property of a silane chain and the temperature-resistant property of the interpenetrating cross-linked network, the obtained composite material can resist the temperature of a welding slag spot, so that the service life of the composite material is prolonged. And the surface of the material is not melted.
Owner:ADVANCED THERMOPLASTIC POLYMER TECH

Aqueous emulsion of ultraviolet-absorbing resin and emulsion resin composition

An aqueous ultraviolet-absorbing resin emulsion, and an aqueous resin emulsion composition containing the emulsion is provided, wherein the emulsion is excellent in compatibility with a synthetic resin and light resistance. Also, the emulsion improves stability in blending with an aqueous emulsion of the synthetic resin, and prevents bleed out of the ultraviolet-absorbing resin on the surface of a coating film. Further, the aqueous ultraviolet-absorbing resin emulsion imparts excellent alkali or solvent resistance to a synthetic resin poor in alkali or solvent resistance. More specifically, an aqueous resin emulsion composition comprising (I) an aqueous ultraviolet-absorbing resin emulsion and (II) an other aqueous resin emulsion is provided, wherein the emulsion (I) is obtained by urethanizing (A) a polyol component having an ultraviolet-absorbing group {e.g., 1,1-bis[3-(2H-benzotriazol-2-yl)-4-hydroxy-benzeneethanol]methane}, (B) a polyol if necessary, (C) an alkyl or aryl dialkanolamine compound, and (D) an organic polyisocyanate in (E) an organic solvent, diluting the reaction mixture with (F) an organic solvent having a boiling point lower than 100° C. to give a resin solution, neutralizing the resin solution with (G) a neutralizing agent, and dispersing the resultant in water.
Owner:DAICEL CORP

Preparation method of non-additive nitrogen-phosphorus-cerium synergistic flame-retardant polyurethane elastomer

ActiveCN119331214APolymer scienceMeth-
The invention discloses a preparation method of a non-additive nitrogen-phosphorus-cerium synergistic flame-retardant polyurethane elastomer, and the polyurethane elastomer is prepared by taking isocyanate as a hard segment and poly (1, 4-butanediol adipate) as a soft segment, and compounding the hard segment and the soft segment with 2-amino-4-hydroxy-6-methylpyrimidine, a phosphorus reactive flame retardant and cerium oxide. The preparation method is simple, the process is easy to control, and the prepared polyurethane elastomer has good tensile strength; besides, the limit oxygen index of the polyurethane elastomer reaches 27.4, the polyurethane elastomer meets commercial standards of flame-retardant materials and UL-94 V-0 flame-retardant grade requirements, the ultraviolet band light transmittance is 0%, ultraviolet rays can be completely isolated, and the polyurethane elastomer has a good anti-oxidation function and can be applied to the industries of wires, cables, pipe profiles, films, general molding and the like.
Owner:INNER MONGOLIA UNIV OF SCI & TECH

Preparation method of 3, 4-difluoro-2-methoxyphenylacetic acid

The invention discloses a preparation method of 3, 4-difluoro-2-methoxyphenylacetic acid, and belongs to the technical field of organic synthesis. The preparation method comprises the following steps: reacting 2, 3-difluorophenol with 3, 4-dihydropyran under the action of sulfonic acid resin to generate an intermediate 2-(2, 3-difluorophenoxy) pyran; then lithiating, reacting with tert-butyl 2-bromoacetate, and performing acidolysis to obtain a 3, 4-difluoro-2-hydroxyphenylacetic acid intermediate; and finally reacting with a methylation reagent in the presence of alkali to generate the target compound 3, 4-difluoro-2-methoxyphenylacetic acid. The preparation method has the advantages that the route is overall reasonable, the preparation method comprises three steps, and a simple and effective new route is provided for the preparation of the 3, 4-difluoro-2-methoxyphenylacetic acid.
Owner:COOL PHARM LTD

