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97results about How to "Small absorption coefficient" patented technology

Device and method for automatic, static continuous preparation of fiber bragg grating array

A device for automatic, static continuous preparation of a fiber bragg grating array comprises an optical fiber paying-off module, a coating layer stripping module, an optical grating inscribing module, a coating module and a fiber winding module, wherein the optical fiber paying-off module, the coating layer stripping module, the optical grating inscribing module, the coating module and the fiber winding module are sequentially arranged in the optical fiber running direction. The optical fiber paying-off module comprises a coiling drum. The coating layer stripping module comprises a CO2 pulse laser, a first reflector, a second reflector, a focusing lens and a cylindrical surface reflector arranged in sequence. The optical grating inscribing module comprises an excimer laser and a phase mask plate. The coating module comprises an automatic ultraviolet light coating device. The fiber winding module comprises an automatic fiber winding device. A method for automatic, static continuous preparation of the fiber bragg grating array aims at non-hydrogen-loaded common fibers, and in the optical fiber paying-off and winding process, the method includes the first step of partially stripping coating layers of fibers through narrow-pulse infrared light, the second step of moving optical fiber portions of the stripped coating layers to the excimer laser for inscribing, the third step of moving the optical fiber portions after being inscribed to the ultraviolet light coating device for ultraviolet light coating and curing, and the fourth step of repeating the first step to the third step to carry out inscribing on multiple fiber bragg gratings to form the fiber bragg grating array.
Owner:WUHAN UNIV OF TECH +1

Method for distinguishing variety of fritillaria and detecting total alkaloid content of fritillaria by virtue of near infrared spectrum

The invention provides a method for distinguishing variety of fritillaria and detecting total alkaloid content of the fritillaria by virtue of near infrared spectrum. The method provided by the invention comprises the following steps: (1) collecting a fritillaria sample; (2) measuring the near infrared diffuse reflection spectrogram of the fritillaria sample, preprocessing the 4000-5000cm<-1> wave band in the spectrogram, and performing cluster analysis on the pre-processed near infrared spectrogram to build a qualitative model; or preprocessing the 4000-7000cm<-1> wave band in the spectrogram, so as to obtain an absorbance, associating the absorbance with the alkaloid content of the sample measured by virtue of bromothymol blue colorimetry, and building a quantitative correction model for detecting alkaloid by one or more methods of a partial least squares method, a principal component regression method and a multiple linear regression method; (3) collecting the near infrared spectrogram of the sample to be measured, after the corresponding preprocessing is performed, distinguishing the variety of the fritillaria and detecting total alkaloid content of the fritillaria by utilizing the built qualitative model or quantitative correction model. The method provided by the invention has the characteristics of fast speed, no damage, environment friendliness and low cost.
Owner:DALIAN UNIV OF TECH

Preparation method of ultraviolet fluorescent-green plastic film by taking rare-earth phosphate glass as photochromic agent and application thereof in anti-counterfeiting aspects

The invention relates to a preparation method of an ultraviolet fluorescent-green plastic film by taking rare-earth phosphate glass as a photochromic agent and application thereof in anti-counterfeiting aspects. Aiming at the problems of doped rare-earth fluorescent polymer materials, such as large polarity difference between an inorganic rare-earth fluorescent agent and a polymer material, rare-earth fluorescent concentration quenching, fluorescence stability and the like, the ultraviolet fluorescent-green plastic film has the characteristics that the phosphate glass is used as the substrate, Tb<3+> ion is used as a fluorescent activator, and Ce<3+> ion is used as a sensitizing agent, so that the fluorescent concentration quenching phenomenon is overcome, and the Eu addition amount and the fluorescence efficiency are increased through the synergistic effect of the phosphate glass matrix, Tb<3+> and Ce<3+> in the formula; glass fragments are pressed by using a melting method and an ice water mixture cooled glass tablet press, and then, the phosphate glass:Tb<3+>, Ce<3+> fluorescent powder with the granularity of being less than 300 nm is prepared through high-pressure grinding of an air-current mill; a surface modifier is added, fluorescent powder and polymer master-batch are molten and blended, and the plastic film obtained by being blown is white and transparent in the sun and emits beautiful green light under irradiation of ultraviolet light; and the plastic film has special transmission spectrum and can be used as an anti-counterfeiting packaging film, an anti-counterfeiting label printing substrate and an anti-counterfeiting safety line substrate.
Owner:BEIJING INSTITUTE OF GRAPHIC COMMUNICATION

