3727results about How to "Large amount of processing" patented technology

The invention discloses a method for comprehensive treatment of oilfield waste, which is characterized by comprising the process steps of cleaning and separation, ultrasonic separation, tempering and destabilization, oil-water separation, centrifugal separation, mixed curing, air floatation separation, adsorption filtration, flocculating settling, oxidization electrolysis, deep purification and permeable filtration. Thus, the oilfield waste is treated and utilized in a classified manner, so that sump oil is recovered, the solid phase achieves the discharge standard of oilfield sludge treatment design specifications (SY/T6851-2012) or is reutilized for construction material manufacturing, and the liquid phase achieves the sewage comprehensive discharge standard (GB8978-1996) after being subjected to water treatment.

The invention relates to a method for preparing graphene powder in large scale, which is characterized by comprising the following steps of: firstly, uniformly peeling graphene oxide into a graphene oxide suspension solution; then, atomizing the graphene oxide solution by using the spray drying technology comprising spray pyrolysis drying and spray freeze drying, and removing a solvent to obtain graphene oxide powder; and finally, oxidizing grapheme by using the non-expansion heat treatment process to obtain non-agglomerative graphene powder. The continuous preparation process of the spray technology and the non-expansion heat treatment process ensure the large-scale preparation of the graphene powder. The prepared graphene powder comprising intermediate product graphene oxide powder does not have agglomeration and has good dispersivity in the solvent. The graphene powder is used as a filling material to prepare high strength composite materials, conductive composite materials, novel air-tight flame-retardant composite materials, novel nanodevices and the like.

The invention relates to method and device for gasifying a multi-segment staged converted fluidized bed. The method comprises the following steps of: supplying coal; supplying gas; gasifying; slagging; and conveying fine powder. The device for gasifying the multi-grade staged converted fluidized bed comprises an agglomerating ash separating unit, a pyrolyzing and gasifying reactor of the multi-segment staged fluidized bed and a semicoke fine powder cyclic feeding unit. The invention has the advantages of high volume utilization rate of a gasifying oven, great handling capacity and high utilization rate of total carbon, is suitable for a coal staging and converting system and can be singly used for producing gas for mass coal-based methane synthesis and coal chemical industry.

The invention provides a membrane dispersion microchannel reactor. An outer pipe and an inner pipe form a bushing, an annular microchannel is formed between the inner pipe and the outer pipe, and the outer pipe is provided with a fluid inlet and a fluid outlet; and one end of the inner pipe is provided with a fluid inlet, while the other end is distributed with a micrporous membrane with a plurality of micropores along the circumferential direction of the pipe wall. Compared with the prior microchannel reactor, the cross section of the channel of the reactor is increased, and the treatment capacity is increased. The mixing and the mass transfer between fluids are strengthened. The stronger micromixing is also guaranteed when the large treatment capacity is achieved. Particularly the rapid micromixing is realized in the synthesis of nanometer particles, and barium sulfate particles with the average particle size of 37 nanometers are synthesized. The reactor has the advantages of simple operation, low operation cost, and large treatment capacity, and has good application prospect in the industrial production relating to the rapid process.

A catalyst for preparing isobutene by cracking methyl turt-butyl ether (MTBE) is prepared from the amorphous SiAl through treating by saturated steam at 100-600 deg.C for 1-10 hr. Its advantages are high conversion rate of MTBE, high selectivity to isobutene, and long service life (at least 3504 hr).

The present invention provides a method for comprehensively treating high salt content organic industrial wastewater, and relates to the field of the organic material preparing technique. The method of the invention mainly comprises the following steps: executing acid-alkali adjustment to the organic wastewater until pH=7-9, preheating to 30-60 DEG C; introducing the wastewater into a triple effect evaporator for executing triple effect evaporation, executing salting out to the evaporated wastewater which is condensed to a certain degree so that the solid and liquid are separated; separating the concentrated liquid for continuing the condensation; when the separated liquid satisfies a certain requirement, atomizing into an incinerator for incinerating and discharging according to the standard, and introducing the triple effect evaporation condensation water into a biochemical treating system. The method of the invention can totally dispose and remove the organic matter in the high salt content organic industrial wastewater so that the high salt content organic industrial wastewater can be charged according to the standard. The method of the invention has the advantages of unique method, simple technical process, easy operation, low operation cost, large treating capacity, low regeneration energy consumption, no easy forming of secondary pollution after abandon, better economic and social benefit, and wide application range. The method of the invention can be widely applied for the treating of the high salt content organic wastewaters of garbage penetrating fluid, dye intermediate wastewater, etc.

