The invention discloses a method for detecting the content of
carbon black in master batch, which comprises the following steps: S1) weighing the master batch with the
mass G into a
reaction tube, adding
methanol, a cosolvent and a catalyst, sealing, and heating for alcoholysis; s2) taking out the
reaction tube, cooling to
room temperature, opening a cover, pouring a solution in the
reaction tube into
filter paper with the
mass of W0, flushing the reaction tube with
ethanol, pouring the solution into the
filter paper to completely transfer the solution, flushing filter residues with hot absolute
ethanol, and
drying the
filter paper with the filter residues, wherein the
mass of the dried filter paper and the filter residues is W1; s3) putting the dried filter paper with the filter residues into a
crucible with the mass of W2,
ashing, transferring the
crucible into a
muffle furnace, calcining, and weighing the mass of the
crucible and the ash content as W3 after the weight is constant; and S4) calculating the
carbon black content in the master batch according to the following formula:
omega = (W1-W0) / G * 100%-(W3-W2) / G * 100%. According to the method, ash content in the detection result is removed, the accuracy is high, the test
repeatability is good, the operation is simple, and the
energy consumption in the detection process is low.