The application belongs to the field of chemical detection and analysis, and particularly relates to a method for analyzing
potassium hydroxide in a hydrazine
boronic acid system, comprising the following steps: step 1, adding
hydrogen peroxide to a sample for sample pretreatment; step 2, adding
bromothymol blue indicator to the pretreated sample, titrating the pretreated sample with
hydrochloric acid, and recording the volume of
hydrochloric acid consumed by the sample; step 3, performing a blank test, and recording the volume of
hydrochloric acid consumed by the blank test; step 4, calculating the concentration of KOH in the sample, denoted as a measured concentration; and step 5, calculating the difference of the measured concentration, and determining the concentration of KOH in the sample. The method can solve the interference of a weak acid and
weak base system on the
titration of
potassium hydroxide, and can quickly and accurately analyze the concentration of
potassium hydroxide in a potassium hydrazine
boronic acid alkali solution by adding
hydrogen peroxide for pretreatment and selecting
bromothymol blue as an indicator.