The invention relates to a methane-generating pit using poultry excrement, which is integrally horizontally placed under the water plane. Partition walls are arranged in the middle of the methane-generating pit for dividing the whole methane-generating pit into a plurality of unit methane-generating pits, and medium channels arranged on the partition walls are communicated with each other. An annular fermentation tank is arranged above the periphery of the methane-generating pit, a plurality of superconductive heat pipes are arranged on the inner side of the annular fermentation tank, and the superconductive heat pipes are inserted into the methane-generating pit. A material inlet and a material outlet are respectively arranged at two ends of the methane-generating pit and under the unit methane-generating pits at two ends of the methane-generating pit, a methane collector is arranged above each unit methane-generating pit, and the methane collectors are directly communicated with a gas storage tank through pipelines. The methane-generating pit has the advantages of being high in material concentration, integrating material inlet, deslagging, methane generating, stirring, temperature controlling, regulating and the like, being high in mechanization degree, large in treating quantity, fast in digesting rate and the like and can meet requirements for scale production, and concentration of inlet materials of a continuous methane-generating pit can reach about 15%.

An optical fiber including: (i) a silica based, rare earth doped core having a first index of refraction n₁; and (ii) at least one silica based cladding surrounding the core and having a second index of refraction n₂, such that n₁>n₂, said cladding having a plurality of stress rods and a plurality of air holes extending longitudinally through the length of said optical fiber; wherein said optical fiber supports a single polarization mode or poses-polarization maintaining properties within the operating wavelength range.

The invention relates to a method for preparing a nano-cellulose antibacterial composite material through on-line culture. The method comprises the following steps of: (1) inoculating an activated bacterial cellulose producing strain into a liquid culture medium, performing amplification culture, transferring the liquid culture medium into a bioreactor, culturing, adding an antibacterial material into the liquid culture medium, and continuing to culture to obtain an unpurified antibacterial bacterial cellulose composite material; and (2) peeling a bacterial cellulose membrane from a framework or directly soaking the composite material in a NaOH solution, treating in water bath, and washing until an obtained product is neutral to obtain the nano-cellulose antibacterial composite material. The preparation efficiency is high, and the method is simple, convenient, feasible and low in cost; and the surface of the bacterial cellulose composite material has a nanoscale three-dimensional fibrous mesh-shaped structure, the tensile strength of the material is greatly improved compared with that of a pure bacterial cellulose membrane, and the material can be widely applied to products such as facial masks, wound dressings, plasters, artificial skins and the like.

The invention provides a process and device for carrying out stage dry distillation on oil shale under the state of full recycle, with the gas as the heat carrier. The oil shale is divided into three different sizes (such as 0-6mm, 6-20mm and 20-50mm) through crushing and screening, and the oil shale is firstly dried and heated to the temperature between 50 DEG C and 150 DEG C by the waste smoke exhausted from gas heating furnaces and then enters into the different sizes of furnaces for dry distillation to undergo dry distillation. After being treated by water spraying and an indirect cooling tower, a rotary trapper and an electric trapper for oil collection, the dry distillation oil and gas undergo oil-gas-water separation, and after separation, the oil enters into a storage tank, the water enters into a circulating water tank and the first part of gases serves as the heat carrier and is recycled, the second part of gases is used as the fuels for the heating furnaces and the third part of gases is used as the fuel gases for power generation.

An information management method using a managing symbol and an information management server for managing a plurality of electronic contents and automatically performing an action according to each content. Association between a bit string assigned to each content and the storage address of the content is stored, and a managing symbol representing the bit string is published. The association is referred to specify the content correspondent to the bit string. The action to be performed on the content is decided by referring to an action type selected beforehand.

