The embodiment of the invention provides a detection method and a detection device for total
sulfur in domestic
sludge. The detection method comprises the following steps: respectively weighing a to-be-detected domestic
sludge sample and an Escherka
reagent, putting the two into a
crucible, and uniformly mixing; the
crucible is placed in heating equipment to be subjected to staged temperature rising and heating; cooling after heating is finished,
mashing a burnt material in the
crucible, transferring the mashed burnt material into a
beaker, continuously adding dilute
nitric acid and distilled boiling water into the
beaker, and carrying out boiling water bath; performing centrifugal motion on the
beaker, extracting supernatant liquid in the beaker, and fixing the volume of the extracted supernatant liquid to a third volume; part of the solution with the third volume is extracted into a storage
bottle, an
yttrium element solution with the preset
solubility is added into the storage
bottle, deionized water is used for
dilution to a preset scale, and then the total
sulfur content is measured through a
plasma emission spectrometer. The detection method disclosed by the embodiment of the invention is simple to operate, high in
recovery rate and small in measurement interference.