506 results about "Magnetic composite" patented technology

The invention belongs to the technical field of optical fiber sensors, and particularly relates to a distributed optical fiber magnetic sensor, a preparation method thereof and a distributed measurement system. The optical fiber comprises an optical fiber and a magnetic composite matrix, a magnetic field measurement grating and a temperature compensation grating are arranged on the optical fiber; the magnetic composite matrix is formed by curing a magnetic composite suspension coating the outer side of the magnetic field measurement grating, the magnetic composite matrix comprises cured resin and magnetostrictive material particles uniformly distributed in the cured resin, and the magnetostrictive material particles are arranged in the cured resin in a predetermined orientation manner, so that the space monitoring range is expanded, and the magnetostrictive material particles are uniformly distributed in the cured resin; multi-point parallel measurement is achieved, and the defect that single-point measurement is prone to being disturbed by a local magnetic field is overcome; the technical problems of high precision, low cost, difficulty in deployment and long-section measurement of a magnetic field measurement sensor in the prior art are solved.

The invention relates to a repeatedly detachable magnetic composite water lubricated bearing and a maintenance method thereof.The water lubricated bearing comprises a cylindrical bearing seat surrounding a ship stern shaft and a permanent magnet assembly detachably connected with the bearing seat, a cylindrical sliding bearing is arranged on the inner side of the bearing seat, a notch is formed in the outer side face of the sliding bearing, and the permanent magnet assembly is detachably connected with the bearing seat; the notch penetrates through the sliding bearing in the axis direction of the sliding bearing, a containing groove used for containing the permanent magnet assembly is defined between the notch and the inner side wall of the bearing seat, when the water lubrication bearing is arranged on the outer side of the ship tail shaft in a sleeving mode, the containing groove is located over the ship tail shaft, and the permanent magnet assembly is in sliding fit with the containing groove in the axis direction of the sliding bearing. According to the scheme, the permanent magnet is configured to be in a detachable form, and the permanent magnet can be conveniently maintained after being demagnetized, so that the maintenance cost of the water-lubricated bearing is reduced, and the load of the water-lubricated bearing can be reduced for a long time.

The utility model discloses polishing equipment which comprises a polishing wheel, a magnet, a first driving device and a second driving device. The radial side face of the polishing wheel is a polishing face, the magnetic field generating device comprises a plurality of magnets, the magnets are distributed in the first direction, the first direction is parallel to the axial direction of the polishing wheel, and the magnetic field generating device is arranged in the polishing wheel and used for generating a magnetic field on the polishing face so that the magnetic composite fluid can be attracted to the polishing face. The first driving device is connected with the polishing wheel; the second driving device is connected to the magnet; and the first driving device and the second driving device can enable the polishing wheel and the magnet to rotate at different rotating speeds. The magnetic field generating device can generate a dynamic magnetic field on the polishing surface, so that the magnetic composite fluid on the polishing surface is more uniform, the magnetic composite fluid of each flexible grinding head is more uniform, the polishing effect is improved, meanwhile, the abrasion speed of each flexible grinding head can be reduced, the liquid supplementing frequency is reduced, and the polishing efficiency is improved.

Embodiments herein relate to a semiconductor device which includes one or more voltage regulator (VR) chiplets coupled to a package interposer, where the package interposer includes coaxial magnetic composite core inductors to provide power to one or more load die. In one possible configuration, the one or more VR chiplets are coupled to the bottom side of the package interposer, the bottom side of the package interposer is coupled to the top side of a motherboard, and the one or more load die are coupled to the top side of the package interposer. In another possible configuration, the one or more VR chiplets are coupled to the bottom side of the package interposer, the top side of the package interposer is coupled to the bottom side of a motherboard and the one or more load die are coupled to the top side of the motherboard.

The invention provides an aero-engine blade maintenance method and system, a robot and a medium, the method is applied to a micro maintenance robot, and the method comprises the steps that when the rotating speed of an aero-engine is not lower than the preset rotating speed, a magnetic-gas composite driving module is used for obtaining a first moving path according to an edge intelligent center system; moving to a blade detection position of the aero-engine blade corresponding to the first moving path; when the moving stop position of the micro maintenance robot is the blade detection position, the bionic reversible adsorption layer in the adsorption state is adsorbed to the blade detection position; detecting first leaf detection data of a leaf detection area corresponding to the leaf detection position by using a multispectral sensing module, and obtaining a repair strategy based on the first leaf detection data; and a repair module is utilized to perform repair operation on the to-be-repaired blade area in the blade detection area according to the repair strategy. In this way, the detection function and the repair function are integrated, and the purposes of rapid detection and minimally invasive repair are achieved.