Strain for synthesizing high-proportion 4-hydroxybutyric acid polyhydroxyalkanoate and construction method thereof

The invention provides a recombinant strain for controllably synthesizing high-proportion 4-hydroxybutyric acid (4HB) polyhydroxyalkanoate (PHA) as well as a construction method and application of the recombinant strain. The recombinant strain disclosed by the invention can be used for efficiently producing high-proportion poly (3-hydroxybutyrate-4-hydroxybutyric acid) (P34HB for short) by using glucose as a unique carbon source or a 4HB structure related or non-related carbon source in amplification production of a shake flask, a 7L fermentation tank, a 100L fermentation tank and a 5000L fermentation tank.
Owner:TSINGHUA UNIVERSITY +1

Waterproof heat-resistant adhesive and preparation method thereof

The invention discloses a waterproof heat-resistant adhesive and a preparation method thereof, and relates to the technical field of adhesives. Tetramethyltri-3-trifluoropropyl cyclotetrasiloxane is used as a raw material to prepare hydroxyl-terminated organic fluorosilicone oil and modified epoxy resin, fluorine atoms are closely arranged around a main chain of the hydroxyl-terminated organic fluorosilicone oil and modified epoxy resin in an umbrella shape, and the hydroxyl-terminated organic fluorosilicone oil and modified epoxy resin cooperate with organic silicon to improve the waterproof and heat-resistant effects; hydroxyl groups on the oxidized carbon nanofibers are reacted and combined with thiocyanate in vulcanized rubber powder, and hybrid filler is formed; residual active groups on the surface of the oxidized carbon fiber are combined and crosslinked with epoxy resin, so that the heat resistance of the epoxy resin is greatly improved; secondly, phenyl maleic anhydride is used as a cross-linking agent to form a three-dimensional cross-linked structure, and meanwhile, phenyl is introduced into the structure, so that the heat-resistant effect and the waterproof effect of the epoxy resin are further improved, and the adhesive prepared by taking the epoxy resin as the raw material has excellent waterproof and heat-resistant performance. The adhesive prepared by the invention has waterproof and heat-resistant effects.
Owner:ZHENGZHOU YONGXIN DECORATION MATERIALS CO LTD

Method for purifying monomer obtained by depolymerizing waste polyester through ethylene glycol

The invention relates to a method for purifying a monomer bis (2-hydroxyethyl) terephthalate (BHET) obtained by depolymerizing waste polyester through ethylene glycol (EG), and belongs to the technical field of polyester recycling. The BHET microwave radiation induced film evaporation separation and molecular distillation refining continuous process provided by the invention solves the problems of long process flow, poor continuity, more side reactions and low purity and yield in the direct separation and refining process of BHET in alcoholysis liquid based on a gas-liquid equilibrium separation method at present. The whole technological parameter requirement is mild, the process is short, continuity is good, the BHET purity of the product is larger than or equal to 99.0 wt%, the hue is good, and the BHET yield is larger than or equal to 80.0%. And meanwhile, the method has the advantages that EG is conveniently recycled in a system, the production process is cleaner and more environment-friendly, and the comprehensive efficiency advantage is obvious.
Owner:CHENGFA TECH HUBEI CO LTD

Hydroxytyrosol-ergothioneine eutectic and preparation method and application thereof

