The invention discloses a Cr-rich multiphase six-element non-
noble metal high-entropy
alloy and a preparation method thereof, and belongs to the technical field of magnetic high-entropy alloys. The preparation raw materials comprise 65 to 70 at.% of Cr, 1 to 5 at.% of Fe, 1 to 5 at.% of Co, 1 to 5 at.% of Ni, 10 to 15 at.% of Al and 10 to 15 at.% of Mo, and the total amount is 100 at. The preparation method comprises the following steps: (1) uniformly mixing the raw materials; (2) continuously introducing
argon; (3) raising the temperature at a
constant speed, synchronously increasing the
argon flow velocity, keeping the temperature at 1200 DEG C for 16 hours, and reducing the
argon flow velocity; (4) cooling at a
constant speed, synchronously increasing the
argon flow velocity, keeping at 900 DEG C for 10 hours, and reducing the
argon flow velocity; and (5) cooling at a
constant speed, keeping the
argon flow speed, and rapidly cooling to
room temperature. According to the preparation method, a precise six-element non-
noble metal element
doping strategy is combined with a one-step heat treatment and staged rapid cooling process, so that cooperative regulation and control of high
Curie temperature Tc and low saturation
magnetization Ms are realized at low cost, and the key bottlenecks of high magnetic loss, poor
magnetic stability and the like of a traditional magnetic material are effectively broken through; and a material basis is provided for development of new-generation high-frequency and high-temperature magnetic devices.