The application relates to the technical field of integrally-formed inductors, in particular to a moisture-resistant soft magnetic composite material and a preparation method thereof and an integrally-formed inductor. The moisture-resistant soft magnetic composite material comprises the following components by mass: 100 parts of soft magnetic powder, 2-5 parts of a resin bonding agent and silicon resin, wherein the mass ratio of the silicon resin to the resin bonding agent is (0.3-2.0):100. The moisture-resistant soft magnetic composite material can avoid the phenomenon of explosion of the integrally-formed inductor during a reflow soldering process after moisture absorption.

The invention relates to the field of water purifying agents, and discloses a polyaluminum chloride water purifying agent for printing and dyeing wastewater and a preparation method thereof.The polyaluminum chloride water purifying agent for printing and dyeing wastewater is prepared from polyaluminum chloride, an adsorption additive, magnetic composite filler and the balance deionized water; the adsorption additive is prepared by ultrasonically compounding a modified ZIF-8 coated iron material and modified nano titanium dioxide; the modified ZIF-8 coated iron material is prepared by coating nano zero-valent iron with ZIF-8 and carrying out high-temperature carbonization. The modified nano titanium dioxide is prepared by doping and modifying cerium; the magnetic composite filler is prepared by the following steps: pretreating sepiolite by using hydrochloric acid, then coating the surface of the pretreated sepiolite with chitosan by adopting a coprecipitation method, and loading ferroferric oxide particles into the chitosan. Therefore, the usage amount of polyaluminum chloride is reduced, and the water purifying agent is endowed with excellent photocatalytic activity and adsorption effect in printing and dyeing wastewater.

The invention provides an anti-offset magnetic coupling mechanism for a wireless charging system of an unmanned aerial vehicle, the magnetic coupling mechanism comprises a transmitting end arranged on a landing platform and a receiving end mounted on the unmanned aerial vehicle, and a transmitting coil is a double-layer circular coil wound at gradient intervals; an axial magnetic field which is uniformly distributed is formed through a non-uniform distribution structure of coil turn spacing; the receiving end is composed of four sets of same magnetic core-coil structures, each set is composed of a lightweight cylindrical novel soft magnetic composite material magnetic core and an externally-wound solenoid coil of a vertical landing gear of the unmanned aerial vehicle, the magnetic cores are located in the vertical landing gear of the unmanned aerial vehicle, and the coils of the four magnetic core-coil structures are closely wound in the axial direction of the outer surface of the landing gear and connected in series. And coil and magnetic core parameters are designed by using an evolutionary algorithm. The problems that in a traditional scheme, the anti-offset capacity is weak, the magnetic core weight is large, and the receiving end is not matched with the special-shaped structure of the unmanned aerial vehicle are solved, and the method is suitable for unmanned aerial vehicle wireless charging scenes.

The invention discloses a preparation method of a wear-resistant magnetic composite nano ferroferric oxide material, and belongs to the technical field of nano ferroferric oxide materials.The preparation method comprises the steps that coated modified ferroferric oxide composite powder, silver nitrate and absolute methanol are added into a reaction kettle, stirring and ultrasonic dispersion are conducted, then 2-aminoterephthalic acid is added, stirring and mixing are conducted, and a mixture is obtained; and after the reaction, separating to obtain the wear-resistant magnetic composite nano ferroferric oxide material. The wear-resistant magnetic composite nano ferroferric oxide material prepared by the preparation method disclosed by the invention overcomes the problem that an existing ferrite material is relatively single in electromagnetic loss mechanism in the aspect of nickel-phosphorus plated fabric, and the electromagnetic shielding effectiveness of the fabric is improved; the coated modified ferroferric oxide composite powder has good dispersity, a polydopamine coating layer on the surface of the coated modified ferroferric oxide composite powder improves the anchoring effect on silver MOF particles through a mussel-like adhesion interface, meanwhile, stress is dispersed and crack propagation is reduced through the buffering effect of the polydopamine coating layer, and the mechanical stability of the wear-resistant magnetic composite nano ferroferric oxide material is improved.

