The invention belongs to the technical field of
alloy foil preparation, and particularly relates to a preparation method of a FeCrCoW4.5
alloy foil. Comprising the following steps that N passes of cold rolling are conducted on a FeCrCoW4.5
alloy blank, N is larger than or equal to 3, the deformation amount of each pass of cold rolling is 40-70%, annealing treatment is conducted at the temperature of 1000-1200 DEG C after the last pass,
work hardening generated by cold rolling is eliminated, final cold rolling is conducted after annealing treatment till the thickness is 0.06 mm, and the alloy foil is obtained. Through multi-pass cold rolling and annealing combined
machining, during cold rolling, a large number of
dislocation and other defects can be generated in a material, so that the
hardness of the material is increased, and the
plasticity is reduced; and annealing is carried out after multi-pass cold rolling, atoms in the material can obtain certain energy,
dislocation and other defects are rearranged and combined, and part of the defects are eliminated, so that the
hardness of the material is reduced, certain
plasticity is recovered, and the comprehensive
mechanical property of the material is improved.