The application discloses a preparation method of nano-
graphene lubricating oil and relates to the technical field of lubricating oil. The modified
zirconium-
titanium composite particles are used as a catalyst to synthesize
base oil, so that the
heat resistance effect is improved; then, under the assistance of microwaves,
graphene is stripped to improve the dispersibility of the
graphene in the lubricating oil, and a
hydrogen bond network is formed on the surface of the modified
zirconium-
titanium particles, so that the fatigue wear is reduced, and the service life is prolonged; on the basis, electrochemical deposition is generated between the particles and the graphene in the friction process, so that the self-repairing effect is achieved. The modified
zirconium-
titanium composite particles are first injected into pre-cooled
liquid nitrogen copper molds by precursor
sol, are rapidly frozen, are dried by
vacuum sublimation to remove
ice crystals, and form
snowflake-like
hierarchical porous structures, so that the lubricating effect is improved; then, low-temperature annealing is performed to form Zr-O-Ti
mixed oxide skeletons, so that the pore collapse is effectively inhibited, and the service life is prolonged; and then, through the surface hydroxyl groups and
capillary action, ionic liquids are adsorbed to form a
coating layer, so that the lubricating effect is enhanced.