The invention discloses a composite
aerogel felt containing organic-inorganic
hybrid hollow microspheres as well as a preparation method and application of the composite
aerogel felt. The method provided by the invention adopts a normal-pressure
drying preparation process and comprises the following steps: adding a
silicon source, a
solvent and
phytic acid into water, carrying out
hydrolysis reaction, and then adjusting the pH value of a
system to obtain a silica
sol solution; adding organic and inorganic
hybrid hollow microspheres into the silica
sol solution, and stirring to obtain a
sol solution containing the organic and inorganic
hybrid hollow microspheres; and soaking a
fiber felt in the sol solution containing the organic-inorganic hybrid hollow microspheres, standing, and
drying to obtain the composite
aerogel felt. The composite aerogel felt provided by the invention is more stable in structure, better in heat insulation performance, free of agglomeration, free of
powder falling, free of repeated washing and replacement, simpler in process and more suitable for large-scale production.