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3549 results about "Test solution" patented technology

Test solution. n. A solution of a reagent in a specified strength, used in chemical analysis or testing.

Bridge field static load test evaluation method

ActiveCN104933285AEffective and comprehensive assessmentImprove securitySpecial data processing applicationsElement modelEvaluation Interval
The present invention relates to a bridge field static load test evaluation method, which is mainly a method for evaluating the bearing capacity and adaptation performance of a bridge by means of a field static load test. The method comprises the following steps: (1) determining specific content and method for collecting relevant data for early stage preparation work; (2) establishing a reasonable and accurate bridge structure finite element model according to the collected data; (3) calculating and analyzing a result according to an endogenous force and a stress of the bridge under dead and live loads, and determining theoretical force bearing safety and live load force bearing characteristics; (4) in combination with a traditional key section of the bridge, determining a bridge test section and completing static load test solution designing; (5) performing the field static test for the bridge and processing the test data; (6) studying an evaluation interval corresponding to a preset test evaluation indicator; and (7) making a reasonable and comprehensive assessment on the structural performance of the bridge. The evaluation method and indicator according to the present invention can more effectively indicate the practical bearing capacity and applicability of the bridge in a refined manner, and improving the reasonability and accuracy of the evaluation result.
Owner:SOUTHWEST JIAOTONG UNIV

Method for measuring contents of aluminum, titanium, manganese, nickel, tungsten and iron in cobalt-base alloy

The invention belongs to a technique for analyzing elements of an alloy, and relates to a method for measuring the contents of aluminum, titanium, manganese, nickel, tungsten and iron in a cobalt-base alloy. The method adopts an inductively coupled plasma atomic emission spectrometer and is different according to different measured elements and different tungsten contents; when high-content tungsten is dissolved, the volume of test solution needs to be maintained between 20 and 40 mL, or the tungsten is easy to be separated out; by performing interference experiments and spectrogram analyses, the method finds the optimal analytical line, overcomes the interferences caused by a plurality of elements such as major elements of cobalt, chromium, tungsten and the like in the cobalt-base alloy, and improves the measuring accuracy; the sample dissolving speed is accelerated, and the sample dissolving time is shortened to 2 hours from about two or three days; and the method has wide measuring ranges including: 0.05 to 0.30 percent of the aluminum, 0.05 to 0.30 percent of the titanium, 0.05 to 1.00 percent of the manganese, 0.05 to 24.00 percent of the nickel, 0.05 to 20.00 percent of the tungsten, and 0.05 to 3.00 percent of the iron.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS

Method for detecting element content in alloy or ore by utilizing ICP emission spectrometer

The invention relates to a method for detecting the element content in alloy or ore by utilizing an ICP emission spectrometer, comprising the following steps: placing the alloy or the ore in solvent,heating and leading the alloy or the ore to be dissolved fully in solution to obtain mixed solution; diluting the mixed solution to obtain test solution; selecting the optimal analysis line of each element according to the composition of substrate of the alloy or the ore; preparing a set of corresponding standard solutions with the concentration sequencing from low to high according to the concentration index of each element in the alloy or the ore; introducing the standard solutions to the ICP emission spectrometer to measure the emission light intensity of the element analysis line and to draw a standard curve; introducing the test solution to the ICP emission spectrometer to measure the emission light intensity corresponding to each element; and determining the content of each element according to the standard curve. The method can detect simultaneously the content of the required element and oxide only by one solution, therefore, the invention has simple operation, shortened measuring cycle, stable detection results with high accuracy degree.
Owner:DATONG ELECTRIC LOCOMOTIVE OF NCR

High performance liquid chromatography detection method for residual quantity of multiple ultraviolet absorbents in cosmetics

The invention relates to the field of analytical chemistry and food safety, and provides a high performance liquid chromatography detection method for residual quantity of multiple ultraviolet absorbents in cosmetics. A cosmetic sample of 0.4g is weighed and placed in a plastic centrifuge tube of 50 ml, sample extraction liquid of 20ml is added, after the cosmetic sample of 0.4g and the sample extraction liquid of 20ml are mixed for 2 minutes in a vortex mode, sonic oscillation extraction is carried out for 20 minutes, 8000 revolutions per minute centrifugation is carried out for 10 minutes and, and supernate is to be purified; and after test solutions sequentially pass through microfiltration membranes of 0.45 micrometer and 0.20 micrometer, a high performance liquid chromatograph is adopted to carry out qualitative determination and quantitative assay. The detection method has the advantages of being simple, fast, accurate, efficient, and the like, and can detect 12 ultraviolet absorbents at the same time. Technical indexes of detection minimum, the recovery rate, the degree of precision, and the like all meet relevant demands for ultraviolet absorbent detection in sun block cosmetics at home and abroad. The method is suitable for detection and monitoring of the ultraviolet absorbents in the sun block cosmetics, and has great significance on promoting of import and export trade of cosmetics of our country, ensuring of safety of the cosmetics, and guarantee of human body health.
Owner:林维宣