The invention discloses a hydroxytyrosol-ergothioneine eutectic crystal as well as a preparation method and application thereof, and belongs to the technical fields of medicines, foods, daily chemicals and the like. The invention provides a hydroxytyrosol-ergothioneine eutectic crystal. The X-ray powder diffraction pattern of the hydroxytyrosol-ergothioneine eutectic crystal has characteristic diffraction peaks at least corresponding to the positions where the 2 theta value is 4.21 degrees + / -0.2 degrees, 8.36 degrees + / -0.2 degrees, 12.29 degrees + / -0.2 degrees, 15.29 degrees + / -0.2 degrees, 19.40 degrees + / -0.2 degrees, 20.98 degrees + / -0.2 degrees, 23.12 degrees + / -0.2 degrees and 28.73 degrees + / -0.2 degrees. According to the hydroxytyrosol-ergothioneine eutectic, the melting point of hydroxytyrosol is increased, the hygroscopicity of hydroxytyrosol is remarkably reduced, and meanwhile the stability of hydroxytyrosol and ergothioneine is enhanced. In addition, after the ergothioneine hydroxytyrosol forms the eutectic crystal, the ergothioneine hydroxytyrosol can also play better anti-oxidation and anti-aging effects.
Owner:SHENZHEN SIYOMICRO BIO TECH CO LTD

Rubber blend, sulfur-crosslinkable rubber mixture, and vehicle tire

The invention relates to a rubber blend, to a sulfur-crosslinkable rubber mixture comprising the rubber blend and to a vehicle tire comprising such a rubber mixture.The rubber blend comprisesat least one solution-polymerized diene polymer A of high molecular weight andat least one solution-polymerized polymer B of low molecular weight,wherein at least one of polymers A and B has been functionalized at the chain end and / or along the polymer chain and / or at a coupling site with at least one group selected from epoxy groups, hydroxyl groups, carboxyl groups, silane sulfide groups, amino groups, siloxane groups, organosilicon groups, phthalocyanine groups and amino group-containing alkoxysilyl groups.
Owner:CONTINENTAL REIFEN DEUTSCHLAND GMBH

Preparation and application of benzoselenadiazole covalent organic framework material

The invention belongs to the technical field of organic photoelectric materials, and particularly relates to preparation and application of a benzoselenadiazole covalent organic framework material. According to the invention, benzoselenadiazolyl tetraaldehyde is used as a construction unit, o-toluidine, 4, 4 '-biphenyl diamine or 3, 3'-dihydroxybenzidine is used as a connecting body, and three kinds of novel rigid COFs, namely HBU-COF-CH3, HBU-COF-H and HBU-COF-OH, are synthesized in sequence. The COFs has high cycling stability, has outstanding advantages in the aspect of sustainable heterogeneity of molecular catalysts, and can be used as a heterogeneous photocatalyst to realize efficient hydrogen peroxide production under visible light, and the photocatalytic hydrogen peroxide production performance of the COFs is superior to that of most reported COFs materials. Wherein the yields of HBU-COF-CH3, HBU-COF-H and HBU-COF-OH are as high as 12910 [mu] mol g <-1 > h <-1 >, 8838 [mu] mol g <-1 > h <-1 > and 7679 [mu] mol g <-1 > h <-1 > in sequence.
Owner:HEBEI UNIVERSITY

Inhibitor suitable for soluble alkaline salt scale and preparation method thereof

The invention discloses a soluble alkaline salt scale inhibitor and a preparation method thereof, and belongs to the technical field of oilfield chemistry. The soluble alkaline salt scale inhibitor is prepared from amphiphilic modified graphene oxide, a surfactant, inorganic salt and deionized water, the amphiphilic modified graphene oxide contains a large amount of carboxyl groups, sulfonic acid groups, hydroxyl groups and the like, and has good metal ion chelating property; meanwhile, through the hydrophobic association effect and hydrogen-bond interaction between modified graphene grafted long carbon chains, the bonding probability between sodium ions of the soluble saline-alkali salt and bicarbonate radicals, carbonate radicals and chloride ions is further weakened, and through the synergistic effect of the amphiphilic modified graphene oxide, the surfactant and the inorganic salt, the salt scale inhibition effect is further improved; the method is especially suitable for soluble alkali salt water quality conditions of high temperature, high alkali and high salinity, can solve the problems of oilfield water injection, fracturing flowback strata and wellbore salt deposition, and has a good popularization prospect.
Owner:XINJIANG GUANGYA OIL & GAS NEW TECH DEV CO LTD