The invention relates to the technical field of biomedical materials, in particular to collagen sponge and a preparation method thereof.The preparation method comprises the following steps that under the condition of 4-8 DEG C, silver-containing turbid liquid is added into a collagen solution, ultrasonic treatment is conducted, magnetic stirring is matched at the same time, and a mixed solution is obtained; performing high-pressure homogenizing and refining treatment on the mixed solution to obtain a homogenized solution; freezing the homogenized liquid at-80 DEG C, and then unfreezing at 4-37 DEG C to obtain pretreated homogenized liquid; and carrying out freeze drying on the pretreated homogeneous liquid to obtain the collagen sponge. According to the preparation method disclosed by the invention, a low-temperature ultrasonic-magnetic composite dispersion method is combined with homogenizing treatment, so that silver salt is uniformly dispersed in a collagen solution on the premise of avoiding thermal denaturation of collagen; and then a freezing-unfreezing pretreatment process is combined, so that the hydrogen-bond interaction between the silver salt uniformly dispersed in the collagen solution and the collagen is enhanced, the binding force between the silver salt and the collagen is improved, and sudden release of the silver salt is avoided.

The invention discloses a soft magnetic composite material, a soft magnetic core ring and a preparation method and application thereof. The preparation method of the soft magnetic composite material comprises the following steps: 1) providing raw materials according to the chemical composition of the soft magnetic material; the raw materials are smelted and rapidly hardened, and soft magnetic material master alloy is obtained; the chemical composition of the soft magnetic material is RE2 (FexCo1-x) 14B, and RE is selected from at least one of La, Ce, Pr, Nd, Sm, Eu and Gd; x is the atomic ratio of Fe, 0.7 < = x < = 1; 2) heating the soft magnetic material mother alloy in vacuum to obtain a soft magnetic material phase alloy; (3) the soft magnetic material phase alloy is prepared into powder with the particle size of 75-200 microns, and soft magnetic material powder is obtained; 4) mixing the soft magnetic material powder with an amino compound to obtain mixed powder; and heating the mixed powder under the conditions of protective gas and 300-600 DEG C to prepare the soft magnetic composite material. The prepared soft magnetic composite material is high in effective magnetic conductivity and low in unit volume power loss.

The invention provides a secondary battery and a manufacturing method thereof, a battery device, an energy storage device and a power utilization device, which are at least beneficial to improving the performance of the secondary battery. The manufacturing method comprises the steps that magnetic composite filler comprising an ionic conductor core is prepared, the surface of the ionic conductor core is sequentially coated with a magnetic functional layer and a protective layer, the magnetic functional layer is made of a magnetic material, and the protective layer is made of an oxide; preparing a polymerization precursor comprising the magnetic composite filler, a polymer matrix, an initiator, a lithium salt and a solvent; coating the polymeric precursor under a pulsed magnetic field to form a film, so that the magnetic composite filler is directionally arranged along the thickness direction of a film layer; initiating the polymerization precursor to generate polymerization reaction, so that the polymerization precursor is cured and molded into a solid electrolyte membrane; a positive plate and a negative plate are provided, the positive plate, the solid electrolyte membrane and the negative plate are subjected to winding treatment or lamination treatment and then put into the shell, and an initial battery cell is formed.

The invention discloses a plate flexible laser cutting production line and method integrating uncoiling, flattening and robot grabbing, and belongs to the technical field of metal plate machining. The plate flexible laser cutting production line comprises the steps that S1, an uncoiling and flattening mechanism, a gas-magnetic composite suspension bed and a sorting robot with a Bernoulli gripper are configured; s2, the coiled materials are fed into a suspension bed, the levelness is locked through permanent magnet attraction, and non-contact suspension and locking flat conveying of the plates are achieved in cooperation with the lifting force of a micropore air cushion; s3, laser head follow-up cutting is carried out, and plate local warping caused by thermal stress release is restrained through a permanent magnetic field; and S4, negative pressure lift force is generated through the Bernoulli effect, and when the lift force overcomes the resultant force of the magnetic attraction force, the gravity and the friction force, the workpiece is separated from the crawler belt and stripped from the framework. The air-magnetic composite suspension bed is constructed, the permanent magnet array is used for generating downward background magnetic attraction force, meanwhile, the high-pressure air bellow is used for spraying airflow through the micropore array to generate air cushion lift force, the plate is in a non-contact suspension state, and the risk of surface scratching is remarkably reduced.