Test method of micro amount of arsenic or antimony in steel

The invention relates to a test method of steel, in particular to a test method of a micro amount of arsenic or antimony in steel. The test method is based on a principle of a flow injection-hydride generation-atomic absorption spectroscopic methodology, and experiments are determined in a flow-injection sample-injection mode. The method comprises the following steps: a test solution is reduced bya thiourea-ascorbic acid mixed solution and a hydrochloric acid solution to convert arsenic (V) into arsenic (III), and convert antimony (V) into antimony (III); the test solution reacts with a potassium borohydride solution under a carrier band of a carrier solution to generate a great amount of nascent oxygen which reacts with the arsenic (III) or the antimony (III) to generate gaseous AsH3 orSbH3; the AsH3 or the SbH3 is led into a specially-designed quartz tube by high-purity argon gas as carrier gas and is atomized into ground-state atomic vapor; ground-state electrons which are on theoutermost layer of the atom are excited by the light energy of a light source of a hollow cathode lamp to transit to a high energy level; and the amount of abortion light intensity is directly proportional to the concentration of the atom. Accordingly, the arsenic or antimony content in the test solution can be quantitatively analyzed.
Owner:CHINA YITUO GROUP

Method for detecting pyrethroid pesticide residue amount in smoke by cigarette filter

The invention discloses a method for detecting pyrethroid pesticide residue amount in smoke by a cigarette filter, belonging to the technical field of tobacco chemical analysis. The method comprises the following steps: placing a sucked filter tip at standard smoking condition into a 150ml of bottle with a tapered plug; adding 100mL of mixed solvent of ethyl acetate and cyclohexane with the volume ratio of 1:1; placing the bottle on an ultrasonic wave generator for extraction for 30min; concentrating to be 0.5mL on a rotary evaporator after drying by anhydrous sodium sulfate; setting the volume to be 2mL by normal hexane to be purified; placing a small graphite carbon black column on a solid phase extractor; activating by 3mL of acetone and 3mL of normal hexane in sequence; transforming the sample test solution to be purified into the small graphite carbon black column; eluting for two times by utilizing 2.5mL of mixed solvent of acetone and normal hexane, wherein the speed does not exceed 5.0mL/min; evaporating and concentrating eluent; setting the volume to be 1.5mL by acetone and normal hexane with the volume ratio of 2:8; and analyzing on GC-ECD. The method of the invention is simple and accurate, and can effectively determine pyrethroid pesticide residue amount in smoke by the cigarette filter.
Owner:YUNNAN RES INST OF TOBACCO SCI

Method for constructing dual-chamber microbial fuel cell-type BOD (biochemical oxygen demand) sensor by using potassium permanganate as cathode electron acceptor

The invention provides a method for constructing a dual-chamber microbial fuel cell (MFC)-type BOD (biochemical oxygen demand) sensor by using potassium permanganate as cathode electron acceptor, which belongs to the field of waste water quality monitoring. The method specially comprises the steps of constructing a dual-chamber MFC reactor; enriching electricigenic microorganisms on an MFC anode plate, and adjusting an external resistor to obtain maximum MFC output power; respectively adding different concentrations of artificial sewage and potassium permanganate solution into an anode chamber and a cathode chamber of the MFC, calculating the generated electricity of the MFC corresponding to different BOD concentrations according to MFC output current and detection time; and processing the generated electricity and BOD by linear fitting to obtain a sensor detection limit and a linear equation. After a to-be-tested solution with unknown BOD value is added into the anode chamber of the MFC, the generated electricity of the MFC is calculated according to the MFC output current and the detection time; and the BOD value of the to-be-tested solution can be calculated according to the known linear equation. The MFC-type BOD sensor using potassium permanganate as cathode electron acceptor has the advantages that the BOD detection range is widened to be 500mg/L; the detection time is shortened by 50% or more; and the detection relative error is less than 10%. Accordingly, the MFC-type BOD sensor has a high application value.
Owner:BEIJING FORESTRY UNIVERSITY
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