The invention discloses a field rapid
analysis method for trace gold, which comprises the following steps: S1, ore
dissolution: taking a rock mineral sample in a container, adding a dissolving agent, and heating until the sample is slightly boiled for high-temperature ore
dissolution; the dissolving agent is
hydrochloric acid,
potassium nitrate and
nitric acid; s2, enrichment: adding
polypropyleneimine into the mineral solution, standing, taking
clear liquid, diluting with
hydrochloric acid, slowly dropwise adding to pass through an adsorption column filled with sulfydryl cotton, taking out the sulfydryl cotton, and washing with a
solvent; s3, secondary ore dissolving after
ashing: squeezing the washed sulfydryl cotton to be dry, heating until the sulfydryl cotton is ashed, then adding
hydrochloric acid, and
drying by
distillation in a water bath; s4, determination: adding a
masking agent and hydrochloric acid after
drying by
distillation, transferring to a colorimetric tube, dropwise adding
urea and a TMK color developing agent, uniformly mixing, standing, and carrying out visual
colorimetry with a standard series; the
masking agent is a mixture of
malic acid,
glutaric acid and
ethylenediaminetetraacetic acid. According to the method, trace gold can be effectively enriched, and the method is
safer and more convenient while the analysis sensitivity and accuracy are guaranteed.