The invention belongs to the technical field of preparation of soft magnetic composite materials, and particularly relates to an insulation coating method and application of a soft magnetic powder material. The insulating coating method comprises the following steps: (1) uniformly mixing low-melting-point metal or alloy powder with silica sol, a silane coupling agent and a thermocuring resin glue solution to obtain coating slurry; and (2) uniformly mixing soft magnetic powder with the coating slurry obtained in the step (1), firstly performing hot-pressing curing molding at the temperature of 60-100 DEG C under a vacuum condition, and then performing hot-pressing sintering treatment at the temperature higher than the melting point temperature of low-melting-point metal or alloy powder and under an oxygen-containing atmosphere condition to obtain the insulated and coated soft magnetic powder material. According to the insulating coating method, the advantages of an organic material insulating coating method and an inorganic material insulating coating method are combined, the defects of the organic material insulating coating method and the inorganic material insulating coating method are overcome, and the stability and the insulating coating effect of the insulating coating layer are remarkably improved.

The present invention provides an iron-based nanocrystalline soft magnetic alloy powder, a soft magnetic composite material and a preparation method thereof, belonging to the technical field of soft magnetic materials. The iron-based nanocrystalline soft magnetic alloy powder has a heterogeneous nanocrystalline structure comprising a three-dimensional island-shaped amorphous region and a nanocrystalline region. The diameter of the three-dimensional island-shaped amorphous region is 50-100 nm, and the number density of the three-dimensional island-shaped amorphous region is 10 19 ‑10 20 m ‑3 The iron-based nanocrystalline soft magnetic alloy powder has the advantages of high sphericity, high saturation magnetization and low coercive force; the soft magnetic composite material comprises soft magnetic powder and a coating layer coated on the surface of the soft magnetic powder, and the coating layer comprises a binder, wherein the soft magnetic powder is the iron-based nanocrystalline soft magnetic alloy powder provided by the present invention, or is composited with at least one of iron-nickel, iron-nickel-molybdenum, iron-silicon, iron-silicon-aluminum, iron-silicon-chromium, carbonyl iron and pure iron powder, and has the advantages of low high-frequency loss, high magnetic permeability and high DC bias.

The invention belongs to the technical field of electronic materials, and particularly relates to a FeSiAl soft magnetic composite material and a preparation method thereof.The preparation method comprises the steps that 1, FeSiAl powder, a silane coupling agent and organic silicon resin are mixed to obtain coated powder; (2) carrying out heat treatment on the coated powder to obtain FeSiAl-coated Al2SiO5 powder; and (3) mixing the FeSiAl-coated Al2SiO5 powder with a lubricant, and carrying out annealing heat treatment to obtain the FeSiAl soft magnetic composite material. The FeSiAl soft magnetic composite material prepared by the method has high magnetic conductivity and lower loss, the insulating layer is compact, the corrosion resistance is excellent, and the preparation method is simple in process, simple and convenient in equipment, short in coating treatment time, high in efficiency, low in cost and suitable for large-scale production.

The invention relates to the technical field of magnetic materials, in particular to a low-loss high-direct-current-bias soft magnetic composite material and a preparation method and application thereof.The low-loss high-direct-current-bias soft magnetic composite material is composed of nanometer titanium dioxide and iron-silicon-aluminum alloy powder; the nano titanium dioxide and the iron-silicon-aluminum alloy powder are combined in a core-shell structure form, the iron-silicon-aluminum alloy powder is used as a core, and the outer side of the iron-silicon-aluminum alloy powder is coated with a nano titanium dioxide shell. The soft magnetic composite material with low loss and high direct current bias has high direct current bias performance, relatively high magnetic conductivity and relatively low high-frequency loss, meanwhile, the preparation process of the soft magnetic composite material is simple, the prepared material has stable performance and very high direct current bias performance, and the soft magnetic composite material can be used for industrial batch production and has a wide application prospect.

