This invention discloses a method for preparing an ultrathin
zinc indium sulfide /
zinc selenide heterojunction photocatalyst: Step 1, a certain amount of ZnCl2, InCl3·4H2O and
oleylamine are mixed and subjected to a first
deoxygenation treatment. A
mixed solution of 1-dodecanethiol and tert-
dodecylmercaptan is rapidly injected under
nitrogen conditions and reacted at a certain temperature for a certain time to obtain ultrathin
zinc indium sulfide nanosheets. After
centrifugation and washing, the nanosheets are redissolved in a certain amount of n-
hexane. Step 2, zincacetate,
oleic acid and 1-
octadecene are mixed and subjected to a second
deoxygenation treatment. The mixture is then heated to a certain temperature under
nitrogen conditions, reacted for a certain time, and cooled. A certain amount of the solution obtained in step S1 is rapidly injected and subjected to a third
deoxygenation treatment. The mixture is then heated under
nitrogen conditions, and a certain amount of a
mixed solution of Se and TOP is slowly injected at a certain rate. The mixture is then kept at a certain temperature and reacted for a certain time. After the injection process is completed, the reaction is allowed to continue. Finally, the solution is cooled to
room temperature and centrifuged to obtain ZIS / ZnSeHNSs.