Preparation method of KTP crystal with anti-soil performance

The invention discloses a method for preparing a KTP crystal capable of resisting gray track, comprising the following steps that: 1) KH2PO4 and TiO2 as raw materials used to synthesize a KTiOPO4 crystal, and K2HPO4 as the raw material used to synthesize a K4P2O7(K4) solvent are mixed according to a certain ratio, and the initial growth mol ratio of the KTiOPO4 to the K4P2O7 obtained after the chemical reaction is about 0.8; 2) the mixed raw materials are put in a platinum crucible and the solution filling amount is between 75 and 85 percent; 3) the platinum crucible is put in a furnace body, a temperature gradient of the furnace is set to be between 3 and 8 DEG C per 10 centimeters, and the furnace is heated so that the raw materials are melted and react to form an even and stable high temperature solution; and 4) the seed crystal is put in the high temperature solution, the temperature is reduced at a temperature gradient of between 1 and 8 DEG C per 100 hours, and the KTiOPO4 crystal is grown at a temperature interval of between 850 and 820 DEG C. The method utilizes the K4P2O7 solvent to prepare the KTP crystal, reduces the absorption coefficient of the KTP crystal, and has evident anti-gray track performance; therefore, the frequency multiplication conversion efficiency of the KTP is improved further, the KTP crystal has good voltage withstanding and modulation performances and can be used as an electrooptical crystal.
Owner:BRIGHT CRYSTALS TECH

Synthesis method for selenium germanium gallium barium polycrystal and growth method for selenium germanium gallium barium monocrystal

The invention discloses a synthesis method for a selenium germanium gallium barium polycrystal and a growth method for a selenium germanium gallium barium monocrystal. The growth of the polycrystal comprises the following steps: putting elemental Ga, elemental Ba and elemental Ge into a PBN boat; then placing the PBN boat at one end of a quartz tube and placing elemental Se at the other end of thequartz tube; conducting vacuumizing, and then carrying out heat sealing; and then putting the quartz tube into a horizontal double-temperature-region resistor furnace for synthesizing, so as to obtain a high-purity single-phase selenium germanium gallium barium polycrystal raw material, wherein the yield of the raw material is greater than 99%. The growth of the selenium germanium gallium bariummonocrystal comprises the following steps: adding the selenium germanium gallium barium polycrystal into a crystal growth crucible and vertically placing the crystal growth crucible into a quartz tube; conducting vacuumizing, and then carrying out heat sealing; and then putting the quartz tube into a vertical double-temperature-region resistor furnace, so as to obtain the selenium germanium gallium barium monocrystal after the growth of the monocrystal is finished. The selenium germanium gallium barium monocrystal obtained by the method disclosed by the invention has the advantages of few defects, high infrared band transmission rate and the like and can be used as a far infrared laser frequency conversion material.
Owner:TECHNICAL INST OF PHYSICS & CHEMISTRY - CHINESE ACAD OF SCI

Visual three-temperature-area gallium selenide single crystal growth device and method