The invention relates to the technical field of flexible composite materials, in particular to an ultrathin flexible magnetic composite material and a preparation method and application thereof.The ultrathin flexible magnetic composite material comprises a polymer matrix and a composite absorbent, and the composite absorbent comprises samarium-iron-nitrogen magnetic powder subjected to surface treatment through phosphoric acid and a benzotriazole corrosion inhibitor, the core-shell structure complex is formed by ferroferric oxide nanoparticles and reduced graphene oxide through chemical bonding; a hyperbranched polyamide-amine dispersant; the polymer matrix is adopted, thermoplastic polyurethane / polydimethylsiloxane is used as a flexible framework, mechanical support and processing fluidity are provided, the glass transition temperature is lower than 25 DEG C, and it is ensured that the material keeps high flexibility at the room temperature. The soft segment of the thermoplastic polyurethane endows the material with elasticity, and the hard segment forms a physical crosslinking point to balance strength and flexibility; a silicon-oxygen bond structure of polydimethylsiloxane endows the material with low-temperature flexibility and chemical stability, and the material is suitable for sensitive scenes such as medical treatment.

The invention designs a preparation method of a magnetic molecular imprinting-aptamer sandwich fluorescence sensor for detecting kanamycin. And the magnetic molecular imprinting composite material Fe3O4 (at) UiO-66 (at) MIP with a specific adsorption target object KANA is prepared. When a detection target object KANA exists, the Fe3O4-coated UiO-66-coated MIP can rapidly and specifically capture the KANA in a short time. Then, a DNA single-stranded aptamer marked with FAM is added, after the aptamer and KANA captured on the surface of the Fe3O4 at-UiO-66 at-MIP are subjected to specific recognition and magnetic separation again, an aptamer probe can enter sediment along with the magnetic composite material Fe3O4 at-UiO-66 at-MIP, the fluorescence intensity of supernate is reduced, and quantitative analysis is conducted according to the fluorescence difference value delta F. When the KANA does not exist, the aptamer cannot enter the precipitate, so that the fluorescence signal intensity is not changed. Double recognition is formed through specific binding of an MIP imprinting cavity and the aptamer, matrix interference is reduced by means of fluorescence characteristics and magnetic separation capacity, the method has the advantages of being high in adsorption capacity, specific in recognition, high in sensitivity, wide in detection range, good in selectivity and the like, and rapid and accurate detection of KANA in a complex sample can be achieved.

The invention discloses a 2: 17 type rare earth soft magnetic / Fe-based soft magnetic laminated composite material and a preparation method thereof. The method sequentially comprises the following steps: 1) screening 2: 17 type rare earth soft magnetic powder, performing insulation coating, mixing with polyurethane, and performing magnetic field orientation to obtain a thin ring green body; (2) Fe-based soft magnetic powder is sieved and mixed with polyurethane, and then a thin ring green body is obtained through magnetic field orientation; (3) alternately stacking the 2: 17 type rare earth soft magnetic thin ring green bodies and the Fe-based soft magnetic thin ring green bodies in the direction perpendicular to the plane of the thin ring green bodies; and 4) carrying out hot press molding on the laminated soft magnetic composite material. Based on the high-frequency characteristic of the 2: 17 type rare earth soft magnetic material and the high magnetic conductivity characteristic of the Fe-based soft magnetic material, collaborative optimization of the magnetic conductivity and the cut-off frequency is achieved within the ultra-wideband range from MHz to GHz, the problem that the magnetic conductivity of a traditional soft magnetic composite material is attenuated along with the frequency is effectively solved, high-frequency loss is greatly reduced, and the service life of the soft magnetic composite material is prolonged. And a solution is provided for high-frequency soft magnetic components (such as inductors and transformers) with high magnetic performance and low power consumption.

The invention provides a solvent-free resin composition and application thereof, the solvent-free resin composition comprises a functional reinforcing phase and a continuous matrix phase, and the functional reinforcing phase comprises a magnetic composite filler; the magnetic composite filler comprises the following components: (A1) FeMn ferrite and / or carbonyl iron, wherein D50 is 0.1-0.9 [mu] m; (A2) FeMn ferrite and / or carbonyl iron, wherein D50 is 1 to 10 [mu] m; (B) a FeSiCr alloy and / or an iron-based nanocrystal, wherein D50 is 1 to 20 [mu] m. According to the resin composition provided by the invention, the magnetic filler with a specific particle size is introduced, and the specific type of the magnetic filler is limited, so that the resin composition has excellent magnetic performance, high magnetic conductivity and low magnetic loss at high frequency (10MHz-100MHz), and the resin composition is solvent-free, has relatively good stability and can realize high filling property.