An RFID tag comprises a semiconductor chip storing therein information of an object to be discriminated and carrying out radio communication with a reader/writer device; and an antenna coil provided with a magnetic core member and connected electrically to the semiconductor chip. The semiconductor chip and the magnetic core member are wrapped by an insulation sheet carrying an interconnection pattern connecting a pad of the semiconductor chip and the antenna coil electrically and plural coil patterns on one side thereof. The plural coil patterns includes bar-shaped conductor patterns formed obliquely to the magnetic core member, each of the bar-shaped conductor patterns having an end connected to an end of an adjacent coil pattern, the bar-shaped conductor patterns thereby forming together a spiral coil around the magnetic core member. The coil patterns being connected with each other at a part where the coil patterns overlap with each other.

The invention relates to a process by adopting supercritical water oxidation technology to treat coking wastewater or organic wastewater. The invention is that: coking wastewater or organic wastewater is pretreated to obtain wastewater without solid granules; the wastewater is heated to 380-450 DEG C with a first interchanger and/or a supercritical boiler, and then enters demineralizing equipment to remove the salt in the wastewater by taking advantage of the property that supercritical inorganic matter is indissoluble; the wastewater after desalting is put in a reaction kettle to generate autothermal reaction with an heated and pressurized oxidant to obtain high-temperature gas-liquid mixture with higher temperature; the high-temperature gas-liquid mixture enters the first interchanger and acts as thermal medium to exchange heat with new coming coking wastewater or organic wastewater and then goes through a secondary interchanger to enter a cooler and is cooled to normal temperature, after pressure thereof is adjusted by a pressure regulation device, the high-temperature gas-liquid mixture enters a gas-liquid separator for separation, and then the air is discharged, while the liquid, namely the treated water is recycled. The organic contamination and oxidant are all dissolved in the wastewater; oxidation reaction is generated in homogeneous phase, in short reaction time, oxygenolysis of organic contamination is carried out quickly.

The invention relates to an iron powder production method by using a tunnel kiln to reduce concentrate pellets containing carbon vanadium ferrotitanium with titanium slag and vanadium pentoxide as combined products. Concentrate pellets are made from vanadium-titanium iron concentrate through crashing and damp milling. The iron powder and tailings are obtained by putting the concentrate pellets into the tunnel kiln to be reduced, crashing, wet-grinding, magnetic separation and gravity separation. The tailings are soaked with titania waste acid to eliminate remnants magnesium and iron. Then the tailings are filtrated and dried to obtain a new material. And then the new material is added with sodium salt to do salt roast and then to be soaked by water, then titanium slag and sodium vanadate are obtained respectively after the water soaking. At last, the vanadium pentoxide is obtained by ammonium vanadate precipitating and calcination deaminase to the sodium vanadate liquid. The invention eliminates the disadvantage of high energy consumption by electric furnace smelting and bad separating effect of vanadium and titanium, difficult control of vanadium and titanium trend and low yield rate of extracting vanadium and titanium through converter blowing iron molten, etc. The invention has the advantages of high yield rate of vanadium, titanium and iron and high resources utilization rate and explores a novel practical way for comprehensive utilization of vanadium, titanium and iron concentrate ore.

The invention discloses a method for coal gasification in a combined type fluidized bed, which comprises coal preparation, gas supply, gasification, slag discharge, dedusting, waste heat recovery and fine powder conveying. An ash agglomeration fluidized bed realizes gasification of large-particle coal; the non-completely converted carryover fine powder enters an entrained flow bed gasifier in a dense phase pneumatic conveying manner; secondary gasification is carried out by using a short retention time high temperature gasification manner; the produced ash slag is carried into an intersection segment of the fluidized bed and the entrained flow bed with high temperature coal gas, and rapidly mixed with ''low temperature'' large-particle partially carbonized coal in the fluidized bed and the produced ''low temperature'' coal gas; and partial ash slag is selectively discharged out of the gasifier in the form of solid. The method and the device of the invention have the advantage of being suitable for various coal types and high in carbon conversion rate.