The inventiondiscloses avisual three-temperature-area gallium selenide single crystal growth device and method, and relates to a crystal growth device and method. The invention aims to solve technicalproblems of uneven stress distribution and low transmittance of gallium selenide single crystal grown by using a bridgman-stockbarger method in the prior art. The device comprises an outer sleeve, aninner sleeve, a heating resistance wire, an annular cavity, a reflection film, a temperature thermocouple, an end cap, and a heat preservation plug; the reflection film is attached to the inner wallof the outer sleeve; the annular cavity between the outer sleeve and the inner sleeve which are prepared from transparent materials is a vacuum cavity; and the heating resistance wire is arranged in the annular cavity. The method comprises the following steps: placing gallium selenide crystal seeds in a PBN boat, obliquely sealing in a vacuum quartz tube in a suspended manner, placing the quartz tube in the middle of the growth device, adjusting the temperature gradient of the three temperature areas, melting a part of the crystal seeds, fully melting polycrystal materials, then cooling for curing, and finally cooling to the room temperature to obtain allium selenide single crystals. The transmittance of the single crystals is 64%-66%, and the single crystals can be applied in civil and national defense fields.
Owner:HARBIN INST OF TECH

System and method for improving anti-radiation capability of BOTDR (Brillouin Optical Time-Domain Reflectometry)

The invention discloses a method for improving the anti-radiation capability of a BOTDR. According to the characteristics that loss of sensing fibers is increased and the action range of Brillouin backward scattering light signals is decreased in the radiation environment, a light pulse sequence is input to the radiated fiber at interval, so that the radiated fiber is full of the light pulse sequence at interval, the Brillouin backward scattering light signals of higher signal to noise ratio are obtained in the interval segments, splicing recombination and matrix transformation coding are carried out on the signals collected in the interval segments, and system response to the whole fiber is obtained. The temperature or strain is sensed according to the relation between Brillouin frequency shift and the frequency/strain. The invention also discloses a system for improving the anti-radiation capability of the BOTDR. The fiber is full of the light pulse sequence at interval, so that the input power is improved, fiber loss caused by radiation is reduced, and the anti-radiation capability of the fiber is improved. Adverse influence caused by fiber loss is avoided, and the anti-radiation capability of the BOTDR system is improved.
Owner:NANJING UNIV

Method for preparing ultraviolet fluorescent red plastic film by taking rare earth phosphate glass as photochromic agent and application of ultraviolet fluorescent red plastic film in aspect of anti-counterfeiting

InactiveCN104262781AGive full play to the fluorescent functionIncrease incorporationStampsIdentification meansRare-earth elementIce water
The invention discloses a method for preparing an ultraviolet fluorescent red plastic film by taking rare earth phosphate glass as a photochromic agent and an application of the ultraviolet fluorescent red plastic film in the aspect of anti-counterfeiting. For solving the problems of large polarity difference between an inorganic rare earth fluorescent agent and a high polymer material, fluorescent concentration quenching and fluorescent stability and the like of a doped rare earth fluorescent high polymer material, by taking phosphate glass as a matrix, taking Eu<3+> ions as a fluorescent activator and taking Ce<3+> ions as a sensitizer, through the synergistic effect of the phosphate glass matrix, the Eu<3+> and the Ce<3+> in a formula, a fluorescent concentration quenching phenomenon is overcome, thereby improving the adding amount and fluorescence efficiency of rare earth element Eu; glass fragments are prepared by pressing through using a melting method and an ice-water mixture cooling glass sheeter, and then the glass fragments are subjected to high-pressure grinding by using an air-current mill so as to prepare phosphate glass with a particle size of less than 300 nm and containing Eu<3+>, Ce<3+> and fluorescent powder; and a surface modifier is added and fluorescent powder and polymer masterbatches are subjected to melt blending, then a plastic film prepared by film blowing is white and transparent in daylight, and emits bright red light under ultraviolet-irradiation, and the plastic film has special transmission spectrum, and can be used as an anti-counterfeiting packaging film, an anti-counterfeiting label printing base material and an anti-counterfeiting safety line base material.
Owner:BEIJING INSTITUTE OF GRAPHIC COMMUNICATION
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