The invention belongs to the technical field of bionic cilium sensors, and particularly discloses a magnetic bionic cilium and vesicle complex and a preparation method and application thereof.The preparation method comprises the following steps that S1, a cilium array male mold is prepared; then carrying out oxygen plasma treatment, silanization and curing stabilization; s3, injecting the magnetic composite precursor into a polydimethylsiloxane female die, applying pressure, and striking off; and S4, coating the mold surface with an Ecoflex precursor, performing thermocuring forming, performing magnetization treatment, and performing stripping to obtain the magnetic bionic cilia. According to the magnetic bionic cilia, the vesicle complex and the preparation method and application of the magnetic bionic cilia, the vesicle complex and the preparation method and application of the magnetic bionic cilia, high-magnetic signal output is achieved while the deformability of the cilia is guaranteed, the magnetic bionic cilia is used for non-contact real-time hemodynamic monitoring, meanwhile, specific response release of the vesicle complex is achieved, and a new thought is provided for design of responsive vascular implants.

The invention discloses an elastic support liquid magnetic composite bearing journal bearing which comprises a bearing bush, a base body arranged on the outer side of the circumference of the bearing bush and a support layer arranged between the base body and the bearing bush, the bearing bush comprises a first permanent magnet layer and a lining layer arranged between the first permanent magnet layer and a journal, the lining layer is provided with a liquid film, the liquid film is arranged between the lining layer and the journal, and the first permanent magnet layer is arranged on the lining layer. The first permanent magnet layer comprises a permanent magnet and a protective shell thereof; a second permanent magnet layer is further arranged on the inner side of the circumference of the liquid film, and the supporting layer comprises an elastic layer arranged between the bearing bush and the base body; the elastic layer comprises elastic elements; according to the bearing, the liquid film is arranged between the lining layer and the shaft neck, and the permanent magnets are arranged in the first permanent magnet layer and the second permanent magnet layer, so that a dynamic complementary mechanism of liquid film dynamic pressure and magnetic suspension force is formed, and the comprehensive bearing capacity is improved.

The invention discloses a high-insulativity coating treatment method of a metal soft magnetic composite material, which belongs to the technical field of metal soft magnetic materials, and comprises the following steps: firstly, performing vacuum dehydration treatment on metal soft magnetic powder, and controlling the moisture content to be not higher than 0.1%; carrying out ultrasonic dispersion treatment on the boron nitride nanosheets to form a suspension, and modifying the magnesium borate nanowires and a silane coupling agent for later use; preparing an inorganic coating solution and an organic coating solution; activating the powder in the fluidized bed by adopting radio frequency plasma of argon-oxygen mixed gas; enabling the activated powder to enter a three-fluid nozzle fluidized bed reactor, and implementing synchronous spray coating in two stages: in the first stage, spraying inorganic coating liquid and applying pulse plasma to form a composite bottom layer; in the second stage, spraying organic coating liquid and carrying out ultraviolet precuring to form a resin layer; and the coated powder is treated by a stepped thermocuring procedure to obtain a finished product. The technical problem of how to improve the insulation coating performance of the metal soft magnetic composite material is solved.

The application provides a quartz sand acid washing waste liquid resource treatment method, and belongs to the field of industrial waste water treatment, and comprises the following steps: adding magnetic composite seeds to the quartz sand acid washing waste liquid, and performing magnetic separation after stirring treatment; adding soluble potassium salt to the treated waste liquid to recover potassium fluosilicate; treating the filtrate through diffusion dialysis to obtain recovered acid and dialysis residual liquid; the diffusion dialysis treatment adopts an asymmetric membrane, the asymmetric membrane has a physical gradient of one side being a dense structure and the other side being a loose structure, and the dense structure side is in contact with the waste liquid; and adding calcium oxide or calcium hydroxide to the dialysis residual liquid for deep treatment and calcium recovery. The application provides a quartz sand acid washing waste liquid resource treatment method which is low in treatment cost, high in resource recovery rate and friendly to the environment, and realizes the differentiated resource recovery of the quartz sand acid washing waste liquid.