The invention discloses a beneficiation method for a pure magnetic iron ore. A crude ore is sequentially treated according to the steps such as first crushing, first-stage dry-type magnetic dressing, medium crushing, second-stage dry-type magnetic dressing, fine crushing and third-stage dry-type magnetic dressing, fine ore is obtained after a great amount of gangues are thrown by the third-stage dry-type magnetic dressing and sent to a grinding head sieve to be griddled and separated, granules griddled by the grinding head sieve are treated in a first-section magnetic dressing process, rough ore griddled by the grinding head sieve is treated in a first-section ball grinding and then enters the first-section magnetic dressing process; ore aggregates obtained from the first-section magnetic dressing process are treated in a second-section ball grinding after discharging gangue sands till the granularity of ore powder is -200meshes being more than or equal to 60 percent, ore powder generated from the second-section ball grinder are treated in second-section magnetic dressing, ore aggregates generated from the second-section magnetic dressing are treated in a high-frequency sieve after discharging gangue sands, products positioned on the high-frequency sieve are filtered to obtain ore concentrate, and products positioned below the high-frequency sieve are treated with desliming and then treated with floatation. The invention adopts two sections of grinding ore open-way processes and distinguishes the ore aggregates during the ore dressing process, thereby greatly reducing the energy consumption of a system, lowering the production cost and enhancing the utility ratio of equipment.

The invention discloses a manganese oxide molecular sieve-doped monolithic catalyst for decomposing ozone (O3) at room temperature and a preparation method thereof, which relates to the fields of catalysis and environmental protection. The preparation method is characterized in that a ceramic honeycomb monolithic type or porous foam metal carrier is adopted, and the manganese oxide molecular sieve doped with cobalt or titanium is taken as an active component. The manganese oxide molecular sieve doped with the cobalt or titanium is characterized in that: 1) the manganese oxide molecular sieve has Hollandite-typed manganese oxide octahedral molecular sieves (OMS-2) structure, the pore size is about 0.46nm multiplied by 0.46nm; 2) cobalt or titanium ions are introduced on a framework of the Hollandite-typed manganese oxide octahedral molecular sieves to form the manganese oxide molecular sieve doped with cobalt or titanium. An ozone decomposition catalyst is prepared by an oxidation reduction-refluxing method or an oxidation reduction-hydrothermal synthesis method, namely, the solution with manganese salt and cobalt salt or titanium salt is added with a strong oxidizer to synthesize the ozone decomposition catalyst by refluxing at the temperature of 90-200 DEG or hydrothermal process for more than 12 hours. The monolithic catalyst is characterized in that the input of additional energy sources such as light, heat, electricity, and the like, is unnecessary, and the ozone can be stably decomposed into oxygen under the conditions of normal temperature, normal humidity and large air volume.

The eddy cavitating unit used in the technological field of chemical separation consists of liquid inlet pipe and three coaxial cylinders including inner cylinder, middle cylinder and outer cylinder, the outer cylinder and the middle cylinder have individual tops with central inlet and common bottom, and the inner cylinder is a hollow cylinder and is connected to the middle cylinder via four radial cross beams. Or, the eddy cavitating unit consists of liquid inlet pipe, paraboloidal cone, disc with slit, flow guide plate and nozzle. Or, the eddy cavitating unit consists of liquid inlet pipe, outer paraboloidal cone, inner funnel cone and nozzle.

The invention discloses a method and a device for extracting lithium, which is used for preparing lithium carbonate, from a lapidolite ore by a chloridizing roasting method. The method comprises the following steps of: firstly, mixing the lapidolite ore, calcium chloride and sodium hydroxide with a compound bonding agent for pellet fabrication; secondly, performing chloridizing roasting in a square-frame shaped track type roasting furnace; thirdly, leaching out soot dust by using solution containing sodium carbonate and potassium carbonate to ensure that potassium, sodium, rubidium and cesium enter the solution and convert the lithium into lithium carbonate; fourthly, filtering the mixture to obtain a lithium carbonate solid, and circularly using the filtrated mother liquor to leach out the soot dust; fifthly, when an alkali metal salt is close to be saturated, indirectly heating the filtrated mother liquor by using the residual heat of the gas in the roasting furnace to evaporate part of water; sixthly, passing CO2 into the filtrated mother liquor to perform carbonation; and seventhly, performing cooling crystallization to separate out a mixed salt of the sodium carbonate and the potassium carbonate, returning part of the mixed salt which is used as an auxiliary material mixed and roasted with lapidolite for cyclic utilization, using another part of the mixed salt as a carbonate reagent needed in dissolution, and using the rest part of the mixed salt as byproducts of the sodium carbonate and the potassium carbonate. The method has the advantages of high lithium recovery rate, good material comprehensive utilization, large equipment productivity, high production efficiency, small water consumption in the process and less wastewater discharge.