The invention discloses a FeNi soft magnetic composite material based on tetrabutyl orthosilicate hydrolysis coating and a preparation method of the FeNi soft magnetic composite material. According to the method, through a controllable sol-gel process, tetrabutyl orthosilicate is hydrolyzed to generate SiO2 gel, then a uniform and ultrathin SiO2 gel layer is generated on the surface of FeNi powder in situ, and then heat treatment densification is performed to obtain the FeNi soft magnetic composite material coated with SiO2 in an insulation mode. The SiO2 insulating layer is firmly combined with the matrix metal powder, the thermal stability is good, high frequency and high resistivity are achieved, and meanwhile dilution of non-magnetic relative magnetic performance is reduced to a great extent. The final magnetic core is obtained through compression molding and annealing heat treatment, has the excellent characteristics of high effective magnetic conductivity and low high-frequency magnetic core loss, and is particularly suitable for various efficient and miniaturized power electronic devices in the MHz frequency band.

The invention provides a magnetic composite material and a preparation method and application thereof. The preparation method comprises the steps that mixed dispersion liquid containing a magnetic material, a magnesium source, a phosphorus source and a solvent is provided, the phosphorus source contains phosphate radicals or can be decomposed into phosphate radicals in the solvent, the pH value of the mixed dispersion liquid is controlled to be 7-12, the magnesium source and the phosphorus source are subjected to a chemical reaction, and the magnetic material is obtained. A magnesium-containing coating layer is formed on the surface of the magnetic material, the magnesium-containing coating layer contains Mg, P and O elements, and the magnetic composite material is obtained. According to the preparation method provided by the invention, the magnesium-containing coating layer which is uniform, compact, high in binding force and hard can be formed on the surface of the magnetic material, and the magnesium-containing coating layer is excellent in high-temperature resistance and high-pressure resistance and is not easy to crack in the hot-pressing treatment process.

The application provides a method for preparing a soft magnetic composite material curing curve, comprising the following steps: preparing a magnetic ring, wherein the material of the magnetic ring comprises a soft magnetic composite material; heating the magnetic ring at different temperature values; testing the crushing strength of the magnetic ring at different heating times at each temperature value; determining the optimal curing time of the soft magnetic composite material at the temperature value according to the crushing strength; and preparing a soft magnetic composite material curing curve according to the crushing strength and the optimal curing time. The soft magnetic composite material curing curve prepared according to the application can shorten the curing time of the soft magnetic composite material, thereby improving the production efficiency. The application also provides a soft magnetic composite material curing curve prepared by the preparation method.

The application provides a semiconductor structure preparation method, a semiconductor structure and a memory. The semiconductor structure preparation method comprises the following steps: providing a substrate; sequentially forming a magnetic composite layer and a transfer mask layer on the substrate; performing a plurality of mask etching processes on the transfer mask layer to form a plurality of mask patterns arranged in an array in the transfer mask layer, and the transfer mask layer between at least part of the mask patterns forms a transfer pattern; and etching the magnetic composite layer along the transfer pattern to form a plurality of columnar structures arranged in an array, and the columnar structures form magnetic tunnel junctions. Adjacent columnar structures are isolated by gaps. The application facilitates the preparation of a semiconductor structure with high-density magnetic tunnel junctions, and can effectively adjust the size of the magnetic tunnel junctions and reduce the difficulty of preparing the semiconductor structure.

The invention discloses myricetin-loaded bone-targeted magnetic composite nanoparticles and a preparation method thereof. The preparation method comprises the following steps: step 1, preparing nanoparticles taking ferroferric oxide as an inner core; step 2, preparing magnetic mesoporous silica nanoparticles with ferroferric oxide as an inner core according to the nanoparticles prepared in the step 1; step 3, performing amination modification treatment on the surfaces of the magnetic mesoporous silica nanoparticles prepared in the step 2 to obtain magnetic mesoporous silica modified nanoparticles; step 4, preparing a ketal thiol-polyethylene glycol-aspartic acid hexapeptide molecule; and step 5, loading myricetin on the magnetic mesoporous silica modified nanoparticles prepared in the step 3, and blocking myricetin by using the ketal thiol-polyethylene glycol-aspartic acid hexapeptide molecules prepared in the step 4 after loading. The invention further discloses application of the compound in image tracing in osteolysis and treatment drugs.